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Technology Process of C5H5FeCO(P(C6H5)3)CCNCH2

C5H5FeCO(P(C6H5)3)CCNCH2

Base Information
  • Chemical Name:C5H5FeCO(P(C6H5)3)CCNCH2
  • CAS No.:114657-25-9
  • Molecular Formula:C27H22FeNOP
  • Molecular Weight:463.299
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>FeCO(P(C<sub>6</sub>H<sub>5</sub>)3)CCNCH<sub>2</sub>

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Chemical Property of C5H5FeCO(P(C6H5)3)CCNCH2
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Technology Process of C5H5FeCO(P(C6H5)3)CCNCH2

There total 1 articles about C5H5FeCO(P(C6H5)3)CCNCH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(cyclopentadienyl)(CO)(PPh3)FeH

(cyclopentadienyl)(CO)(PPh3)FeH

propiolonitrile
1070-71-9

propiolonitrile

C<sub>5</sub>H<sub>5</sub>FeCO(P(C<sub>6</sub>H<sub>5</sub>)3)CHCHCN
114681-02-6

C5H5FeCO(P(C6H5)3)CHCHCN

C<sub>5</sub>H<sub>5</sub>FeCO(P(C<sub>6</sub>H<sub>5</sub>)3)CCNCH<sub>2</sub>
114657-25-9

C5H5FeCO(P(C6H5)3)CCNCH2

Guidance literature:
In toluene; the iron complex in toluene is frozen in liquid nitrogen and the alkyneis condensed into the reaction tube (using Schlenk technique), the mixt. is stirred at room temp. for 6 to 40 h; the soln. is evaporated, the residue is dissolved in CH2Cl2 and chromd.on Florisil, elution with CH2Cl2/THF, chromy. on alumina gave a mixt. of two isomers, identified by spectroscopy;
DOI:10.1016/S0022-328X(00)99754-7
upstream raw materials:

propiolonitrile

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