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10544-72-6

Basic Information
CAS No.: 10544-72-6
Name: Nitrogen oxide (N2O4)
Molecular Structure:
Molecular Structure of 10544-72-6 (Nitrogen oxide (N2O4))
Formula: N2O4
Molecular Weight: 92.02
Synonyms: Dinitrogentetraoxide; Dinitrogen tetroxide; Nitrogen tetraoxide; Nitrogen tetroxide
EINECS: 234-126-4
Density: 2.62 g/mL at 25 °C(lit.)
Melting Point: ?11 °C(lit.)
Boiling Point: 21 °C(lit.)
Flash Point: °C
Solubility: reacts with water
Appearance: Transparent gas
Hazard Symbols: VeryT+
Risk Codes: 26-34
Safety: A poison. Moderately toxic by inhalation. When heated to decomposition it emits toxic fumes of NOx. See also NITROGEN MONOXIDE, mixed with NITROGEN TETROXIDE.
Transport Information: UN 1067 2
PSA: 91.64000
LogP: 0.50120
Synthetic route
626-35-7

nitroacetic acid ethyl ester

64-17-5

ethanol

sodium nitrite

sodium nitrite

A

10544-72-6

dinitrogen tetraoxide

B

15719-64-9, 15719-76-3, 97762-63-5

methylammonium carbonate

C

nitrogen

nitrogen

110-46-3

isopentyl nitrite

A

10544-72-6

dinitrogen tetraoxide

B

15719-64-9, 15719-76-3, 97762-63-5

methylammonium carbonate

C

590-86-3

isovaleraldehyde

D

nitrogen

nitrogen

Conditions
ConditionsYield
at 50 - 80℃; Kinetics; Pyrolysis;
7664-93-9

sulfuric acid

10544-72-6

dinitrogen tetraoxide

Conditions
ConditionsYield
at 85℃; Rate constant;
114959-87-4

(+/-)-erythro-2,3-dibromo-butyrohydroxamic acid

ammonium hydroxide

A

625-37-6

crotonamide

B

10544-72-6

dinitrogen tetraoxide

7647-01-0

hydrogenchloride

ethylnitrolic acid

A

10544-72-6

dinitrogen tetraoxide

B

64-19-7

acetic acid

Conditions
ConditionsYield
at 20 - 40℃; Rate constant;

ethylnitrolic acid

7664-93-9

sulfuric acid

A

10544-72-6

dinitrogen tetraoxide

B

64-19-7

acetic acid

Conditions
ConditionsYield
at 39.5℃; Rate constant;
4312-87-2

formohydroxamic acid

7664-93-9

sulfuric acid

sodium nitrite

sodium nitrite

A

64-18-6

formic acid

B

10544-72-6

dinitrogen tetraoxide

C

15719-64-9, 15719-76-3, 97762-63-5

methylammonium carbonate

D

nitrogen

nitrogen

60-29-7

diethyl ether

5156-40-1

cyclohexyl nitrite

lithium alanate

lithium alanate

A

7664-41-7

ammonia

B

10544-72-6

dinitrogen tetraoxide

C

108-93-0

cyclohexanol

D

hydrogen

hydrogen

Conditions
ConditionsYield
anschliessend Behandeln mit Wasser;
60-29-7

diethyl ether

2108-66-9

cyclohexyl nitrate

lithium alanate

lithium alanate

A

7664-41-7

ammonia

B

10544-72-6

dinitrogen tetraoxide

C

108-93-0

cyclohexanol

D

hydrogen

hydrogen

Conditions
ConditionsYield
anschliessend Behandeln mit Wasser;
623-11-0

1-methyl-4-nitrosobenzene

495-18-1

Benzohydroxamic acid

potassium permanganate

potassium permanganate

A

10544-72-6

dinitrogen tetraoxide

B

nitrogen

nitrogen

16824-89-8, 12533-50-5

N-oxo-N-nitrosoamine

10102-43-9

nitrogen(II) oxide

A

10544-72-6

dinitrogen tetraoxide

B

122413-35-8

nitrous anhydride

Conditions
ConditionsYield
In further solvent(s) repeated distn. of NO/cis-ONNO soln. in liq. argon at temps. below -150°C; IR spectroscopy;
10102-44-0

