PdClHN(C₂H₄As(CH₃)2)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=PdClHN(C₂H₄As(CH₃)2)2B(C₆H₅)4

Base Information

• Chemical Name: PdClHN(C₂H₄As(CH₃)2)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=PdClHN(C₂H₄As(CH₃)2)2B(C₆H₅)4
• CAS No.: 117074-88-1
• Molecular Formula: C₈H₂₁As₂ClNPd*C₂₄H₂₀B
• Molecular Weight: 742.211
• Mol file: 117074-88-1.mol

Synonyms:

Chemical Property of PdClHN(C₂H₄As(CH₃)2)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=PdClHN(C₂H₄As(CH₃)2)2B(C₆H₅)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of PdClHN(C₂H₄As(CH₃)2)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=PdClHN(C₂H₄As(CH₃)2)2B(C₆H₅)4

There total 1 articles about PdClHN(C₂H₄As(CH₃)2)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=PdClHN(C₂H₄As(CH₃)2)2B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium tetrachloropalladate(II) + sodium tetraphenyl borate (143-66-8) + bis<-2(dimethylarsinoethyl)>amine (117013-44-2) → PdClHN(C2H4As(CH3)2)2(1+)*B(C6H5)4(1-)=PdClHN(C2H4As(CH3)2)2B(C6H5)4 (117074-88-1)

Guidance literature:

In acetonitrile; to acetonitrile soln. of Pd compd. was added soln. of amine with stirrind and NaBPh4 both in CH3CN, after stirring for 13 h mixt. was evapd. in vac., residue dissolved in CH2Cl2; soln. filtered, evapd. to dryness, washed with ether and dried in. vac.; elem. anal.;

DOI:10.1002/recl.19881070708

upstream raw materials:

sodium tetraphenyl borate

bis<-2(dimethylarsinoethyl)>amine