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Basic Information
CAS No.: 1024598-06-8
Name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Molecular Structure:
Molecular Structure of 1024598-06-8 (11,12-Dihydro-11-phenylindolo[2,3-a]carbazole)
Formula: C24H16N2
Molecular Weight: 332.404
Synonyms: 11,12-dihydro-11-phenyl-Indolo[2,3-a]carbazole; Indolo[2,3-a]carbazole, 11,12-dihydro-11-phenyl-;
Density: 1.26
Boiling Point: 598.8±32.0 °C(Predicted)
PSA: 20.72000
LogP: 6.41820
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Synthetic route
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1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h;83%
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene; toluene for 24h; Inert atmosphere; Reflux;75%
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 17h; Inert atmosphere;73%
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9-phenyl-9H-carbazol-1-amine

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(2-bromophenyl)boronic acid

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11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Stage #1: 9-phenyl-9H-carbazol-1-amine With hydrogen bromide; dihydrogen peroxide In water; acetonitrile at -20℃;
Stage #2: (2-bromophenyl)boronic acid With palladium diacetate; caesium carbonate; (RP,RP)-1,2-bis[(o-anisyl)(phenyl)phosphino]ethane In 1-methyl-pyrrolidin-2-one at 20℃; Inert atmosphere; Reflux;		78.4%
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2-(2-nitrophenyl)-9-phenyl-9H-carbazole

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 12h; Inert atmosphere;71.5%
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 24h; Inert atmosphere;55%
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iodobenzene

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11,12-dihydroindolo[2,3-a]carbazole

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 3h; Inert atmosphere; Reflux;65%
With 18-crown-6 ether; copper; potassium carbonate In 1,2-dichloro-benzene for 12h; Reflux; Inert atmosphere;64%
With 18-crown-6 ether; copper In 1,2-dichloro-benzene for 12h; Reflux; Inert atmosphere;64%
108-86-1

bromobenzene

13716-12-6

tri-tert-butyl phosphine

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11,12-dihydroindolo[2,3-a]carbazole

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0) In water; toluene55%
...Expand
591-50-4

iodobenzene

222-19-5

indolo[2,3-a]carbazole

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine In 1,4-dioxane for 24h; Inert atmosphere; Reflux;51%
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phenylhydrazine hydrochloride

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4.08 h / 20 - 65 °C / Inert atmosphere
1.2: 15 h / 100 °C
2.1: potassium carbonate; copper(l) iodide; quinoline / 72 h / 190 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere
1.2: 12 h / 100 °C
2.1: copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C
1.2: 100 °C
2.1: copper; potassium carbonate; 18-crown-6 ether / 1,2-dichloro-benzene / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere
1.2: 12 h / 100 °C
2.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: ethanol / 0.5 h
1.2: 10 h / 65 °C
2.1: copper; 18-crown-6 ether; potassium carbonate / 1,2-dichloro-benzene / 48 h / 180 °C
View Scheme
765-87-7

cyclohexane-1,2-dione

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4.08 h / 20 - 65 °C / Inert atmosphere
1.2: 15 h / 100 °C
2.1: potassium carbonate; copper(l) iodide; quinoline / 72 h / 190 °C / Inert atmosphere
View Scheme

phenyl hydrazine hydrochloride

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere
1.2: 12 h / 100 °C / Inert atmosphere
2.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere
View Scheme
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(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

1024598-06-8

11,12-dihydro-11-phenylindolo[2,3-a]carbazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; water; ethanol / 24 h / 120 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 12 h / 180 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere
2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere
View Scheme
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    1024598-06-8

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    1024598-06-8

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    Product name: 11-Phenyl-11,12-Dihydroindolo[2,3-a]Carbazole CAS No.：1024598-06-8 Molecule Formula：C24H16N2 Molecule Weight：332.40 Purity: 97.0% Package: 25kg/drum Description：White to off-white solid Manufacture Standards：Enterprise Standard

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  • 11,12-Dihydro-11-phenylindolo[2,3-a]carbazoleCAS NO.: 1024598-06-8

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    1024598-06-8

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    1024598-06-8

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  • Casno:

    1024598-06-8

    11,12-Dihydro-11-phenylindolo[2,3-a]carbazole

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    Product Name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Synonyms: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole;11-phenyl-11,12-dihydroindolo[2,3-a]carbazole;Indolo[2,3-a]carbazole, 11,12-dihydro-11-phenyl-;11-phenylindolo[2,3-a]carbazole;1

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  • Casno:

    1024598-06-8

    Indolo[2,3-a]carbazole

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    1024598-06-8

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  • Casno:

    1024598-06-8

    Indolo[2,3-a]carbazole

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    Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

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  • Casno:

    1024598-06-8

    11,12-Dihydro-11-phenylindolo[2,3-a]carbazole

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    zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed produc

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  • Casno:

    1024598-06-8

    Indolo[2,3-a]carbazole

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    1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

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  • 11-phenylindolo[2,3-a]carbazole

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    1024598-06-8

    11-phenylindolo[2,3-a]carbazole

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    ★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support ★.Shortest delivery time . Sales term: Has a strong chemical professional quality and strong sense

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    1024598-06-8

    11,12-Dihydro-11-phenylindolo[2,3-a]carbazole

    Min.Order: 1 Gram

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    Hangzhou KieRaychem Co.,Ltd.is located in Yuhang District of Hangzhou City and specialized in the chemical product customization, development, sales, import and export. Current business is focused on fine chemicals, pharmaceutical materials and inter

    Hangzhou KieRaychem Co.,Ltd.is located in Yuhang District of Hangzhou City and specialized in the chemical product customization, development, sales, import and export. Current bus

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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  • SAGECHEM/11-phenyl-11,12-dihydroindolo[2,3-a]carbazole/SAGECHEM/Manufacturer in China

  • Casno:

    1024598-06-8

    SAGECHEM/11-phenyl-11,12-dihydroindolo[2,3-a]carbazole/SAGECHEM/Manufacturer in China

    Min.Order: 0

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    SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86818502

    Address:Room C1301, New Youth Plaza, 8 Jia Shan Road, Hangzhou, China

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  • Casno:

    1024598-06-8

    11-phenyl-11,12-dihydroindolo[2,3-a]carbazole

    Min.Order: 1 Kilogram

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    GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

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    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:18958062155

    Address:1

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