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10361-92-9

Basic Information
CAS No.: 10361-92-9
Name: YTTRIUM CHLORIDE
Article Data: 75
Molecular Structure:
Molecular Structure of 10361-92-9 (YTTRIUM CHLORIDE)
Formula: Cl3Y
Molecular Weight: 195.265
Synonyms: Yttriumchloride;Yttrium chloride (Y2Cl6);Yttrium trichloride;Yttrium(III) chloride;
EINECS: 233-801-0
Density: 2.67 g/mL at 25 °C(lit.)
Melting Point: 721 °C(lit.)
Boiling Point: °Cat760mmHg
Flash Point: °C
Solubility: Soluble.
Appearance: powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: Poison by intraperitoneal route. When heated to decomposition it emits toxic fumes of Cl. See also YTTRIUM and RARE EARTHS.
PSA: 0.00000
LogP: 2.06850
Synthetic route

hexaaquadichloroyttrium(III) chloride

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
In neat (no solvent, solid phase) byproducts: H2O; Schlenk techniques; heating Y compd. under vacuum (1E-3 Torr);99%

yttrium(III) oxide

erbium(III) oxide

potassium chloride

7782-50-5

chlorine

A

10138-41-7

erbium(III) chloride

B

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
With pyrographite In gas byproducts: CO; by chlorination-chem. vapor transport react.; mixt. of Er2O3 and Y2O3 with carbon and KCl (1:1:6:1 at. ratio) placed in alumina reactor and chlorinated with dry Cl2 (20 cm**3/min) at 800 K for 2 h; gas replace by Ar:Cl2 at 800-1300 K; detn. of separation factor;A 31.74%
B 21.33%
7647-01-0

hydrogenchloride

yttrium(III) oxide

ammonium chloride

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
In hydrogenchloride Y2O3 dissolved in 10 ml HCl (6m); addn. of solid NH4Cl (n(NH4Cl):n(Y2O3) approx. 15), addn. of 10 ml concd. HCl, heating to near dryness, cooling, ground; transferred to a quartz tube with a side arm, evacuation to ca. 10 Pa, heated to 373 K for 15-18 h, then temp. rise to 673 K (sublimation of NH4Cl), then temp. rise to 1223 K (sublimation of YCl3); elem. anal.;

yttrium(III) oxide

ammonium chloride

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
Y2O3 is reacted with NH4Cl; purified by two distn. in tantalum crucibles under high vac.;
In hydrogenchloride react. of oxide and excess NH4Cl in concd. HCl at 100°C; sublimation at 360°C/0.1 mmHg;
In not given extd. with THF;
7647-01-0

hydrogenchloride

yttrium(III) chloride hexahydrate

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
In neat (no solvent) heating (70°C, vac.; 100-250°C, HCl atm.);

yttrium(III) chloride hydrate

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
With NH4Cl In neat (no solvent) heating of YCl3*99H2O in the presence of NH4Cl (Handbuch der preparativen anorganischen Chemie, Herausg. G. Brauer, Studgardt, 1975);

3NH4(1+)*YCl6(3-) = (NH4)3YCl6

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
In neat (no solvent, solid phase) thermolysis (vac., 400°C); sublimation (870°C, 1E-5 torr);
In neat (no solvent) Y compd. transferred to platinum crucible under dry conditions, evacuation temp. raised slowly to 350-400°C, complete decompn. after fewhs.;

yttrium(III) oxide

7782-50-5

chlorine

7429-90-5

aluminium

A

1333-84-2, 1344-28-1

aluminum oxide

B

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
In neat (no solvent) heating (200°C, vac.; 300°C, 2 d); separated by chemical transport;

yttrium

10025-73-7

chromium(III) chloride

A

7440-47-3

chromium

B

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
In melt exchange reaction (KCl/NaCl melt, 1073 K);
In melt exchange reaction (KCl-NaCl melt, 1073 K);

yttrium(III) oxide

7719-09-7

thionyl chloride

10361-92-9

yttrium(III) chloride

Conditions
ConditionsYield
at 300°C, 1-2 d, sealed tube;
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Chemistry

IUPAC Name: Trichloroyttrium
The MF of Yttrium(III) chloride (CAS NO.10361-92-9) is Cl3Y.

                              
The MW of Yttrium(III) chloride (CAS NO.10361-92-9) is 195.26.
Synonyms of Yttrium(III) chloride (CAS NO.10361-92-9): Yttrium chloride ; Yttrium chloride (YCl3) ; Yttrium chloride solution ; Yttrium trichloride
Product Categories: Inorganics;Catalysis and Inorganic Chemistry;Chemical Synthesis;Crystal Grade Inorganics;Metal and Ceramic Science;Salts;Yttrium Salts
Density: 2.67 g/mL at 25 °C
Melting Point: 721 °C
Storage temp: 2-8 °C
Sensitive: Hygroscopic
EINECS: 1036-192-9 
Merck: 14,10107
Form: powder

Uses

  Yttrium(III) chloride (CAS NO.10361-92-9) is used as analytical reagent.It is also used as a catalyst and in superconductors and has been linked to pulmonary edema and liver damage.

Production

 Yttrium(III) chloride can be formed by reacting yttrium(III) oxide with hydrochloric acid, among other methods.

Toxicity Data With Reference

1.    

ipr-rat LD50:45 mg/kg

    AMIHAB    AMA Archives of Industrial Health. 16 (1957),475.
2.    

ipr-mus LD50:88 mg/kg

    AMIHAB    AMA Archives of Industrial Health. 16 (1957),475.
3.    

ipr-gpg LD50:85 mg/kg

    AEHLAU    Archives of Environmental Health. 5 (1962),437.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intraperitoneal route. When heated to decomposition it emits toxic fumes of Cl. See also YTTRIUM and RARE EARTHS.Safety information of Yttrium(III) chloride (CAS NO.10361-92-9):
Hazard Codes  IrritantXi
Risk Statements 
36/37/38 Irritating to eyes, respiratory system and skin
Safety Statements 
26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
37/39 Wear suitable gloves and eye/face protection
WGK Germany  3
RTECS  ZG3150000

Standards and Recommendations

ACGIH TLV: TWA 1 mg(Y)/m3

Specification

 Yttrium(III) chloride is an ionic compound of yttrium and chlorine. It is a salt that is solid at room temperature, highly soluble in water, and deliquescent. YCl3 in the solid state has a crystal structure with cubic close packed chloride ions and yttrium ions filling one third of the octahedral holes and the resulting YCl6 octahedra sharing three edges with adjacent octahedra give a layer structure. This structure is shared by a range of compounds notably AlCl3