4-(phenylsulfonyl)benzonitrile

Base Information

• Chemical Name: 4-(phenylsulfonyl)benzonitrile
• CAS No.: 28525-13-5
• Molecular Formula: C13H9NO2S
• Molecular Weight: 243.286
• Hs Code.: 2926909090
• Mol file: 28525-13-5.mol

Synonyms:4-Phenylsulfon-benzonitril;4-Phenylsulfon-benzoesaeure-nitril;4-benzenesulfonylbenzonitrile;4-Benzolsulfonyl-benzaldehyd;4-phenylsulfonyl-azetidinone;4-Benzosulfonyl-benzaldehyd;4-Benzolsulfonyl-benzonitril;4-benzenesulfonyl-azetidin-2-one;

Chemical Property of 4-(phenylsulfonyl)benzonitrile

Chemical Property:

• PSA: 66.31000
• LogP: 3.47188
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-(Phenylsulfonyl)benzonitrile 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(phenylsulfonyl)benzonitrile

There total 25 articles about 4-(phenylsulfonyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-iodobenzonitrile (3058-39-7) + sodium benzenesulfonate (873-55-2) → 4-(phenylsulfonyl)benzonitrile (28525-13-5)

Guidance literature:

With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; caesium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h; Inert atmosphere; Irradiation;

DOI:10.1002/chem.201905281

Reference yield: 95.0%

4-fluorobenzonitrile (1194-02-1,143234-87-1) + sodium benzenesulfonate (873-55-2) → 4-(phenylsulfonyl)benzonitrile (28525-13-5)

Guidance literature:

In dimethyl sulfoxide; at 130 ℃; for 16h;

DOI:10.1021/jo00280a045

Reference yield: 93.0%

4-cyanophenyldiazonium tetrafluoroborate (2252-32-6) + sodium benzenesulfonate (873-55-2) → 4-(phenylsulfonyl)benzonitrile (28525-13-5)

Guidance literature:

With eosin; In water; acetonitrile; at 20 ℃; for 12h; Irradiation; Inert atmosphere;

DOI:10.1039/c9ob00864k

upstream raw materials:

benzenesulfonamide

4-(phenylsulfonyl)benzoic acid

4-benzenesulfonyl-benzoic acid amide

4-fluorobenzonitrile

Downstream raw materials:

3,4-diphenyl-furazan 2-oxide

5-(4-benzenesulfonyl-phenyl)-3-phenyl-[1,2,4]oxadiazole

4'-(phenylsulfonyl)acetophenone

4-(phenylsulfonyl)benzaldehyde