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1107-00-2

Basic Information
CAS No.: 1107-00-2
Name: 4,4'-(Hexafluoroisopropylidene)diphthalic anhydride
Article Data: 15
Molecular Structure:
Molecular Structure of 1107-00-2 (4,4'-(Hexafluoroisopropylidene)diphthalic anhydride)
Formula: C19H6F6O6
Molecular Weight: 444.243
Synonyms: Hexafluoroisopropylidene-2,2-bis(phthalic anhydride);[2,2,2-Trifluoro-1-(trifluoromethyl)ethylidene]diphthalic anhydride;Phthalicanhydride, 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylidene]di- (7CI);Phthalic anhydride, 4,4'-[trifluoro-1-(trifluoromethyl)ethylidene]di- (8CI);2,2-Bis(3,4-dicarboxyphenyl)-1,1,1,3,3,3-hexafluoropropane dianhydride;2,2-Bis(3,4-dicarboxyphenyl)hexafluoropropane dianhydride;4,4'-(Hexafluoroisopropylidene)bis(phthalic anhydride);4,4'-(Hexafluoroisopropylidene)diphthalic dianhydride;4,4'-Hexafluoroisopropylidenebis(benzene-1,2-dicarboxylic acid dianhydride);4,4'-Hexafluoroisopropylidenebisphthalic dianhydride;4,4'-Hexafluoropropylidenebisphthalic acid dianhydride;
EINECS: 214-170-0
Density: 1.697 g/cm3
Melting Point: 244-247 ºC
Boiling Point: 494.5 ºC at 760 mmHg
Flash Point: 243.7 ºC
Solubility: Insoluble in water
Appearance: White powder
Hazard Symbols: IrritantXi,CorrosiveC
Risk Codes: 34
Safety: 26-36/37/39-45
Transport Information: UN 3261 8/PG 2
PSA: 86.74000
LogP: 3.71850
Synthetic route
3016-76-0

1,1,1,3,3,3-hexafluoro-2,2-di(3,4-dicarboxyphenyl)-propane

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
at 250℃; for 3h; Temperature;89%
With 2,6-bis[(2,2,6,6-tetramethylpiperidin-1-yl)methyl]phenylboronic acid In propyl cyanide for 12h; Reflux;85%
In o-xylene at 180℃; for 3h;3.5 g
108-24-7

acetic anhydride

65294-20-4

4,4'-(perfluoropropane-2,2-diyl)bis(1,2-dimethylbenzene)

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Stage #1: 4,4'-(hexafluoroisopropylidene)-bis-(o-xylene) With pyridine; potassium permanganate In water at 100℃; for 3h;
Stage #2: acetic anhydride In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 0.666667h; Temperature;
79%
95-47-6

o-xylene

aluminium silicate

aluminium silicate

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: AlCl3 / 16 h / 110 °C
2: aq. KMnO4 / pyridine / 12 h / Heating
3: 3.5 g / o-xylene / 3 h / 180 °C
View Scheme
Multi-step reaction with 3 steps
1: 69 percent / HF / 18 h / 130 °C / 22065.2 Torr
2: aq. KMnO4 / pyridine / 12 h / Heating
3: 3.5 g / o-xylene / 3 h / 180 °C
View Scheme
65294-20-4

4,4'-(perfluoropropane-2,2-diyl)bis(1,2-dimethylbenzene)

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aq. KMnO4 / pyridine / 12 h / Heating
2: 3.5 g / o-xylene / 3 h / 180 °C
View Scheme
91-15-6

phthalonitrile

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: benzenesulfonic acid / dichloromethane / 60 h / 150 - 160 °C / Inert atmosphere
2: water; potassium hydroxide / methanol / 40 h / 110 °C
3: acetic anhydride / toluene / 10 h / 120 °C
View Scheme
95-47-6

o-xylene

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: Reflux
1.2: 17 h / 115 °C / 7980.54 Torr / Autoclave; Inert atmosphere
2.1: pyridine; potassium permanganate / water / 3 h / 100 °C / pH 1
3.1: 3 h / 250 °C
View Scheme
1515-72-6

N-butylphthalimide

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: iron(III) chloride; sulfuric acid / 80 h / 100 °C
2: water; potassium hydroxide / 18 h / 95 °C
3: 3 h / 250 °C
View Scheme

4,4'-(hexafluoroisopropylidene)bis(N-butylphthalimide)

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: water; potassium hydroxide / 18 h / 95 °C
2: 3 h / 250 °C
View Scheme
73340-33-7

