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| CAS No.: | 110-60-1 |
|---|---|
| Name: | 1,4-Diaminobutane |
| Molecular Structure: | |
|
|
|
| Formula: | C4H12N2 |
| Molecular Weight: | 88.1527 |
| Synonyms: | Tetramethylenediamine(7CI);1,4-Butylenediamine;1,4-Diamino-n-butane;1,4-Tetramethylenediamine;NSC 60545;Putramine;Putrascine;Putrescin;Putrescine;a,w-Butanediamine; |
| EINECS: | 203-782-3 |
| Density: | 0.865 g/cm3 |
| Melting Point: | 27 °C |
| Boiling Point: | 159.01 °C at 760 mmHg |
| Flash Point: | 51.667 °C |
| Solubility: | cell culture medium: 0.16 mg/mL |
| Appearance: | colourless liquid |
| Hazard Symbols: |
 F,  T
|
| Risk Codes: | 11-21/22-23-34 |
| Safety: | 16-26-36/37/39-45 |
| Transport Information: | UN 2928 6.1/PG 2 |
| PSA: | 52.04000 |
| LogP: | 1.08460 |
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| Conditions | Yield |
|---|---|
| With potassium hydroxide In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; | 95.4% |
| Conditions | Yield |
|---|---|
| With rubidium hydroxide; hydrogen; ethylenediamine; RaNi catalyst doped with Fe and Cr, slurry in water In water at 80℃; under 525053 Torr; Product distribution / selectivity; | A 3% B 1% C 92% |
| With cesium hydroxide; hydrogen; ethylenediamine; RaNi catalyst doped with Fe and Cr, slurry in water In water at 80℃; under 525053 Torr; Product distribution / selectivity; | A 3% B 5% C 90% |
| With sodium hydroxide; hydrogen; ethylenediamine; RaNi catalyst doped with Fe and Cr, slurry in water In water at 80℃; under 525053 Torr; Product distribution / selectivity; | A 4% B 5% C 85% |
| Conditions | Yield |
|---|---|
| With ammonium formate; zinc In methanol for 0.133333h; Heating; | 91% |
| With ammonium formate; magnesium In methanol at 20℃; for 0.833333h; | 81% |
| With hydrogenchloride; ethanol; water Hydrogenation.an Platin; | |
| With ethanol; sodium bei Siedehitze; | |
| With sodium amalgam; ethanol; acetic acid at 50 - 60℃; |
- 32754-99-7
4-aminobutyronitrile
- 110-60-1
1,4-diaminobutane
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; nickel dichloride In ethanol; acetonitrile at 20℃; | 79% |
| Conditions | Yield |
|---|---|
| With Cp*Rh(2-(2-pyridyl)phenyl)H; hydrogen In neat (no solvent) at 100℃; under 27361.8 Torr; for 48h; Catalytic behavior; Glovebox; | 78% |
| With potassium hydroxide; aluminum nickel for 2.5h; | 61% |
| With ethanol; sodium |
| Conditions | Yield |
|---|---|
| With ammonia; nickel at 140℃; under 80905.8 Torr; Hydrogenation; |
| Conditions | Yield |
|---|---|
| With cobalt catalyst; ammonia at 120℃; under 62518.2 - 154457 Torr; Hydrogenation; | |
| With Methyl formate; cobalt catalyst at 65 - 85℃; under 102971 - 154457 Torr; Hydrogenation.anschl. Eindampfen mit konz. HCl; | |
| With ethanol; ammonia; nickel at 100℃; under 62518.2 Torr; Hydrogenation; |
| Conditions | Yield |
|---|---|
| With potassium carbonate; N,N-dimethyl-formamide anschl. mit wss. NaOH; |
| Conditions | Yield |
|---|---|
| With chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid at 40℃; | |
| With chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid at 40℃; | |
| With chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid at 40℃; |
- 70-26-8, 348-66-3, 616-07-9, 7006-33-9
2,5-diaminopentanoic acid
- 110-60-1
1,4-diaminobutane
| Conditions | Yield |
|---|---|
