ReN(TClP)

Base Information

Chemical Name:ReN(TClP)
CAS No.:128709-58-0
Molecular Formula:C₄₄H₂₄Cl₄N₅Re
Molecular Weight:950.727
Hs Code.:

Synonyms:

Suppliers and Price of ReN(TClP)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ReN(TClP)

Chemical Property:

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Technology Process of ReN(TClP)

There total 4 articles about ReN(TClP) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128709-73-9
ReO(TClP)Cl

: 7803-57-8,79785-97-0
hydrazine hydrate

: 128709-58-0
ReN(TClP)

Guidance literature:: In ethanol; chloroform; addn. of hydrazine hydrate to Re complex soln.; gently heating to reflux; monitoring progress of react. by UV; evapn.; pptn.; filtration; washing with water; drying; chromy. (alumina, CH2Cl2-methanol); evapn. of third fraction; recrystn. from CH2Cl2; elem. anal.;

Reference yield:

: 128709-63-7
Re(TClP)Cl₃

: 7803-57-8,79785-97-0
hydrazine hydrate

: 128709-58-0
ReN(TClP)

Guidance literature:: In ethanol; chloroform; addn. of hydrazine hydrate to Re complex soln.; stirring, room temp., 1h; heating to reflux, 30 min.; monitoring progress of react. by UV; evapn.; pptn.; filtration; washing with water; drying; chromy. (alumina, CH2Cl2-methanol); evapn. of third fraction; recrystn. from CH2Cl2; elem. anal.;

Reference yield:

: 37338-88-8
{ReO(OEP)}2O

: 7803-57-8,79785-97-0
hydrazine hydrate

: 128709-58-0
ReN(TClP)

Guidance literature:: In ethanol; chloroform; addn. of hydrazine hydrate to Re complex soln.; gently heating to reflux; monitoring progress of react. by UV; evapn.; pptn.; filtration; washing with water; drying; chromy. (alumina, CH2Cl2-methanol); evapn. of third fraction; recrystn. from CH2Cl2; elem. anal.;