Technology Process of Ditelluride, bis(4-bromophenyl)
There total 10 articles about Ditelluride, bis(4-bromophenyl) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tellurium; potassium hydroxide;
In
dimethyl sulfoxide;
at 90 ℃;
for 4h;
regioselective reaction;
DOI:10.1055/s-0033-1338488
- Guidance literature:
-
4-bromophenyl halide;
With
iodine; magnesium;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
With
tellurium;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
With
ammonium chloride;
In
tetrahydrofuran; ethyl acetate;
for 2h;
DOI:10.1016/j.tetlet.2009.12.028
