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108-03-2

Basic Information
CAS No.: 108-03-2
Name: 1-Nitropropane
Article Data: 53
Molecular Structure:
Molecular Structure of 108-03-2 (1-Nitropropane)
Formula: C3H7NO2
Molecular Weight: 89.0941
Synonyms: NSC 6363;
EINECS: 203-544-9
Density: 0.981 g/cm3
Melting Point: -108 °C
Boiling Point: 131.714 °C at 760 mmHg
Flash Point: 42.337 °C
Solubility: 1.40 g/100 mL in water
Appearance: liquid
Hazard Symbols: HarmfulXn
Risk Codes: 10-20/21/22
Safety: 9
Transport Information: UN 2608 3/PG 3
PSA: 45.82000
LogP: 1.19630
Synthetic route
627-39-4

propionaldehyde oxime

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With magnesium hydroxide; dihydrogen peroxide In propan-1-ol; water at 80℃; under 5250.53 Torr;95.5%
With ammonium hydroxide; dihydrogen peroxide In methanol at 70℃; under 760.051 Torr; Green chemistry; chemoselective reaction;97 %Chromat.
75-52-5

nitromethane

557-20-0

diethylzinc

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With diethyl ether anschliessend Behandeln mit Wasser;
543-67-9

n-propyl nitrite

108-03-2

1-Nitropropane

Conditions
ConditionsYield
at 125 - 130℃;
beim Erhitzen;
74-98-6

propane

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With oxygen; nitric acid in der Gasphase;
With nitric acid; chlorine in der Gasphase;
With bromine; oxygen; nitric acid in der Gasphase;
With oxygen; nitric acid; chlorine in der Gasphase;
74-98-6

propane

A

79-46-9

2-nitropropane

B

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With nitric acid at 400℃;
With Nitrogen dioxide at 250 - 795℃;
With Nitrogen dioxide at 250℃;
With nitric acid In water at 285℃; under 72402.6 Torr; Product distribution / selectivity;
106-94-5

propyl bromide

A

543-67-9

n-propyl nitrite

B

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With silver(I) nitrite
107-08-4

1-iodo-propane

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With silver(I) nitrite
With poly(N-ethyl-4-vinylpyridinium)nitrite In hexane at 20℃; for 43h;
107-08-4

1-iodo-propane

A

543-67-9

n-propyl nitrite

B

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With silver(I) nitrite
3156-70-5

1-Nitropropen

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With tetrahydrofuran; diethyl ether; Trimethyl borate; sodium at -70℃;
106-97-8

n-butane

108-03-2

1-Nitropropane

Conditions
ConditionsYield
With nitric acid at 375℃;
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Chemistry

IUPAC Name: 1-Nitropropane
Product Name: 1-Nitropropane
The MF of 1-Nitropropane (CAS NO.108-03-2) is C3H7NO2.

                             
The MW of 1-Nitropropane (CAS NO.108-03-2) is 89.09.
Synonyms of 1-Nitropropane (CAS NO.108-03-2): 1-Nitropane ; 1-Nitropan ; 1-Nitro-propan ; 1-NP ; Ai3-02264 ; N-C3H7NO2 ; NiPar S-10 ; Nitropropane(non-specificname)
Product Categories: Industrial/Fine Chemicals;Organics;Nitro Compounds;Nitrogen Compounds;Organic Building Blocks;Alpha Sort;Chemical Class
Appearance: Colorless liquid with a somewhat disagreeable odor
Stability: Stable. Flammable. Incompatible with strong bases, strong oxidizing agents
Index of Refraction: 1.398  
EINECS: 203-544-9
Density: 0.98 g/ml 
Flash Point: 42.3 °C
Boiling Point: 131.7 °C
Melting Point: -108 °C
Storage temp: Flammables area
Water Solubility: 1.40 g/100 mL
Merck: 14,6627
BRN: 506236

Uses

  1-Nitropropane (CAS NO.108-03-2) is used as primarily as solvents and intermediates, jet engine fuel, sprays and so on.

Production

Preparation Products: Isobutyric acid-->Nitroethane-->2-Nitropropane
Raw materials: Nitric acid-->Nitromethane-->Nitroethane-->2-Nitropropane

Toxicity Data With Reference

1.    

eye-hmn 150 ppm/15M

    JIHTAB    Journal of Industrial Hygiene and Toxicology. 28 (1946),262.
2.    

dns-rat:lvr 1 µmol/L

    MUREAV    Mutation Research. 221 (1989),263.
3.    

ihl-hmn TCLo:150 ppm:EYE

    JIHTAB    Journal of Industrial Hygiene and Toxicology. 28 (1946),262.
4.    

orl-rat LD50:455 mg/kg

    NPIRI*    Raw Material Data Handbook, Vol.1: Organic Solvents, 1974. 1 (1974),91.
5.    

ihl-rat LC50:3100 ppm/8H

    NPIRI*    Raw Material Data Handbook, Vol.1: Organic Solvents, 1974. 1 (1974),91.
6.    

orl-mus LD50:800 mg/kg

    GISAAA    Gigiena i Sanitariya. 32 (9)(1967),9.
7.    

ipr-mus LD50:250 mg/kg

    KHFZAN    Khimiko-Farmatsevticheskii Zhurnal. Chemical Pharmaceutical Journal. 10 (6)(1976),53.
8.    

orl-rbt LDLo:250 mg/kg

    JIHTAB    Journal of Industrial Hygiene and Toxicology. 22 (1940),315.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by ingestion and intraperitoneal routes. Mildly toxic by inhalation. A human eye irritant. Human systemic effects by inhalation: conjunctiva irritation. Mutation data reported. Very dangerous fire hazard when exposed to heat, open flame, or oxidizers. Reacts violently with Ca(OH)2, hydrocarbons, hydroxides, inorganic bases. May explode on heating. Metal oxides increase its sensitivity to thermal ignition. To fight fire, use alcohol foam, CO2, dry chemical, water spray. When heated to decomposition it emits toxic fumes of NOx. See also 2-NITROPROPANE, NITROALKANES, and NITRO COMPOUNDS.Safety information of 1-Nitropropane (CAS NO.108-03-2):
Hazard Codes  HarmfulXn
Risk Statements 
10 Flammable
20/21/22 Harmful by inhalation, in contact with skin and if swallowed
Safety Statements 
9 Keep container in a well-ventilated place
RIDADR  UN 2608 3/PG 3
WGK Germany  1
RTECS  TZ5075000
HazardClass  3
PackingGroup  III
HS Code  29042000

Standards and Recommendations

OSHA PEL: TWA 25 ppm
ACGIH TLV: TWA 25 ppm; Not Classifiable as a Human Carcinogen
DFG MAK: 25 ppm (92 mg/m3)

Analytical Methods

For occupational chemical analysis use OSHA: #46.