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11113-50-1

Basic Information
CAS No.: 11113-50-1
Name: Boric acid
Molecular Structure:
Molecular Structure of 11113-50-1 (Boric acid)
Formula: BH3O3
Molecular Weight: 61.83
Synonyms: UNII-R57ZHV85D4;
EINECS: 234-343-4
Density: 1.437 g/cm3
Melting Point: 170.9oC
Boiling Point:
Flash Point:
Solubility: 49.5 g/L (20℃)
Appearance: White powder
Hazard Symbols: R60:;
Risk Codes:  T:Toxic;
">  T:Toxic;
Safety:
Transport Information:
PSA: 60.69000
LogP: -2.05180
Synthetic route
916730-63-7

1-boranyl-1,3,5-triaza-7-phosphaadamantane

A

11113-50-1

boric acid

B

53597-69-6

(1,3,5-triaza-7-phosphaadamantane)

Conditions
ConditionsYield
In water; acetone B-complex reacted with water in acetone/water (1:1) at 80°C for ca. 48 h; detn. by IR, 11B-NMR;A 100%
B n/a
In acetone slow reaction of B-complex with water; acceleration at higher temp.;A 100%
B n/a
4262-38-8

1,3,5,7-Tetra-tert-butyl-2,4,6,8-tetrachloro-[1,3,5,7,2,4,6,8]tetrazatetraborocane

A

11113-50-1

boric acid

B

75-64-9

tert-butylamine

Conditions
ConditionsYield
With water In further solvent(s) byproducts: HCl; solvent cyclohexanol, in tube 20.5 h at 160°C;A n/a
B 97%
With H2O In further solvent(s) byproducts: HCl; solvent cyclohexanol, in tube 20.5 h at 160°C;A n/a
B 97%
With water In xylene byproducts: HCl; in tube 20.5 h boiling;A n/a
B 62%
With H2O In xylene byproducts: HCl; in tube 20.5 h boiling;A n/a
B 62%
27120-66-7

closo-1-sulfinic acid-1,12-dicarbadodecaborane(12)

7722-84-1

dihydrogen peroxide

A

226255-50-1

closo-1,12-(H)2-1,12-C2B10(OH)10

B

396695-66-2

closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1-sulfonic acid-1,12-dicarbadodecaborane(12)

C

11113-50-1

boric acid

Conditions
ConditionsYield
In water aq. 30% H2O2 added to B compd.; refluxed for 3.5 h; monitored by (11)B NMR spectra; cond. HBr added; stirred (room temp., 2 h); kept. (80°C, 8 h); Br2 removed by N2 steam; volatiles removed in vac.; triturated in MeOH; centrifuged; supernatant sepd.; repeated 5 times; residue dissolved in water; filtered; dried;A 5%
B 88%
C 3%

[Pt((c-C5H9)7Si7O10(OH)2)(C6H5)(1,2-bis(diphenylphosphino)ethane)]

5720-07-0

4-methoxyphenylboronic acid

[Pt(C6H4OCH3-p)(C6H5)(1,2-bis(diphenylphosphino)ethane)]*H2O

B

11113-50-1

boric acid

Conditions
ConditionsYield
In tetrahydrofuran byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; B compd. was added to soln. of Pt complex in THF; heated at 60°C for 30 min; concd. (vac.); hexane added; cooled at -20°C; filtered; washed (H2O); dried (vac.); elem. anal.;A 88%
B n/a
In benzene-d6 byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; mixt. of B compd. and Pt complex in C6D6 was heated at 60°C for 30 min; NMR monitoring;
In tetrahydrofuran-d8 byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; mixt. of B compd. and Pt complex in THF-d8was heated at 60°C for 15 min; NMR monitoring;
1666-13-3

diphenyl diselenide

4844-17-1

2,4,5-triphenyl-1,3-dioxoborole

A

11113-50-1

boric acid

B

84-11-7

9,10-phenanthrenequinone

Conditions
ConditionsYield
In benzene Irradiation (UV/VIS); irrdn. for 2 h 40 min with a 450 W medium pressure mercury lamp (290 to 330 nm), under Ar; extn. (aq. NaOH), dried (Na2SO4), evapd., crystn. from hexane, yields 9,10-phenanthraquinone;A n/a
B 84%

[(Pt(Ph)(1,5-cyclooctadiene))2(μ-OH)](BF4)

182482-25-3

2,4,6-trifluorophenylboronic acid

899439-56-6

Pt(C6H2F3-2,4,6)(Ph)(1,5-cyclooctadiene)

B

11113-50-1

boric acid

Conditions
ConditionsYield
In water; toluene room temp., 1 h, toluene/H2O = 100/1;A 83%
B n/a
In toluene under inert atm. to suspn. Pt complex in toluene water and (C6H2F3-2,4,6)B(OH)2 were added and stirred at room temp. for 1 h; solvent was evapd., residue was extd. by CDCl3; product was identified by NMR;A 83%
B n/a

cesium(1+)*arachno-6-SB9H12(1-)