2,2-bis(3-nitro-4-hydroxyphenyl)hexafluoropropane

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: palladium on activated charcoal; hydrogen / 2-methyl-propan-1-ol; acetic acid butyl ester
2: ammonia
3: nitrosylsulfuric acid / acetic acid
4: water
5: Heating; Acidic conditions
6: Heating
View Scheme
Multi-step reaction with 6 steps
1: hydrogen; palladium on activated charcoal / butan-1-ol; acetic acid butyl ester
2: ammonia
3: nitrosyl sulphuric acid / acetic acid
4: urea
5: Heating; Acidic conditions
6: Heating
View Scheme
83558-87-6

2,2-bis(3-amino-4-hydroxyphenyl)hexafluoropropane

1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: ammonia
2: nitrosylsulfuric acid / acetic acid
3: water
4: Heating; Acidic conditions
5: Heating
View Scheme
Multi-step reaction with 5 steps
1: ammonia
2: nitrosyl sulphuric acid / acetic acid
3: urea
4: Heating; Acidic conditions
5: Heating
View Scheme
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    Product Name: 4,4'-(Hexafluoroisopropylidene)diphthalic anhydride CAS: 1107-00-2 MF: C19H6F6O6 MW: 444.24 EINECS: 214-170-0 4,4'-(Hexafluoroisopropylidene)diphthalic anhydride Structure 4,4'-(Hexafluoroisopropylidene)diph

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  • CAS 1107-00-2 2,2-Bis(3,4-anhydrodicarboxyphenyl)- hexafluoropropane(6FDA)

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    4,4'-(Hexafluoroisopropylidene)diphthalic anhydride Basic information Product Name: 4,4'-(Hexafluoroisopropylidene)diphthalic anhydride Synonyms: 4,4'-(Hexafluoroisop;[2,2,2-Trifluoro-1-(trifluoroMethyl)ethylidene]diphthalic anhydride;2,2

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Chemistry

The Molecular Structure of 1,3-Isobenzofurandione, 5,5'-(2,2,2-trifluoro-1-(trifluoromethyl)ethylidene)bis- (CAS NO.1107-00-2):

Empirical Formula: C19H6F6O6
Molecular Weight: 444.2378 
IUPAC: 5-[2-(1,3-dioxo-2-benzofuran-5-yl)-1,1,1,3,3,3-hexafluoropropan-2-yl]-2-benzofuran-1,3-dione
Product Categories: Aromatic Tetracarboxylic Dianhydrides (for High-Performance Polymer Research);Bisphenol AF type Compounds (for High-Performance Polymer Research);Functional Materials;Reagent for High-Performance Polymer Research;Anhydride Monomers;Monomers;Polymer Science
Nominal Mass: 444 Da
Average Mass: 444.2378 Da
Monoisotopic Mass: 444.006857 Da 
Index of Refraction: 1.556
Molar Refractivity: 84.17 cm3
Molar Volume: 261.7 cm3
Surface Tension: 50.2 dyne/cm
Density: 1.697 g/cm3
Flash Point: 243.7 °C
Enthalpy of Vaporization: 76.19 kJ/mol
Boiling Point: 494.5 °C at 760 mmHg
Vapour Pressure: 6.4E-10 mmHg at 25°C 
Sensitive: Moisture Sensitive
InChI
InChI=1/C19H6F6O6/c20-18(21,22)17(19(23,24)25,7-1-3-9-11(5-7)15(28)30-13(9)26)8-2-4-10-12(6-8)16(29)31-14(10)27/h1-6H
Smiles
C(C(F)(F)F)(C(F)(F)F)(c1cc2c(cc1)C(=O)OC2=O)c1cc2C(OC(=O)c2cc1)=O

Safety Profile

Hazard Codes: CorrosiveCIrritantXi
Risk Statements: 34 
R34: Causes burns
Safety Statements: 26-36/37/39-45 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: UN 3261 8/PG 2
WGK Germany: 1
F 21: Sensitive to humidity
Hazard Note: Irritant
TSCA: T
HazardClass: 8
PackingGroup: II

Specification

 1,3-Isobenzofurandione, 5,5'-(2,2,2-trifluoro-1-(trifluoromethyl)ethylidene)bis- (CAS NO.1107-00-2) is also called as 2,2'-Bis(3,4-dicarboxyphenyl)hexafluoropropane dianhydride ; 4,4'-(Hexafluoroisopropylidene)bis(phthalic anhydride) ; EINECS 214-170-0 ; 4,4'-(2,2,2-Trifluoro-1-(trifluoromethyl)ethylidene)diphthalic anhydride .