Nitrogen dioxide

A

15969-55-8

dinitrogen tetroxide

B

10544-73-7

dinitrogen trioxide

C

10544-72-6

dinitrogen tetraoxide

D

10102-03-1

dinitrogen pentoxide

Conditions
ConditionsYield
In gaseous matrix gas-phase react. of NO2/ Ar deposited on a cold CsI window with O3/ Ar (deposition rates of O3: 0.09 to less than 0.27 mmol/ h); not isolated, detected by IR spectroscopy;;

silver nitrate

2696-92-6

nitrosylchloride

A

10544-72-6

dinitrogen tetraoxide

B

silver(I) chloride

Conditions
ConditionsYield
In neat (no solvent) vigorous react. at 25°C; heating on a water bath for 2 days;;A >99
B >99

silver nitrate

2696-92-6

nitrosylchloride

10544-72-6

dinitrogen tetraoxide

Conditions
ConditionsYield
In neat (no solvent) byproducts: AgCl; at ambient temp.;;
In further solvent(s) byproducts: AgCl; further solvent: N2O4;;>99
In not given
In further solvent(s) byproducts: AgCl; further solvent: N2O4;;>99
In neat (no solvent) byproducts: AgCl; at ambient temp.;;
14545-72-3

chlorine nitrate

2696-92-6

nitrosylchloride

A

7782-50-5

chlorine

B

10544-72-6

dinitrogen tetraoxide

Conditions
ConditionsYield
In neat (no solvent) at -78°C;;
In neat (no solvent) at -78°C;;
In neat (no solvent) at -78°C;;
In neat (no solvent) at -78°C;;

lead(II) nitrate

2696-92-6

nitrosylchloride

A

10544-72-6

dinitrogen tetraoxide

B

lead(II) chloride

Conditions
ConditionsYield
In neat (no solvent) excess of NOCl;;
In neat (no solvent) excess of NOCl;;
7446-09-5

sulfur dioxide

10102-03-1

dinitrogen pentoxide

A

7446-11-9

sulfur trioxide

B

10544-72-6

dinitrogen tetraoxide

Conditions
ConditionsYield
With oxygen; ozone 30°C, several h,;
7727-37-9

nitrogen

A

15969-55-8

dinitrogen tetroxide

B

13354-65-9

nitric oxide dimer

C

10102-43-9

nitrogen(II) oxide

D

10544-72-6

dinitrogen tetraoxide

E

10102-44-0

Nitrogen dioxide

Conditions
ConditionsYield
In gaseous matrix byproducts: N2O3; at liquid N2 temp., 1atm of O2, in Ar;; IR;
7697-37-2

nitric acid

arsenic(III) trioxide

A

10544-73-7

dinitrogen trioxide

B

10102-43-9

nitrogen(II) oxide

C

10544-72-6

dinitrogen tetraoxide

Conditions
ConditionsYield
various prods. for various concn. of HNO3;
various prods. for various concn. of HNO3;

nitrosylsulfuric acid

7697-37-2

nitric acid

A

7664-93-9

sulfuric acid

B

10544-72-6

dinitrogen tetraoxide

Conditions
ConditionsYield
In not given
In water
In nitric acid equilibrium in concd. HNO3; dependence of content of water discussed;;
7631-99-4

sodium nitrate

7697-37-2

nitric acid

10544-72-6

dinitrogen tetraoxide

Conditions
ConditionsYield
In not given byproducts: H2O; in concd. soln.;
In not given byproducts: H2O; in concd. soln.;
10025-71-5

tellurium dichloride

10544-72-6

dinitrogen tetraoxide

7446-07-3

tellurium(IV) oxide

Conditions
ConditionsYield
In neat (no solvent) byproducts: NOCl; reaction of TeCl2 with liquid N2O4;;100%
10544-72-6

dinitrogen tetraoxide

tetrabutylammonium nitrite

tetrabutylammonium nitrate

Conditions
ConditionsYield
In neat (no solvent) stirring (vacuum, 20°C, 30 min), nitrogen oxides evapn. (-10°C, vacuum); recrystn. (ethyl acetate); elem. anal.;100%
7705-08-0

iron(III) chloride

10544-72-6

dinitrogen tetraoxide

10102-44-0

Nitrogen dioxide

Fe(3+)*3NO3(1-)*1.5N2O4=Fe(NO3)3*1.5N2O4

Conditions
ConditionsYield
In ethyl acetate bubbling NO2/N2O4 mixt. (generated by thermal decompn. of Pb(NO3)2) though FeCl3 soln. (-10°C, stirring; 1 h); evapn. (vac.);100%
10544-72-6

dinitrogen tetraoxide

lead dioxide

lead(II) nitrate

Conditions
ConditionsYield
In neat (no solvent)97%
In neat (no solvent)97%
10102-43-9

nitrogen(II) oxide

10544-72-6

dinitrogen tetraoxide

10544-73-7

dinitrogen trioxide

Conditions
ConditionsYield
In toluene -20°C,for 2h;94.4%
In toluene -20°C,for 2h;94.4%
-20°C, absorption of NO;
1120-36-1

