trans-[Pd(C₆H₃-5-CF₃-O-2-(C₆H₅O₂))I(PPh₃)2]

Base Information

Chemical Name:trans-[Pd(C₆H₃-5-CF₃-O-2-(C₆H₅O₂))I(PPh₃)2]
CAS No.:1259387-51-3
Molecular Formula:C₄₉H₃₈BrF₃O₃P₂Pd
Molecular Weight:980.106
Hs Code.:

trans-[Pd(C<sub>6</sub>H<sub>3</sub>-5-CF<sub>3</sub>-O-2-(C<sub>6</sub>H<sub>5</sub>O<sub>2</sub>))I(PPh<sub>3</sub>)2]

Synonyms:

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Chemical Property of trans-[Pd(C₆H₃-5-CF₃-O-2-(C₆H₅O₂))I(PPh₃)2]

Chemical Property:

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Technology Process of trans-[Pd(C₆H₃-5-CF₃-O-2-(C₆H₅O₂))I(PPh₃)2]

There total 2 articles about trans-[Pd(C₆H₃-5-CF₃-O-2-(C₆H₅O₂))I(PPh₃)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0)

: 1259312-92-9
4-(2-bromo-4-(trifluoromethyl)phenoxy)-6-methyl-2-pyrone

: 603-35-0
triphenylphosphine

: 1259387-51-3
trans-[Pd(C₆H₃-5-CF₃-O-2-(C₆H₅O₂))I(PPh₃)2]

Guidance literature:: In tetrahydrofuran-d8; a soln. of Pd-complex and 4 equiv of P(C6H5)3 in THF-d8 was stirred under N2 at ambient temp. for 15 min, 2 equiv of pyrone-compound was added, the soln. was stirred for 1 h at 70°C; not sepd., detected by NMR spectra;
DOI:10.1039/c0dt00421a

Reference yield:

: tris(dibenzylideneacetone)dipalladium ⁽⁰⁾

: 1259312-92-9
4-(2-bromo-4-(trifluoromethyl)phenoxy)-6-methyl-2-pyrone

: 603-35-0
triphenylphosphine

: 1259387-51-3
trans-[Pd(C₆H₃-5-CF₃-O-2-(C₆H₅O₂))I(PPh₃)2]

Guidance literature:: In tetrahydrofuran; a soln. of Pd-complex and 4 equiv of P(C6H5)3 in THF was stirred under N2 at ambient temp. for 15 min, 2 equiv of pyrone-compound was added, thesoln. was stirred for 1 h at 70°C; THF was removed in vac., dissolved in diethyl ether, stored at room temp. for 16 h;
DOI:10.1039/c0dt00421a