PotassiuM thiobenzoate, 95%

Base Information

• Chemical Name: PotassiuM thiobenzoate, 95%
• CAS No.: 28170-13-0
• Molecular Formula: C7H6OS.K
• Molecular Weight: 176.28
• Mol file: 28170-13-0.mol

Synonyms:thiobenzoic acid , potassium-compound;potassium thiobenzoate;thiobenzoic acid, potassium salt;potassium benzothioate;

Chemical Property of PotassiuM thiobenzoate, 95%

Chemical Property:

• Melting Point: >260 °C (decomp)
• PSA: 17.07000
• LogP: 1.37370

Purity/Quality:

99% ^*data from raw suppliers

BENZENECARBOTHIOICACID,POTASSIUMSALT 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Potassium thiobenzoate is used as an organic chemical synthesis intermediate.

Technology Process of PotassiuM thiobenzoate, 95%

There total 1 articles about PotassiuM thiobenzoate, 95% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

thiobenzoic acid (98-91-9) → thiobenzoic acid potassium salt (28170-13-0)

Guidance literature:

With potassium hydroxide; In methanol; ethanol; at 50 ℃; for 2.5h; Time;

Reference yield: 94.0%

thiobenzoic acid potassium salt (28170-13-0) + 1-bromo-octane (111-83-1) → S-1-octyl benzothioate (10489-23-3)

Guidance literature:

With silica gel; In benzene; at 80 ℃; for 4h;

DOI:10.1081/SCC-120025193

Reference yield: 91.0%

thiobenzoic acid potassium salt (28170-13-0) + C12H20N2O6S → C18H22N2O4S (141818-73-7)

Guidance literature:

In dimethyl sulfoxide; at 110 ℃; for 6h; Temperature; Inert atmosphere;

upstream raw materials:

thiobenzoic acid

Downstream raw materials:

bis-benzoylmercapto-phenyl-methane

thiobenzoic acid S-[2]quinolylmethyl ester

bis-benzoylmercapto-methane

(S)-benzoylmercaptosuccinic acid

Refernces

• 1、 Kato, Shinzi,Oguri, Motohiro,Ishida, Masaru. "A Convenient Preparation of Anhydrous Alkali Metal Thiocarboxylates". . p. 1585 - 1590. Retrieved 2007/10/02.