1-tetradecene

10544-72-6

dinitrogen tetraoxide

638-53-9

tridecanoic acid

Conditions
ConditionsYield
In N-methyl-acetamide; water; benzene92%

[Au2(μ-(CH2)2PPh2)2]

10544-72-6

dinitrogen tetraoxide

113008-27-8

{gold(II)((CH2)2PPh2)NO2}2

Conditions
ConditionsYield
In toluene bubbling of N2O4 through the Au compd. in toluene; mp.;90%
146164-93-4

[5,10,15,20-tetrakis(3',5'-di-tert-butylphenyl)porphyrinato]copper(II)

10544-72-6

dinitrogen tetraoxide

copper(II) 2-nitro-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)porphyrin dihydrate

Conditions
ConditionsYield
In dichloromethane Cu complex reacted with N2O4 in CH2Cl2; elem. anal.;89%
13517-35-6

tris(triphenylphosphine)platinum(0)

10544-72-6

dinitrogen tetraoxide

cis-[Pt(PPh3)2(NO3)2] * 0.50 CH2Cl2

Conditions
ConditionsYield
In neat (no solvent) byproducts: Ph3PO; treatment of Pt-complex with N2O4 (1 atm, 25°C, 15 h); drying (vac.), recrystn. (CH2Cl2/MeOH); elem. anal.;88%

lead(II,IV) oxide

10544-72-6

dinitrogen tetraoxide

lead(II) nitrate

Conditions
ConditionsYield
9h;;86%
9h;;86%
71356-91-7

Rh2(η5-pentamethylcyclopentadienyl)2(N3)4

10544-72-6

dinitrogen tetraoxide

[Rh(pentamethylcyclopentadienyl)(NO3)2]

Conditions
ConditionsYield
In further solvent(s) N2-atmosphere; stirring of suspn. of Rh-complex in N2O4 (0°C, 2 h); solvent removal (vac.), washing (Et2O), crystn. (CH2Cl2/(i-Pr)2O); elem.anal.;86%

lead(II) oxide

10544-72-6

dinitrogen tetraoxide

lead(II) nitrate

Conditions
ConditionsYield
7h at 87°C;;84%
7h at 87°C;;84%
10544-72-6

dinitrogen tetraoxide

Ir(3+)*2P(C6H5)3*CO*H(1-)*NO2(1-)*NO3(1-)=Ir(P(C6H5)3)2(CO)H(NO2)(NO3)

Conditions
ConditionsYield
In benzene byproducts: NO; absence of air and moisture; condensation of N2O4 onto frozen soln. of Ir-complex, warming to 6°C; solvent removal (vac.), washing (ether), recrystn. (CH2Cl2/ether); elem.anal.;82%
In neat (no solvent)
7787-71-5

bromine trifluoride

phosphorous

7726-95-6

bromine

10544-72-6

dinitrogen tetraoxide

19200-21-6

nitronium hexafluorophosphate

Conditions
ConditionsYield
In not given treating red P with Br2; addn. of N2O4 and BrF3;;80%
In not given treating red P with Br2; addn. of N2O4 and BrF3;;80%

((CH3)3PbCCNO2)(CHCNO2)3

10544-72-6

dinitrogen tetraoxide

lead(II) nitrate

Conditions
ConditionsYield
In dichloromethane byproducts: nitrosotetranitrocubane; -15°C;75%
15390-38-2, 15131-25-6

bis(1,2-bis(diphenylphosphino)ethane)iridium(I) chloride

10544-72-6

dinitrogen tetraoxide

Ir(3+)*2(C6H5)2PCH2CH2P(C6H5)2*2NO2(1-)*Cl(1-)*2CH2Cl2=[Ir((C6H5)2PCH2CH2P(C6H5)2)2(NO2)2]Cl*2CH2Cl2

Conditions
ConditionsYield
In chloroform absence of air and moisture; condensation of excess N2O4 onto frozen soln. of Ir-complex, warming to 0°C, standing (0°C, 10 min); solvent removal (vac.), crystn. (CH2Cl2/MeOH); elem. anal.;72%

