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104-78-9

Basic Information
CAS No.: 104-78-9
Name: 3-Diethylaminopropylamine
Article Data: 49
Molecular Structure:
Molecular Structure of 104-78-9 (3-Diethylaminopropylamine)
Formula: C7H18N2
Molecular Weight: 130.233
Synonyms: 1,3-Propanediamine,N,N-diethyl- (6CI,7CI,8CI,9CI);(3-Diethylaminopropan-1-yl)amine;1-Amino-3-(diethylamino)propane;3-(Diethylamino)-n-propylamine;3-(Diethylamino)propanamine;3-(Diethylamino)propylamine;3-(N,N-Diethylamino)-1-propylamine;3-(N,N-Diethylamino)propylamine;3-Diethylamino-1-propylamine;Diethylaminotrimethylenamine;N,N-Diethyl-1,3-diaminopropane;N,N-Diethyl-1,3-propanediamine;N,N-Diethyl-1,3-propylenediamine;N,N-Diethyltrimethylenediamine;N,N-Ethylpropane-1,3-diamine;N-(3-Aminopropyl)-N,N-diethylamine;N-(3-Aminopropyl)diethylamine;N-(3-Diethylaminopropyl)amine;N-(Diethylaminopropyl)amine;N-Aminopropyl-N,N-diethylamine;N1,N1-Diethylpropane-1,3-diamine;NSC 7776;g-(Diethylamino)propylamine;
EINECS: 203-236-4
Density: 0.84 g/cm3
Melting Point: -60 °C
Boiling Point: 170.7 °C at 760 mmHg
Flash Point: 58.9 °C
Solubility: miscible with water
Appearance: clear colorless to slightly yellowish liquid
Hazard Symbols: IrritantXi, CorrosiveC
Risk Codes: 10-21/22-34-43
Safety: 26-36/37/39-45
Transport Information: UN 2684 3/PG 3
PSA: 29.26000
LogP: 1.37730
Synthetic route
20824-58-2

2-(3-diethylaminopropyl)-1H-isoindole-1,3(2H)-dione

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With hydrazine hydrate In ethanol for 24h; Reflux;73%
With hydrazine hydrate In ethanol for 3h; Reflux;14%
With hydrazine
5351-04-2

3-diethylaminopropionitrile

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With ethanol; sodium for 3h; Reflux;56%
With sodium-potassium alloy; butan-1-ol
With ethanol; sodium
136918-14-4

phthalimide

104-77-8

3-diethylaminopropyl chloride

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With xylene Hydrolyse des entstandenen N-<3-Diaethylamino-propyl>-phthalimids mit konz.HCl bei Siedetemperatur.;
With xylene Hydrolyse des entstandenen N-<3-Diaethylamino-propyl>-phthalimids mit konz.HCl bei Siedetemperatur.;
5460-29-7

2-(3-bromopropyl)isoindole-1,3-dione

109-89-7

diethylamine

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
Hydrolyse des entstandenen N-<3-Diaethylamino-propyl>-phthalimids mit konz.HCl bei Siedetemperatur.;
(i) KOH, MeOH, (ii) aq. KOH, (heating); Multistep reaction;
Hydrolyse des entstandenen N-<3-Diaethylamino-propyl>-phthalimids mit konz.HCl bei Siedetemperatur.;
5351-04-2

3-diethylaminopropionitrile

A

6050-28-8

bis-(3-diethylamino-propyl)-amine

B

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With sodium-potassium alloy; butan-1-ol
With nickel at 100℃; under 62518.2 Torr; Hydrogenation;
100536-45-6

tetra-N-ethyl-ξ-propenediyldiamine

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With ammonia; nickel at 100℃; under 91938.4 Torr; Hydrogenation;
With ammonia; nickel at 100℃; under 91938.4 Torr; Hydrogenation;
109-89-7

diethylamine

156-87-6

propan-1-ol-3-amine

A

107-11-9

1-amino-2-propene

B

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With thorium dioxide at 270 - 290℃;
503-29-7

azetidine

109-89-7

diethylamine

A

103502-67-6

1-<(3-aminopropyl)aminopropyl>diethylamine

B

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With perchloric acid at 25℃; Rate constant; Thermodynamic data; E(a), ΔS(excit.);
N,N-diethyl-β-alynyne-nitrile

