2-(chloro-phenyl-arsino)-benzoic acid

Base Information

• Chemical Name: 2-(chloro-phenyl-arsino)-benzoic acid
• CAS No.: 861294-13-5
• Molecular Formula: C₁₃H₁₀AsClO₂
• Molecular Weight: 308.596
• Mol file: 861294-13-5.mol

Synonyms:

Chemical Property of 2-(chloro-phenyl-arsino)-benzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(chloro-phenyl-arsino)-benzoic acid

There total 1 articles about 2-(chloro-phenyl-arsino)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-Carboxybenzenediazonium (17333-86-7) + dichlorophenylarsine (696-28-6) → 2-(chloro-phenyl-arsino)-benzoic acid (861294-13-5)

Guidance literature:

With alkali; durch Reduktion des Reaktionsprodukts mit Schwefeldioxyd in salzsaurer Loesung bei 80grad und anschliessende Behandlung mit Chlorwasserstoff in Benzol;

Reference yield:

2-(chloro-phenyl-arsino)-benzoic acid (861294-13-5) → 2-arsenoso-benzophenone (861307-31-5)

Guidance literature:

Multi-step reaction with 3 steps

1: chloroform; phosphorus pentachloride

2: aluminium chloride; carbon disulfide / beim Zersetzen des Reaktionsprodukts mit Salzsaeure

3: NaOH-solution

With carbon disulfide; sodium hydroxide; aluminium trichloride; chloroform; phosphorus pentachloride;

Reference yield:

2-(chloro-phenyl-arsino)-benzoic acid (861294-13-5) → 2-(chloro-phenyl-arsino)-benzoyl chloride (861294-14-6)

Guidance literature:

With chloroform; phosphorus pentachloride;

upstream raw materials:

o-Carboxybenzenediazonium

dichlorophenylarsine

Downstream raw materials:

2-(chloro-phenyl-arsino)-benzoyl chloride

2-arsenoso-benzophenone

o-dichloroarsinobenzophenone

(2-benzoyl-phenyl)-arsonic acid