Cu(C19H23N3O3)

10544-72-6

dinitrogen tetraoxide

Cu(C19H22N4O5)

Conditions
ConditionsYield
In chloroform room temperature, 4-6 h; pptn. with ether, filtration, washing with ether, recrystn. (chloroform); elem. anal.;70%
116-14-3

polytetrafluoroethylene

10544-72-6

dinitrogen tetraoxide

426-03-9

difluoronitroacetic acid

Conditions
ConditionsYield
With H2O shaking;65%

tetrafluoroboric acid

10544-72-6

dinitrogen tetraoxide

nitrosonium tetrafluoroborate

Conditions
ConditionsYield
In water addn. of N2O4 to 75-80% aq. HBF4 (molar ratio 2.5:1, ice-cooling, stirring), stirring at 0-10°C for 30min, filtration of (NO)(BF4) (under CO2), washing with cold glacial acetic acid and CCl4, drying in vac.;;62%
In water addn. of N2O4 to 75-80% aq. HBF4 (molar ratio 2.5:1, ice-cooling, stirring), stirring at 0-10°C for 30min, filtration of (NO)(BF4) (under CO2), washing with cold glacial acetic acid and CCl4, drying in vac.;;62%
In water
116-14-3

polytetrafluoroethylene

10544-72-6

dinitrogen tetraoxide

356-16-1

1,1,2,2-tetrafluoro-1,2-dinitro-ethane

Conditions
ConditionsYield
in glas tube 8 h at 60°C;53%
in glas tube 8 h at 60°C;53%
in glas tube 24 h at 20°C;7.5%
674-90-8

tris(trifluoromethylsulfanyl)phosphine

10544-72-6

dinitrogen tetraoxide

57368-29-3

tris(trifluoromethylsulfanyl)phosphine oxide

Conditions
ConditionsYield
sublimation;50%
sublimation;50%

(CO)2Fe(P(C6H5)3)2NO(1+)*Cl(1-)=((CO)2Fe(P(C6H5)3)2NO)Cl

10544-72-6

dinitrogen tetraoxide

(CO)2Fe(P(C6H5)3)2NO(1+)*NO3(1-)=((CO)2Fe(P(C6H5)3)2NO)NO3

Conditions
ConditionsYield
In benzene 0°C, 30 min, 10% soln. of N2O4 in dry benzene; recrystn. from methanol/ethanol;45%
In benzene 0°C, 30 min, 10% soln. of N2O4 in dry benzene; recrystn. from methanol/ethanol;45%
Conditions
ConditionsYield
In ethyl acetate bubbling NO2/N2O4 mixt. (generated by thermal decompn. of Pb(NO3)2) though suspn. of Cu powder (-10°C, stirring; 2 h), stirring for 10 h; filtration, evapn. (vac.);44%
53687-46-0

closo-3,3-(PPh3)2-3-H-3,1,2-RhC2B9H11

10544-72-6

dinitrogen tetraoxide

82807-97-4

[closo-3-triphenylphosphine-3,3-nitrato-3,1,2-RhC2B9H11]

Conditions
ConditionsYield
With NO2 In benzene under Ar, gentle stream of NO2/N2O4 mixt. bubbled through stirred suspn. of Rh complex in benzene at room temp. for 15 min, stirred for further5 min; evapd. to dryness in vac., chromd., treated with hexane, evapd., added hexane, allowed stand overnight, filtered;34%
15318-32-8, 30669-24-0

trans-carbonylchlorobis(diphenylmethylphosphine)iridium(I)

10544-72-6

dinitrogen tetraoxide

Ir(3+)*2P(C6H5)2CH3*CO*Cl(1-)*NO2(1-)*NO3(1-)=Ir(P(C6H5)2CH3)2(CO)Cl(NO2)(NO3)