N,N-diethyl-β-alynyne-nitrile

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride; diethyl ether
5351-04-2

3-diethylaminopropionitrile

Raney nickel

Raney nickel

A

6050-28-8

bis-(3-diethylamino-propyl)-amine

B

104-78-9

diethylaminopropylamine

Conditions
ConditionsYield
Hydrogenation;
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Chemistry

Product Name:3-Diethylaminopropylamine
The MF of 3-Diethylaminopropylamine(104-78-9) is C7H18N2.

                        
The MW of 3-Diethylaminopropylamine(104-78-9) is 130.23.
Synonyms:1-(Diethylamino)propylamine-3;1,3-Propanediamine,N,N-diethyl-;3-(N,N-Diethylamino)-1-propylamine;N-(3-Diethylaminopropyl)amine;3-Propanediamine,N,N-diethyl-1;Diethylaminotrimethylenamine;N,N-(Diethylamino)propylamine
EINECS: 203-236-4 
Mol File: 104-78-9.mol
Surface Tension: 30.8 dyne/cm 
Density: 0.84 g/ml
Flash Point: 58.9 °C 
Enthalpy of Vaporization: 40.71 kJ/mol 
Boiling Point: 170.7 °C at 760 mmHg 
Vapour Pressure: 1.45 mmHg at 25°C 
Water Solubility: MISCIBLE
Sensitive: Air Sensitive
BRN: 741879
CAS DataBase Reference: 104-78-9(CAS DataBase Reference)
NIST Chemistry Reference: 104-78-9(NIST)
EPA Substance Registry System: 104-78-9(EPA Substance)

Uses

The 3-Diethylaminopropylamine(104-78-9) is used as a solvent, extraction agents and organic synthesis intermediates, dyes, pigments, surface active agent.

Toxicity Data With Reference

1.   

skn-rbt 100 µg/24H open

   AIHAAP    American Industrial Hygiene Association Journal. 23 (1962),95.
2.   

orl-rat LD50:1410 mg/kg

   UCDS**    Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide Corp., 270 Park Ave., New York, NY 10017) 2/27 ,1967.
3.   

skn-rbt LD50:750 mg/kg

   AIHAAP    American Industrial Hygiene Association Journal. 23 (1962),95.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by ingestion and skin contact. Corrosive to the eyes, skin, and mucous membranes. A sensitizer. See also AMINES. Flammable liquid when exposed to heat or flame; can react with oxidizing materials. To fight fire, use foam, CO2, dry chemical. When heated to decomposition it emits toxic fumes of NOx.
Safety information of 3-Diethylaminopropylamine(104-78-9):
Hazard Codes: C,Xi
Risk Statements: 10-21/22-34-43
R10:Flammable ;
R21/22:Harmful in contact with skin and if swallowed ;
R34:Causes burns ;
R43:May cause sensitization by skin contact ;
Safety Statements: 26-36/37/39-45
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice ;
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection ;
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) ;
RIDADR: UN 2684 3/PG 3
WGK Germany: 1
RTECS: TX7350000
HazardClass: 3
PackingGroup: III
HS Code: 29212900

Standards and Recommendations

DOT Classification:  8; Label: Corrosive, Flammable Liquid

Specification

The 3-Diethylaminopropylamine(104-78-9) is stable but imcompatible with strong oxidizing agents, acids, acid chlorides, carbon dioxide, nitrites, acid anhydrides, nitric oxide.Hazardous decomposition products are nitrogen oxides, carbon monoxide, carbon dioxide, nitrosamines.