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1089687-03-5

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Basic Information
CAS No.: 1089687-03-5
Name: Di(2-ethylhexyl)dichlorosilane
Article Data: 3
Molecular Structure:
Molecular Structure of 1089687-03-5 (Di(2-ethylhexyl)dichlorosilane)
Formula: C16H34Cl2S
Molecular Weight: 325.437
Synonyms: Di(2-ethylhexyl)dichlorosilane; Dichlorodi(2-ethylhexyl)silane;
EINECS: 802-348-6
Density: 0.924±0.06 g/cm3(Predicted)
Boiling Point: 132-138°C / 1.5
Risk Codes: 10-23/24/35-36/37/38
Safety: 36/37/39-62-43-26
PSA: 0.00000
LogP: 7.33900
Related products
Synthetic route
222058-04-0

trichloro(2-ethylhexyl)silane

2-ethylhexylmagnesium bromide

1089687-03-5

dichloro-bis(2-ethylhexyl)silane

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃;71%
In tetrahydrofuran at -10 - 20℃; for 6h;20%
32281-36-0

4,8-dihydrobenzo[1,2-b:4,5-b']dithiophene-4,8-dione

A

3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

B

1089687-03-5

dichloro-bis(2-ethylhexyl)silane

Conditions
ConditionsYield
In tetrahydrofuranA 71%
B n/a

2-ethylhexylmagnesium bromide

1089687-03-5

dichloro-bis(2-ethylhexyl)silane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: magnesium; tetrachlorosilane / water; tetrahydrofuran / 12 h / 20 °C
2: tetrahydrofuran / 6 h / -10 - 20 °C
View Scheme
1089687-03-5

dichloro-bis(2-ethylhexyl)silane

207742-50-5

3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene

1089687-04-6

4,4'-bis(2-ethylhexyl)-5,5'-bis(trimethylsilyl)dithieno[3,2-b:2',3'-d]silole

Conditions
ConditionsYield
Stage #1: 3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.25h;
Stage #2: dichloro-bis(2-ethylhexyl)silane In tetrahydrofuran; hexane at -78 - 20℃;		72%
Stage #1: 3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene With n-butyllithium In tetrahydrofuran at 20℃; for 0.333333h;
Stage #2: dichloro-bis(2-ethylhexyl)silane In tetrahydrofuran at 75℃; for 2h;		67%
Stage #1: 3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.583333h; Inert atmosphere;
Stage #2: dichloro-bis(2-ethylhexyl)silane In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere;		58%
With n-butyllithium
Stage #1: 3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene With n-butyllithium In tetrahydrofuran; hexane at -80℃; for 0.583333h;
Stage #2: dichloro-bis(2-ethylhexyl)silane In tetrahydrofuran; hexane at -80 - 20℃; for 2h;
51751-44-1

3,3'dibromo-2,2'-bithiophene

1089687-03-5

dichloro-bis(2-ethylhexyl)silane

1207627-85-7

4,4'-bis-(2-ethylhexyl)-dithieno[3,2-b:2',3'-d]silole

Conditions
ConditionsYield
Stage #1: 3,3'dibromo-2,2'-bithiophene With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran; hexane at -78℃; for 1h;
Stage #2: dichloro-bis(2-ethylhexyl)silane In tetrahydrofuran; hexane at -78 - 20℃;		67%
Stage #1: 3,3'dibromo-2,2'-bithiophene With n-butyllithium In tetrahydrofuran; diethyl ether; hexane at -78℃; for 3h; Inert atmosphere;
Stage #2: dichloro-bis(2-ethylhexyl)silane In tetrahydrofuran; diethyl ether; hexane at -78 - 20℃; Inert atmosphere;		30%
1089687-03-5

dichloro-bis(2-ethylhexyl)silane

207742-50-5

3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene

1207627-85-7

4,4'-bis-(2-ethylhexyl)-dithieno[3,2-b:2',3'-d]silole

Conditions
ConditionsYield
Stage #1: 3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene With n-butyllithium In tetrahydrofuran
Stage #2: dichloro-bis(2-ethylhexyl)silane In tetrahydrofuran
1089687-03-5

dichloro-bis(2-ethylhexyl)silane

1089687-05-7

4,4’-bis(2-ethylhexyl)-5,5’-dibromo-dithieno[3,2-b:2',3'-d]silole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 0.33 h / 20 °C
1.2: 2 h / 75 °C
2.1: N-Bromosuccinimide / water; tetrahydrofuran / 10 °C
View Scheme
1089687-03-5

dichloro-bis(2-ethylhexyl)silane

1089687-06-8

2,2′-bistrimethylstannyl-4,4′-bis-(2-ethylhexyl)dithieno[3,2-b:2′,3′-d]silole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 0.33 h / 20 °C
1.2: 2 h / 75 °C
2.1: N-Bromosuccinimide / water; tetrahydrofuran / 10 °C
3.1: n-butyllithium / tetrahydrofuran / 0.67 h / 20 °C
3.2: 2 h / 20 °C
View Scheme
1089687-03-5

dichloro-bis(2-ethylhexyl)silane

C74H94F2N6S6Si

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran / 0.33 h / 20 °C
1.2: 2 h / 75 °C
2.1: N-Bromosuccinimide / water; tetrahydrofuran / 10 °C
3.1: n-butyllithium / tetrahydrofuran / 0.67 h / 20 °C
3.2: 2 h / 20 °C
4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 2 h / 170 °C / Inert atmosphere
View Scheme
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