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102-50-1

Basic Information
CAS No.: 102-50-1
Name: 2-Methyl-4-methoxybenzenamine
Article Data: 32
Molecular Structure:
Molecular Structure of 102-50-1 (2-Methyl-4-methoxybenzenamine)
Formula: C8H11NO
Molecular Weight: 137.181
Synonyms: p-Anisidine,2-methyl- (7CI,8CI);2-Amino-5-methoxytoluene;2-Methyl-4-(methyloxy)aniline;2-Methyl-4-anisidine;2-Methyl-4-methoxyaniline;2-Methyl-4-methoxybenzenamine;2-Methyl-p-anisidine;4-Methoxy-2-methylaniline;4-Methoxy-2-methylbenzenamine;4-Methoxy-o-toluidine;NSC 66563;[2-Methyl-4-(methyloxy)phenyl]amine;
EINECS: 203-036-7
Density: 1.065 g/cm3
Melting Point: 13-14 °C(lit.)
Boiling Point: 249.4 °C at 760 mmHg
Flash Point: 113.5 °C
Solubility: insoluble,
Appearance: brick red crystals or liquid
Hazard Symbols: IrritantXi,HarmfulXn,ToxicT
Risk Codes: 36/37/38-40-45
Safety: 26-36/37/39-53-45
PSA: 35.25000
LogP: 2.16700
Synthetic route
5367-32-8

5-methoxy-2-nitrotoluene

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With hydrogen; platinum(IV) oxide In isopropyl alcohol under 2327.2 Torr;98.5%
With sodium formate In ethanol at 85℃; for 1h;87%
With tetrahydroxydiboron; water at 80℃; for 8h;80%
208399-66-0

4-methoxy-2-methylphenyl boronic acid

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With sodium hydroxide; hydroxylamine-O-sulfonic acid In acetonitrile at 20℃; for 16h;89%
27060-75-9

4-bromo-3-methylanisole

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With ammonium sulfate; (R)-(-)-1-[(SP)-2-(dicyclohexylphosphino)ferrocenyl]ethyldi-tert-butylphosphine; bis(tri-ortho-tolylphosphine)palladium(0); sodium t-butanolate In 1,4-dioxane at 100℃; for 6h; Inert atmosphere; Glovebox;80%
With ammonium hydroxide; copper(l) iodide; potassium carbonate; 4R-4-hydroxyproline In dimethyl sulfoxide at 70℃; for 36h;77%
154876-10-5

1-(4-methoxy-2-methylphenyl)-1,2-hydrazinedicarboxylic acid bis(2,2,2-trichloroethyl) ester

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With acetic acid; zinc for 0.75h; Ambient temperature;76%
13334-71-9

1-chloro-4-methoxy-2-methylbenzene

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With ammonium hydroxide; potassium phosphate; copper(l) iodide; N1,N2-bis(2,4,6-trimethoxyphenyl)oxalamide In water; dimethyl sulfoxide at 120℃; for 48h; Inert atmosphere;64%
With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; ammonia; sodium t-butanolate In 1,4-dioxane at 65℃; for 24h; Inert atmosphere; chemoselective reaction;52%
31601-41-9

N-(4-methoxy-2-methylphenyl)acetamide

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With hydrogenchloride
67-56-1

methanol

611-22-3

N-(o-tolyl)hydroxylamine

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With sulfuric acid at 25℃; durch wochenlange Einw.;
100-17-4

para-methoxynitrobenzene

676-58-4

methylmagnesium chloride

A

5961-59-1

N-methyl-N-(4-methoxyphenyl)amine

B

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With lithium aluminium tetrahydride; palladium on activated charcoal 1) THF, 20 min, -30 deg C, 2) 20 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
4-methoxy-2-methyl-acetophenone oxime

4-methoxy-2-methyl-acetophenone oxime

102-50-1

2-methyl-4-methoxyaniline

Conditions
ConditionsYield
With hydrogenchloride
7647-01-0

hydrogenchloride

75112-71-9

1-(4-methoxy-2-methyl-phenyl)-ethanone oxime

102-50-1

2-methyl-4-methoxyaniline

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Chemistry

MF: C8H11NO
MW: 137.18
EINECS: 203-036-7
2-METHYL-p-ANISIDINE(102-50-1),Its melting point is about  13-14 °C(lit.);boiling point is  248-249 °C(lit.);density is 1.065 g/mL at 25 °C(lit.) .Following is the molecular structure of 2-METHYL-p-ANISIDINE(102-50-1):

Uses

2-METHYL-p-ANISIDINE(102-50-1) can be used as medicine and dye intermediates.

Toxicity Data With Reference

1.   

otr-rat:emb 51,500 ng/plate

   JJATDK    JAT, Journal of Applied Toxicology. 1 (1981),190.

RTECS  :BZ6730000

Consensus Reports

IARC Cancer Review: Group 3 IMEMDT    IARC Monographs on the Evaluation of Carcinogenic Risk of Chemicals to Man . 7 ,1987,p. 56.(World Health Organization, Internation Agency for Research on Cancer,Lyon, France.: ) (Single copies can be ordered from WHO Publications Centre U.S.A., 49 Sheridan Avenue, Albany, NY 12210) ; Animal Inadequate Evidence IMEMDT    IARC Monographs on the Evaluation of Carcinogenic Risk of Chemicals to Man . 27 ,1982,p. 91.(World Health Organization, Internation Agency for Research on Cancer,Lyon, France.: ) (Single copies can be ordered from WHO Publications Centre U.S.A., 49 Sheridan Avenue, Albany, NY 12210) . NCI Carcinogenesis Bioassay (gavage); Clear Evidence: rat NCITR*    National Cancer Institute Carcinogenesis Technical Report Series. (Bethesda, MD 20014) No. NCI-CG-TR-105 ,1978. ; (gavage); Inadequate Studies: mouse NCITR*    National Cancer Institute Carcinogenesis Technical Report Series. (Bethesda, MD 20014) No. NCI-CG-TR-105 ,1978. . Reported in EPA TSCA Inventory.

Safety Profile

Suspected carcinogen with experimental carcinogenic and tumorigenic data. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx.

Other safty informations about 2-METHYL-p-ANISIDINE(102-50-1):
Hazard Codes:  Xi,Xn,T (Irritant;Harmful;Toxic)
Risk Statements :
R36/37/38:Irritating to eyes, respiratory system and skin
R40:Limited evidence of a carcinogenic effect
R45 :May cause cancer
Safety Statements :
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection
S53:Avoid exposure - obtain special instruction before use 
S45 :In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
RIDADR : 2810
WGK Germany : 3