CAS No.111-95-5,BIS(2-METHOXYETHYL)AMINE Suppliers

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Basic Information

Molecular Structure:
CAS No.:	111-95-5
Name:	BIS(2-METHOXYETHYL)AMINE
Article Data:	14

Formula:	C₆H₁₅NO₂
Molecular Weight:	133.191
Synonyms:	Diethylamine,2,2'-dimethoxy- (6CI,7CI,8CI);2,2'-Dimethoxydiethylamine;2-Methoxy-N-(2-methoxyethyl)ethanamine;Di(2-methoxyethyl)amine;N,N-Bis(2-methoxyethyl)amine;NSC 78431;
EINECS:	203-923-9
Density:	0.893 g/cm³
Melting Point:	< -60 °C
Boiling Point:	171 °C at 760 mmHg
Flash Point:	58.3 °C
Solubility:	Completely miscible in water
Appearance:	Colorless to yellow liquid
Hazard Symbols:	C
Risk Codes:	34
Safety:	26-36/37/39-45
Transport Information:	UN 2734
PSA:	30.49000
LogP:	0.25970

Synthetic route

: 89855-74-3
N,N-bis(2-methoxyethyl)formamide

: 111-95-5
Bis-(2-methoxyethyl)amine

Conditions

Conditions	Yield
With RuCl2[(Ph2PCH2CH2)2NH](t-Bu-NC); potassium tert-butylate; deuterium at 120℃; under 15201 Torr; for 16h;

: N,N-bis(2-methoxyethyl)tritylamine

: 111-95-5
Bis-(2-methoxyethyl)amine

Conditions

Conditions	Yield
Stage #1: N,N-bis(2-methoxyethyl)tritylamine With naphthalene; lithium In tetrahydrofuran at 0℃; for 2h; Stage #2: With water In tetrahydrofuran at 0 - 20℃;	90%

: bis(2-methoxyethyl)(triphenylsilyl)amine

: 111-95-5
Bis-(2-methoxyethyl)amine

Conditions

Conditions	Yield
With naphthalene; lithium In tetrahydrofuran; methanol at 20℃; for 5h;	97%

: 343581-97-5
N,N-bis(2-methoxyethyl)-4-methylbenzenesulfonamide

: 111-95-5
Bis-(2-methoxyethyl)amine

Conditions

Conditions	Yield
Product distribution / selectivity;	86%
Stage #1: N,N-bis(2-methoxyethyl)-4-methylbenzenesulfonamide With Na/K absorbed into silica gel In tetrahydrofuran at 20℃; Inert atmosphere; Stage #2: With water In tetrahydrofuran	85%

: N,N-bis(2-methoxyethyl)pivalamide

: 111-95-5
Bis-(2-methoxyethyl)amine

Conditions

Conditions	Yield
With naphthalene; lithium In tetrahydrofuran at 0℃; for 1h;	45 % Chromat.

: 6482-24-2
2-Bromoethyl methyl ether

A: 111-95-5
Bis-(2-methoxyethyl)amine

B: 2-methoxy-ethylamine; hydrobromide

Conditions

Conditions	Yield
With ammonia In methanol at 130℃; for 2.5h; microwave irradiation;

: N,N-bis(2-methoxyethyl)benzenesulfonamide

: 111-95-5
Bis-(2-methoxyethyl)amine

Conditions

Conditions	Yield
Product distribution / selectivity;	75%

: 627-42-9
2-chloroethyl methyl ether

: 111-95-5
Bis-(2-methoxyethyl)amine

Conditions

Conditions	Yield
With ammonia In methanol

: 109-86-4
2-methoxy-ethanol

A: 111-95-5
Bis-(2-methoxyethyl)amine

B 2-methoxy-ethylamine and tris-<2-methoxy-ethyl>-amine: 2-methoxy-ethylamine and tris-<2-methoxy-ethyl>-amine

Conditions

Conditions	Yield
With ammonia; nickel at 240℃;

: 627-42-9
2-chloroethyl methyl ether

: 109-85-3
2-methoxyethylamine

: 111-95-5
Bis-(2-methoxyethyl)amine

Raw Materials

627-42-9

109-85-3

109-86-4

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Specification

The Ethanamine, 2-methoxy-N-(2-methoxyethyl)-, with the CAS registry number of 111-95-5, is also known as Bis(2-methoxyethyl)amine. It belongs to the product categories of Amino Alcohols; Organic Building Blocks; Oxygen Compounds. Its EINECS registry number is 203-923-9. This chemical's molecular formula is C₆H₁₅NO₂ and molecular weight is 133.19. What's more, its IUPAC name is 2-Methoxy-N-(2-methoxyethyl)ethanamine. In addition, it must be stored in airtight containers and placed in a cool, ventilated place. Meanwhile, it should be avoided contact with ignition source, heat source, air, oxidant, acid.

Physical properties about Ethanamine, 2-methoxy-N-(2-methoxyethyl)- are: (1)ACD/LogP: -0.26; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -3.09; (4)ACD/LogD (pH 7.4): -1.55; (5)ACD/BCF (pH 5.5): 1; (6)ACD/BCF (pH 7.4): 1; (7)ACD/KOC (pH 5.5): 1; (8)ACD/KOC (pH 7.4): 1; (9)#H bond acceptors: 3; (10)#H bond donors: 1; (11)#Freely Rotating Bonds: 6; (12)Polar Surface Area: 21.7 Å²; (13)Index of Refraction: 1.409; (14)Molar Refractivity: 36.93 cm³; (15)Molar Volume: 149.1 cm³; (16)Surface Tension: 26.4 dyne/cm; (17)Density: 0.893 g/cm³; (18)Flash Point: 58.3 °C; (19)Enthalpy of Vaporization: 40.74 kJ/mol; (20)Boiling Point: 171 °C at 760 mmHg; (21)Vapour Pressure: 1.43 mmHg at 25 °C.

Uses of Ethanamine, 2-methoxy-N-(2-methoxyethyl)-: it is used to produce other chemicals. For example, it is used to produce N, N-Bis-(2-methoxy-ethyl)-aniline. This reaction needs reagent KOH, catalyst Naphthoquinone imidazolin-2-ylidene-palladium(0) complex and solvent Dioxane. The reaction time is 16 hours with reaction temperature of 100 °C. The yield is about 67 %.

Ethanamine, 2-methoxy-N-(2-methoxyethyl)- can react with 3, 6-Dichloro-pyridazine to get N, N-Bis-(2-methoxy-ethyl)-aniline.

When you are using this chemical, please be cautious about it as the following:
This chemical may cause burns on contact. During using it, wear suitable protective clothing, gloves and eye/face protection. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1) SMILES: O(C)CCNCCOC
(2) InChI: InChI=1/C6H15NO2/c1-8-5-3-7-4-6-9-2/h7H,3-6H2,1-2H3
(3) InChIKey: IBZKBSXREAQDTO-UHFFFAOYAE