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Basic Information
| CAS No.: | 104-68-7 |
|---|---|
| Name: | 2-(2-phenoxyethoxy)ethanol |
| Article Data: | 14 |
| Molecular Structure: | |
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| Formula: | C10H14 O3 |
| Molecular Weight: | 182.219 |
| Synonyms: | 2-(2-Phenoxyethoxy)ethanol;Diethylene glycol monophenyl ether; Diethylene glycol phenyl ether; NSC 406593;Phenoxydiglycol; Phenyl Di Glycol; Phenyl carbitol; Sunfine PH 20 |
| Density: | 1.092g/cm3 |
| Melting Point: | -49.9°C |
| Boiling Point: | 309.3°Cat760mmHg |
| Flash Point: | 140.9°C |
| Solubility: | 35g/L at 20℃ |
| Safety: | Moderately toxic by ingestion and skin contact. A skin and severe eye irritant. Some glycol ethers have dangerous human reproductive effects. When heated to decomposition it emits acrid smoke and irritating fumes. See also GLYCOL ETHERS. |
| PSA: | 38.69000 |
| LogP: | 1.07430 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: phenol With potassium hydroxide In acetonitrile at 60℃; for 2h; Inert atmosphere; Stage #2: 2-(2-bromoethoxy)ethan-1-ol With potassium iodide In acetonitrile at 60℃; for 10h; Inert atmosphere; | 72% |
- 108-86-1
bromobenzene
- 62-53-3
aniline
- 111-46-6
diethylene glycol
A
- 104-68-7
2-(2-phenoxyethoxy)ethanol
B
- 122-39-4
diphenylamine
Conditions
| Conditions | Yield |
|---|---|
| With copper(II) acetate monohydrate; potassium carbonate at 110℃; for 8h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; | A 28% B 70% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| at 95℃; for 2h; | 69% |
- 108-86-1
bromobenzene
- 100-01-6
4-nitro-aniline
- 111-46-6
diethylene glycol
A
- 836-30-6
4-ntrophenyl(phenyl)amine
B
- 104-68-7
2-(2-phenoxyethoxy)ethanol
Conditions
| Conditions | Yield |
|---|---|
| With copper(II) acetate monohydrate; potassium carbonate at 110℃; for 20h; Inert atmosphere; | A 68% B 22% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With N-Methyldicyclohexylamine; C46H67BN2; nickel dibromide In N,N-dimethyl-formamide at 60℃; for 24h; | 65% |
- 108-86-1
bromobenzene
- 95-53-4
o-toluidine
- 111-46-6
diethylene glycol
A
- 104-68-7
2-(2-phenoxyethoxy)ethanol
B
- 1205-39-6
N-phenyl-2-methylaniline
Conditions
| Conditions | Yield |
|---|---|
| With copper(II) acetate monohydrate; potassium carbonate at 110℃; for 12h; Inert atmosphere; | A 33% B 63% |
...Expand
- 108-86-1
bromobenzene
- 24544-04-5
2,6-diisopropylbenzenamine
- 111-46-6
diethylene glycol
A
- 104-68-7
2-(2-phenoxyethoxy)ethanol
Conditions
| Conditions | Yield |
|---|---|
| With copper(II) acetate monohydrate; potassium carbonate at 110℃; for 20h; Inert atmosphere; | A 30% B 11% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With sodium phenoxide at 200℃; |
Conditions
| Conditions | Yield |
|---|---|
| at 100℃; Einleiten von Aethylenoxyd; |
- 31603-33-5
bis(phenoxyethoxyethyl) peroxydicarbonate
A
- 124-38-9
carbon dioxide
B
- 622-87-7
β,β'-Bis(phenoxyethyl)ether
C
- 104-68-7
2-(2-phenoxyethoxy)ethanol
D
- 141-46-8
Glycolaldehyde
Conditions
| Conditions | Yield |
|---|---|
| In benzene at 60℃; Rate constant; Kinetics; var. temp., also with inhibiting addition of styrene or α-naphthol, Eact; |
...Expand
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2-(2-phenoxyethoxy)ethanol
Chemistry
MF: C10H14O3
MW: 182.21636
EINECS: 203-227-5
MW: 182.21636
EINECS: 203-227-5
Toxicity Data With Reference
| 1. | skn-rbt 505 mg open MLD | UCDS** Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide Corp., 270 Park Ave., New York, NY 10017) 8/16 ,1961. | ||
| 2. | eye-rbt 2 mg open SEV | AMIHBC AMA Archives of Industrial Hygiene and Occupational Medicine. 10 (1954),61. | ||
| 3. | orl-rat LD50:2140 mg/kg | AMIHBC AMA Archives of Industrial Hygiene and Occupational Medicine. 10 (1954),61. | ||
| 4. | skn-rbt LD50:2120 mg/kg | UCDS** Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide Corp., 270 Park Ave., New York, NY 10017) 8/16 ,1961. |
RTECS: KM0875000
Consensus Reports
Glycol ether compounds are on the Community Right-To-Know List. Reported in EPA TSCA Inventory.
Safety Profile
Moderately toxic by ingestion and skin contact. A skin and severe eye irritant. Some glycol ethers have dangerous human reproductive effects. When heated to decomposition it emits acrid smoke and irritating fumes. See also GLYCOL ETHERS.