Technology Process of 1,3,5-Trihydroxy-2,4-bis(3-methyl-2-butenyl)-9(10H)-acridinone
There total 8 articles about 1,3,5-Trihydroxy-2,4-bis(3-methyl-2-butenyl)-9(10H)-acridinone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium ethanolate;
palladium on activated charcoal;
In
ethanol;
for 0.666667h;
Heating;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 900 mg / methanol; diethyl ether / 12 h / 0 °C
2: 10 mg / conc. H2SO4 / 12 h
3: 4 g / NaHCO3, NaI / acetone / 18 h / Heating
4: 200 mg / BF3 etherate / dioxane / 2 h
5: 50 mg / NaI, K2CO3 / acetone / 6 h / Heating
6: 25 mg / K2CO3 / acetone / 12 h / Heating
7: 6 mg / NaOEt / 10percent Pd-C / ethanol / 0.67 h / Heating
With
sulfuric acid; boron trifluoride diethyl etherate; sodium ethanolate; sodium hydrogencarbonate; potassium carbonate; sodium iodide;
palladium on activated charcoal;
In
1,4-dioxane; methanol; diethyl ether; ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 200 mg / BF3 etherate / dioxane / 2 h
2: 50 mg / NaI, K2CO3 / acetone / 6 h / Heating
3: 25 mg / K2CO3 / acetone / 12 h / Heating
4: 6 mg / NaOEt / 10percent Pd-C / ethanol / 0.67 h / Heating
With
boron trifluoride diethyl etherate; sodium ethanolate; potassium carbonate; sodium iodide;
palladium on activated charcoal;
In
1,4-dioxane; ethanol; acetone;