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105618-26-6

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Basic Information
CAS No.: 105618-26-6
Name: NOR-BINALTORPHIMINE DIHYDROCHLORIDE
Article Data: 4
Molecular Structure:
Molecular Structure of 105618-26-6 (NOR-BINALTORPHIMINE DIHYDROCHLORIDE)
Formula: C40H43 N3 O6
Molecular Weight: 734.72
Synonyms: 4,8:11,15-Dimethano-20H-bisbenzofuro[2,3-a:3',2'-i]dipyrido[4,3-b:3',4'-h]carbazole-1,8a,10a,18-tetrol,7,12-bis(cyclopropylmethyl)-5,6,7,8,9,10,11,12,13,14,19a,20b-dodecahydro-,[8R-(4bS*,8a,8ab,10aa,11b,14aS*,19aa,20bb)]-; N-Demethylbinaltorphimine;N-Demethylbinaltrorphimine; NorBNI; Norbinaltorphimine; Norbinaltorphine;Norbinaltrorphimine
Density: 1.63 g/cm3
Melting Point: 280ºC
Boiling Point: °Cat760mmHg
Flash Point: °C
Solubility: Soluble in ethanol; sonification required.
Appearance: Tan solid.
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
PSA: 121.65000
LogP: 5.30390
Related products
Synthetic route
16676-29-2

naltrexone Hydrochloride

105618-26-6

norbinaltorphimine

Conditions
ConditionsYield
With hydrazine dihydrochloride; methanesulfonic acid In N,N-dimethyl-formamide at 105℃; Temperature; Solvent; Reagent/catalyst; Inert atmosphere;96%
With hydrazine dihydrochloride; methanesulfonic acid 1.) DMF, 100 deg C, 6 h, 2.) DMSO, 130 deg C, 3 h; Yield given. Multistep reaction;
16676-29-2

naltrexone Hydrochloride

A

C40H46N4O6*2ClH

B

105618-26-6

norbinaltorphimine

Conditions
ConditionsYield
With hydrazine dihydrochloride In N,N-dimethyl-formamide at 100℃; Reagent/catalyst; Temperature;A 80%
B 9%
With hydrazine dihydrochloride; methanesulfonic acid In N,N-dimethyl-formamide at 109℃; Reagent/catalyst; Temperature;A 30%
B 60%
16676-29-2

naltrexone Hydrochloride

71-68-1

hydromorphone hydrochloride

A

105618-26-6

norbinaltorphimine

B

17-(cyclopropylmethyl),17'-methyl-6,6',7,7'-tetradehydro-4,5:4',5'-diepoxy-6,6'-(imino)<7,7'-bimorphinan>-3,3',14-triol

C

C34H35N3O4*2ClH

Conditions
ConditionsYield
With 1-amino-pyrrolidine-2,5-dione; hydrochloride In N,N-dimethyl-formamide at 100℃; for 18h;A 19%
B 24.5%
C 12%
...Expand
16590-41-3

Naltrexone

105618-26-6

norbinaltorphimine

Conditions
ConditionsYield
Stage #1: Naltrexone With hydrazine In N,N-dimethyl-formamide at 100℃;
Stage #2: With methanesulfonic acid In dimethyl sulfoxide at 130℃;
4224-69-5

methyl 2-(bromomethyl)propenoate

105618-26-6

norbinaltorphimine

3,3'-bis<(2-carbomethoxyallyl)oxy>-17,17'-bis(cyclopropylmethyl)-6,6',7,7'-tetradehydro-4,5:4',5'-diepoxy-6,6'-imino<7,7'-bimorphinan>-14,14'-diol

Conditions
ConditionsYield
With sodium hydroxide; tetrabutylammomium bromide In dichloromethane for 2h;97%
100-39-0

benzyl bromide

105618-26-6

norbinaltorphimine

17,17'-bis(cyclopropylmethyl)-6,6',7,7'-tetrahydro-4,5:4',5'-diepoxy-6,6'-(benzylimino)[7,7'-bimorphinan]-3,3',14,14'-tetrol dihydrochloride

Conditions
ConditionsYield
Stage #1: norbinaltorphimine With 18-crown-6 ether; sodium hydride In tetrahydrofuran at 20℃; for 0.333333h;
Stage #2: benzyl bromide In tetrahydrofuran for 43h;
Stage #3: With hydrogenchloride In methanol at 90℃; for 40h;		63%
186581-53-3, 908094-01-9

diazomethane

105618-26-6

norbinaltorphimine

A

17,17'-bis(cyclopropylmethyl)-3-methoxy-6,6',7,7'-tetradehydro-4,5:4',5'-diepoxy-6,6'-(imino)<7,7'-bimorphinan>-3',14,14'-triol

B

17,17'-bis(cyclopropylmethyl)-3,3'-dimethoxy-6,6',7,7'-tetradehydro-4,5:4',5'-diepoxy-6,6'-(imino)<7,7'-bimorphinan>-14,14'-diol

Conditions
ConditionsYield
In methanol; diethyl ether at 24℃; for 0.166667h;A 56%
B 28%
...Expand
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