| durch Einwirkung von Clostridium septicum; | |
| durch Einwirkung von Proteus vulgaris; | |
| durch Einwirkung von Proteus morganii; | |
| durch Einwirkung von Escherichia coli; |
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- Total:30 Page 1 of 1 1
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Chemistry
Chemical Name: 1,4-Diaminobutane
IUPAC NAME: Butane-1,4-diamine
CAS No.: 110-60-1
EINECS: 203-782-3
Molecular Formula: C4H12N2
Molecular Weight: 88.15 g/mol
Melting Point: 27 °C
Density: 0.864 g/cm3
Flash Point: 51.7 °C
Boiling Point: 159 °C at 760 mmHg
Following is the structure of 1,4-Butanediamine (110-60-1):
Product Categories about 1,4-Butanediamine (110-60-1) are alpha,omega-Alkanediamines ; alpha,omega-Bifunctional Alkanes ; Monofunctional & alpha,omega-Bifunctional Alkanes
The chemical synonymous of 1,4-Butanediamine (110-60-1) are 1,4-Butylenediamine ; 1,4-Tetramethylenediamine ; Butylene-1,4-diamine ; H2N(CH2)4NH2 ; Tetramethyldiamine ; RARECHEM AL BW 0068 ; Putrescin ; Putrescine
Uses
The major use of 1,4-Butanediamine (110-60-1) is as an intermediate in organic synthesis and it used for the pharmaceutical and biochemical research.
Toxicity Data With Reference
| 1. | cyt-hmn:hla 2 mmol/L | JCLLAX Journal of Cellular Physiology. 78 (1971),217. | ||
| 2. | dns-mus:lvr 2 mmol/L | AMOKAG Acta Medicia Okayama. 33 (1979),149. | ||
| 3. | dni-mus:ast 10 mmol/L | AMOKAG Acta Medicia Okayama. 33 (1979),149. | ||
| 4. | dni-mus:lvr 20 mmol/L | AMOKAG Acta Medicia Okayama. 33 (1979),149. | ||
| 5. | orl-mus LDLo:1600 mg/kg | AECTCV Archives of Environmental Contamination and Toxicology. 14 (1985),111. | ||
| 6. | orl-rbt LDLo:1600 mg/kg | CRSBAW Comptes Rendus des Seances de la Societe de Biologie et de Ses Filiales. 83 (1920),481. | ||
| 7. | orl-rbt LDLo:1600 mg/kg | CRSBAW Comptes Rendus des Seances de la Societe de Biologie et de Ses Filiales. 83 (1920),481. | ||
| 8. | scu-rbt LDLo:1 g/kg | ZEPTAT Zeitschrift fuer Experimentelle Pathologie und Therapie. 17 (1915),59. | ||
| 9. | ivn-rbt LDLo:80 mg/kg | CRSBAW Comptes Rendus des Seances de la Societe de Biologie et de Ses Filiales. 83 (1920),481. | ||
| 10. | rec-rbt LDLo:400 mg/kg | CRSBAW Comptes Rendus des Seances de la Societe de Biologie et de Ses F |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Poison by subcutaneous, intravenous, and rectal routes. Moderately toxic by ingestion. An experimental teratogen. Human mutation data reported. When heated to decomposition it emits toxic fumes of NOx. See also 1,3-BUTANEDIAMINE and AMINES.
Hazard Codes:
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Risk Statements about 1,4-Butanediamine (110-60-1):
R20/21/22 Harmful by inhalation, in contact with skin and if swallowed.
R34 Causes burns.
Safety Statements about 1,4-Butanediamine (110-60-1):
S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39 Wear suitable protective clothing, gloves and eye/face protection.
S45 In case of accident or if you feel unwell, seek medical advice immediately (show the label where possible).
Attentions:
1. Storage: Keep away from sources of ignition. Store in a cool, dry place. Store in a tightly closed container. Corrosives area. Store under nitrogen.
2. Handling: Do not get on skin and clothing. Do not breathe dust, vapor, mist, or gas. Use only in a chemical fume hood.