Conditions
ConditionsYield
In toluene absence of air and moisture; condensation of N2O4 onto frozen soln. of Ir-complex, warming to 0°C, standing (15 min); washing (ether), recrystn. (CH2Cl2/MeOH); elem. anal.;30%
10544-72-6

dinitrogen tetraoxide

7719-12-2, 52843-90-0

phosphorus trichloride

A

10544-73-7

dinitrogen trioxide

B

P4O4Cl10

C

13498-14-1

pyrophosphoryl chloride

D

10102-43-9

nitrogen(II) oxide

Conditions
ConditionsYield
In neat (no solvent) byproducts: NOCl, NO2Cl; Irradiation (UV/VIS); passing dry N2O4 over the surface of freshly distd. PCl3 cooled at -40 °C and under irradiation with UV light; absortion under formation of a dark red liq.; expelling NO, N2O3, NOCl, NO2Cl;; isolation of liquid products by fractionation; liquid phase containing POCl3, P2O3Cl4 and P4O4Cl10; yield of P2O3Cl4 25 %, P4O4Cl10 3 %;;A n/a
B 3%
C 25%
D n/a
E n/a
In neat (no solvent) byproducts: NOCl, NO2Cl; passing dry N2O4 over the surface of freshly distd. PCl3 cooled at -40 °C; absortion under formation of a dark red liq.; expelling NO, N2O3, NOCl, NO2Cl; liquid phase contg. POCl3, P2O3Cl4 and a small amount of P4O4Cl10;; isolation of liquid products by fractionation; yield of P2O3Cl4 5 %, P4O4Cl10 10 %;;A n/a
B 10%
C 5%
D n/a
E n/a
116-14-3

polytetrafluoroethylene

10102-43-9

nitrogen(II) oxide

10544-72-6

dinitrogen tetraoxide

356-16-1

1,1,2,2-tetrafluoro-1,2-dinitro-ethane

Conditions
ConditionsYield
molar ratio of NO:CF2CF2:N2O4=1:1:0.5;24%
molar ratio of NO:CF2CF2:N2O4=1:1:0.5;24%
10544-72-6

dinitrogen tetraoxide

7719-12-2, 52843-90-0

phosphorus trichloride

A

10544-73-7

dinitrogen trioxide

B

P4O4Cl10

C

P2O6NCl2

D

13498-14-1

pyrophosphoryl chloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: NOCl, NO2Cl, NO; passing dry N2O4 over the surface of freshly distd. PCl3 cooled at -10 °C; absortion under formation of a dark red liq.; expelling NO, N2O3, NOCl, NO2Cl and pptn. of P2O6NCl2; liquid phase contg. POCl3, P2O3Cl4 and a small amount of P4O4Cl10;; isolation of liquid products by fractionation; yield of P2O3Cl4 17 % and of P4O4Cl10 5 %;;A n/a
B 5%
C n/a
D 17%
E n/a
31702-89-3

1-nitrosotetrafluoroethanesulfonyl fluoride

10544-72-6

dinitrogen tetraoxide

31702-90-6

1-nitrotetrafluoroethanesulfonyl fluoride

Conditions
ConditionsYield
at 50°C 5 h in autoclav;15%

O11Pr6, β

10544-72-6

dinitrogen tetraoxide

praseodymium(III) nitrate

Conditions
ConditionsYield
In nitromethane suspension of Pr6O11 in nitromethane; ambient temp.;10%
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  • NITROGEN DIOXIDE CAS NO.10544-72-6

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    Product Name: NITROGEN DIOXIDE Synonyms: Distickstofftetroxid;N2O4;Nitrogen dioxide, di-;Nitrogen oxide (N2O4);nitrogenoxide(n2o4);nitrogentetraoxide;nitrogentetroxide,liquid;DINITROGEN TETROXIDE

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Chemistry

Synonyms: Distickstofftetroxid;N2O4;nitrogentetroxide,liquid;Nitrogen oxide (N2O4);nitrogenoxide(n2o4);nitrogentetraoxide;
MF: N2O4
MW: 92.01
mp:-11℃(lit.)
bp:21℃(lit.)
density:2.62 g/mL at 25 ℃(lit.)
vapor pressure:14.33 psi (20℃)
vapor density:1.58 (21℃, vsair)
EINECS: 233-272-6

Uses

It mainly  used as a rocket propellant。

Toxicity Data With Reference

1.   

ihl-rbt LC50:315 ppm/15M

   AIHAAP    American Industrial Hygiene Association Journal. 23 (1962),457.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

A poison. Moderately toxic by inhalation. When heated to decomposition it emits toxic fumes of NOx. See also NITROGEN MONOXIDE, mixed with NITROGEN TETROXIDE.
WGK Germany:1
Hazard Codes:T+
RTECS:QX1575000
RIDADR :UN 1067 2.3
Risk Statements:26-34
Safety Statements:9-26-28-36/37/39-45

Standards and Recommendations

DOT Classification:  2.3; Label: Poison Gas, Oxidizer