1-ethyl-2(1H)-quinolinone (1-ethyl-2(1H)-quinolinylidene)hydrazone

Base Information

• Chemical Name: 1-ethyl-2(1H)-quinolinone (1-ethyl-2(1H)-quinolinylidene)hydrazone
• CAS No.: 2814-57-5
• Molecular Formula: C22H22N4
• Molecular Weight: 342.443
• Mol file: 2814-57-5.mol

Synonyms:Bis-(1-aethyl-1H-[2]chinolyliden)-hydrazin;N,N'-Bis-[1-ethyl-1H-quinolin-(2Z)-ylidene]-hydrazine;1-Ethylchinolon-(2)-azin;bis-(1-ethyl-1H-[2]quinolylidene)-hydrazine;

Chemical Property of 1-ethyl-2(1H)-quinolinone (1-ethyl-2(1H)-quinolinylidene)hydrazone

Chemical Property:

• PSA: 34.58000
• LogP: 4.05240

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-ethyl-2(1H)-quinolinone (1-ethyl-2(1H)-quinolinylidene)hydrazone

There total 3 articles about 1-ethyl-2(1H)-quinolinone (1-ethyl-2(1H)-quinolinylidene)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.3%

2-Azido-1-ethylchinolinium-tetrafluoroborat → 2-aminoquinoline (580-22-3) + 1-Ethyl-1,2-dihydro-2-iminochinolin (54677-32-6) + 1-Ethyl-1,2-dihydrochinolin-2-on (53761-50-5) + 1-ethylchinolin-2(1H)-on-azin (2814-57-5)

Guidance literature:

With tetrafluoroboric acid; In water; for 0.5h; Irradiation;

DOI:10.1002/hlca.19870700810

Reference yield:

2-Azido-1-ethylchinolinium-tetrafluoroborat → 1-Ethyl-1,2-dihydrochinolin-2-on (53761-50-5) + 1-ethylchinolin-2(1H)-on-azin (2814-57-5) + 1-ethylchinolinium-2(1H)-methoxyimin + 2-amino-1-ethylchinolinium-tetrafluoroborat

Guidance literature:

With tetrafluoroboric acid; In methanol; for 0.416667h; Further byproducts given; Irradiation;

DOI:10.1002/hlca.19870700810

Reference yield:

2-Azido-1-ethylchinolinium-tetrafluoroborat → 1-Ethyl-1,2-dihydrochinolin-2-on (53761-50-5) + 1-ethylchinolin-2(1H)-on-azin (2814-57-5) + 1-ethylchinolinium-2(1H)-methoxyimin + 2-amino-1-ethylchinolinium-tetrafluoroborat + 1,1'-diethyl-2,2'-azodi + C22H22N4(1+)*BF4(1-)

Guidance literature:

With tetrafluoroboric acid; In methanol; for 0.416667h; Mechanism; Irradiation;

DOI:10.1002/hlca.19870700810

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