1-Azacyclohexadecane

Base Information

Chemical Name:1-Azacyclohexadecane
CAS No.:295-66-9
Molecular Formula:C₁₅H₃₁N
Molecular Weight:225.418
Hs Code.:
Mol file:295-66-9.mol

Synonyms:Pentadecamethylenimine

Suppliers and Price of 1-Azacyclohexadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Azacyclohexadecane

Chemical Property:

PSA：12.03000
LogP:4.98970

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Azacyclohexadecane

There total 5 articles about 1-Azacyclohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 50768-64-4
15-aminopentadecanoic acid lactam

: 295-66-9
azacyclohexadecane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jo01308a002

Reference yield:

: 502-72-7
cyclopentadecanone

: 295-66-9
azacyclohexadecane

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂OH; sodium acetate / methanol / 1 h / 20 °C

2: pyridine; tosyl chloride / CH₂Cl₂ / 20 °C

3: LiAlH₄ / tetrahydrofuran / 16 h / 70 °C

With pyridine; lithium aluminium tetrahydride; hydroxylamine; sodium acetate; p-toluenesulfonyl chloride; In tetrahydrofuran; methanol; dichloromethane; 2: Beckman rearrangement;
DOI:10.1021/jo016101c

Reference yield:

: 34341-05-4
cyclopentadecanone oxime

: 295-66-9
azacyclohexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; tosyl chloride / CH₂Cl₂ / 20 °C

2: LiAlH₄ / tetrahydrofuran / 16 h / 70 °C

With pyridine; lithium aluminium tetrahydride; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; 1: Beckman rearrangement;
DOI:10.1021/jo016101c