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1029364-77-9

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Basic Information
CAS No.: 1029364-77-9
Name: 8-Fluoro-6-methoxy Moxifloxacin Dihydrochloride
Article Data: 2
Molecular Structure:
Molecular Structure of 1029364-77-9 (8-Fluoro-6-methoxy Moxifloxacin Dihydrochloride)
Formula: C21H24FN3O4
Molecular Weight: 401.438
Synonyms: UNII-8175L96X3L; 8-Fluoro-6-methoxy Moxifloxacin Dihydrochloride; 8-Fluoro-6-methoxymoxifloxacin; Moxifloxacin hydrochloride specified impurity D [EP]; Moxifloxacin Imp. D (EP/BP) as diHCl salt;
Density: 1.408
Melting Point: 100-104°C
Boiling Point: 633.9±55.0 °C(Predicted)
Safety: 24/25
PSA: 83.80000
LogP: 2.76430
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Synthetic route

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Conditions
ConditionsYield
Stage #1: C14H11F2NO4 With isobutylamine; copper dichloride In methanol; ethylene glycol at 50℃; for 4h; Inert atmosphere;
Stage #2: (1S,6S)-2,8-diazabicyclo[4.3.0]nonane In methanol; ethylene glycol for 5h; Reflux;		88.3%

C8H4ClF3O2

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1.1: tetrachloromethane; magnesium / ethanol; toluene / 55 - 60 °C
1.2: 2 h / 30 - 35 °C
2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; water / 10 h / 100 - 110 °C
3.1: 110 - 120 °C
4.1: dichloromethane / 0 - 40 °C
5.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 75 - 80 °C
6.1: zinc(II) chloride / 2 h / 110 - 115 °C
6.2: 85 - 115 °C
7.1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
8.1: sodium hydroxide / 80 - 85 °C
View Scheme

C25H29BFN3O8

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
With sodium hydroxide at 80 - 85℃;58 g

C15H15F3O6

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; water / 10 h / 100 - 110 °C
2.1: 110 - 120 °C
3.1: dichloromethane / 0 - 40 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 75 - 80 °C
5.1: zinc(II) chloride / 2 h / 110 - 115 °C
5.2: 85 - 115 °C
6.1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
7.1: sodium hydroxide / 80 - 85 °C
View Scheme

C12H11F3O4

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: 110 - 120 °C
2.1: dichloromethane / 0 - 40 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 75 - 80 °C
4.1: zinc(II) chloride / 2 h / 110 - 115 °C
4.2: 85 - 115 °C
5.1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
6.1: sodium hydroxide / 80 - 85 °C
View Scheme

C15H15F3O5

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: dichloromethane / 0 - 40 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 75 - 80 °C
3.1: zinc(II) chloride / 2 h / 110 - 115 °C
3.2: 85 - 115 °C
4.1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
5.1: sodium hydroxide / 80 - 85 °C
View Scheme

C16H16F3NO4

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 75 - 80 °C
2.1: zinc(II) chloride / 2 h / 110 - 115 °C
2.2: 85 - 115 °C
3.1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
4.1: sodium hydroxide / 80 - 85 °C
View Scheme

C14H11F2NO4

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: zinc(II) chloride / 2 h / 110 - 115 °C
1.2: 85 - 115 °C
2.1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
3.1: sodium hydroxide / 80 - 85 °C
View Scheme

C18H16BF2NO8

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
2: sodium hydroxide / 80 - 85 °C
View Scheme
38233-47-5

2,3,4-trifluoro-5-methoxybenzoic acid

1029364-77-9

1-cyclopropyl-6-fluoro-1,4-dihydro-8-methoxy-7-[(4aS,7aS)-octahydro-1H-pyrrolo[3,4-b]pyridin-6-yl]-4-oxo-3-quinolinecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 9 steps
1.1: N,N-dimethyl-formamide; thionyl chloride / 2.5 h / 90 - 95 °C
2.1: tetrachloromethane; magnesium / ethanol; toluene / 55 - 60 °C
2.2: 2 h / 30 - 35 °C
3.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; water / 10 h / 100 - 110 °C
4.1: 110 - 120 °C
5.1: dichloromethane / 0 - 40 °C
6.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 75 - 80 °C
7.1: zinc(II) chloride / 2 h / 110 - 115 °C
7.2: 85 - 115 °C
8.1: triethylamine / acetonitrile / 3 h / 20 - 95 °C
9.1: sodium hydroxide / 80 - 85 °C
View Scheme
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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0086-311-66600578

    Address:C-2103 Wonder Mall Business Square, 15 Yuhua West Rd., Shijiazhuang 050000, Hebei, China

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  • 8-Fluoro-6-methoxy moxifloxacin manufacturer

  • Casno:

    1029364-77-9

    8-Fluoro-6-methoxy moxifloxacin manufacturer

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutical Tran

    Shaanxi Mingqi Chemical Co., Ltd is committed to the development of import and export trade in the production, operation and plant extracts of pharmaceutical raw materials and inte

  • Shaanxi Mingqi Chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+8618092428356

    Address:Weiyang District

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  • leading factory 8-Fluoro-6-methoxy moxifloxacin

  • Casno:

    1029364-77-9

    leading factory 8-Fluoro-6-methoxy moxifloxacin

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    fast delivery, competitive price, good quality, world class quality Storage:Storage in place with condition of being dry and ventilated Package:according to customer's requirement Application:raw material for production Transportation:by express, by

    With headquarter located in shanghai, We start research and develop cesium salt in the year of 1998. From then on, we focus development on pharmaceutical intermediate, catalyst, re

  • Chemical Solution Industrial

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:18896851556

    Address:#501, Huanqing Building, Yushan town, kunshan, suzhou

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