A

arachno-4-SB8H12

B

11113-50-1

boric acid

Conditions
ConditionsYield
With hydrogenchloride; formaldehyd In dichloromethane; water byproducts: H2, CH3OH; addn. of CH2Cl2, aq. soln. of CH2O and aq. HCl to suspn. of B-compd. in H2O, stirring (ambient temp., 20 min); sepn. of CH2Cl2 layer, drying (CaCl2), evapn. to dryness, sublimation (25°C, 1.3 Pa, cold surface at -70°C);A 81%
B n/a
31139-16-9

cyanoborane

A

74-90-8

hydrogen cyanide

B

1333-74-0

hydrogen

C

11113-50-1

boric acid

Conditions
ConditionsYield
hydrolysis at 90-95°C;A 60%
B 80%
C 60%
1111-47-3

tris(triphenylsiloxy)borane

11113-50-1

boric acid

Conditions
ConditionsYield
With acetic acid In benzene byproducts: triphenylacetoxysilane; reflux for 3h, molar ratio B-compd.:AcOH=1:3; H3BO3 pptd., elem. anal.;78%
1259401-57-4

[Pt((c-C5H9)7Si7O10(OH)2)(C6H5)(2,2'-bipyridine)]

5720-07-0

4-methoxyphenylboronic acid

[Pt(C6H4OCH3-p)(C6H5)(2,2'-bipyridine)]*H2O

B

11113-50-1

boric acid

Conditions
ConditionsYield
In tetrahydrofuran byproducts: (c-C5H9)7Si7O9(OH)3; (Ar); std. Schlenk technique; B compd. was added to soln. of Pt complex in THF; heated at 60°C for 4 h; concd. (vac.); hexane added; cooled at -20°C; filtered; washed (H2O); dried (vac.); elem. anal.;A 75%
B n/a
20644-59-1

o-carboranylacetic acid

443770-01-2

2-aminoethyl β-D-galactopyranosyl-(1->4)-O-β-D-glucopyranoside

A

(2-[(1,2-dicarba-nido-undecaborane(12)-1-yl)acetylamino]ethyl) 4-O-(β-D-galactopyranosyl)-β-D-glucopyranoside(1-)

B

(2-[(1,2-dicarba-closo-dodecaborane(12)-1-yl)acetylamino]ethyl) 4-O-(β-D-galactopyranosyl)-β-D-glucopyranoside

C

11113-50-1

boric acid

Conditions
ConditionsYield
With 4-(4,6-dimethoxy[1.3.5]triazin-2-yl)-4-methylmorph In methanol; water under Ar atm. to soln. carbohydrate amine and o-carboranylacetic acid inaq. MeOH 4-(4,6-dimethoxy(1.3.5)triazin-2-yl)4-methylmorpholinium chlor ide was added and stirred at room temp. for 22 h; volatiles were removed in vacuo, residue was dissolved in H2O, reverse-phase chromy. (SepPak C18, H2O -> MeOH);A 7.6%
B 74.2%
C n/a
121-43-7

Trimethyl borate

102-24-9

cyclotriboric acid trimethyl ester

A

67-56-1

methanol

B

11113-50-1

boric acid

Conditions
ConditionsYield
With waterA 72.5%
B n/a

tetramethyl-tetracarba-closo-docecaborane(12)

A

(CH3)4C4B7H9

B

11113-50-1

boric acid

Conditions
ConditionsYield
In ethanol; water stirred in air for 12 h; EtOH removed in vac., extd. (hexane), filtered on SiO2, evapd., productyield dependence on H2O concn. in EtOH (40-60%);A 48%
B 68%

[(Pt(Ph)(1,5-cyclooctadiene))2(μ-OH)](BF4)

98-80-6

phenylboronic acid

diphenyl(1,5-cyclooctadiene)platinum(II)

B

11113-50-1

boric acid

Conditions
ConditionsYield
In water; toluene room temp., 1 h, toluene/H2O = 100/1;A 66%
B n/a
In toluene under inert atm. to suspn. Pt complex in toluene water and PhB(OH)2 wereadded and stirred at room temp. for 1 h; solvent was evapd., residue was extd. by CDCl3; product was identified by NMR;A 66%
B n/a
In toluene room temp., 1 h;A 38%
B n/a

[(Pt(Ph)(1,5-cyclooctadiene))2(μ-OH)](BF4)

5720-07-0

4-methoxyphenylboronic acid

diphenyl(1,5-cyclooctadiene)platinum(II)

791838-95-4

(1,5-cyclooctadiene)Pt(C6H4-4-OMe)(C6H5)

C

11113-50-1

boric acid

Conditions
ConditionsYield
In toluene room temp., 1 h;A 64%
B 14%
C n/a
99506-47-5

phenyl(m-carboran-9-yl)chloronium tetrafluoroborate

A

17819-85-1

9-chloro-m-carborane

B

54360-42-8

9-hydroxy-1,7-dicarba-closo-dodecaborane

C

11113-50-1

boric acid

Conditions
ConditionsYield
With water In water stirred for 200 h, 20-40°C; extracted with benzene, evaporated to dryness, chromatographed on silica (1. benzene-hexane (1:1), 2. ether), IR;A 8%
B 56%
C 33%

anhydride of boric acid

11113-50-1

boric acid

Conditions
ConditionsYield
In water under N2 or Ar; by a react. of B-contg. compd. with H2O; evapn. of water at 80°C under vac.;52%
10294-33-4

boron tribromide

A

boron

B

boron trioxide

C

10043-11-5

boron nitride

boron

E

11113-50-1

boric acid

Conditions
ConditionsYield
With H2; N2 In neat (no solvent) Electric Arc; pulse heating (plasma, puls repitition rate 5-12,5 Hz, N2 flow 0.2 - 1.65 l/min, H2 flow 1.13 - 3.5 l/min9; further products; X-ray diffraction;A n/a
B n/a
C 50%
D n/a
E n/a
23704-81-6

1,6-dicarba-closo-decaborane(10)

11113-50-1

boric acid

Conditions
ConditionsYield
With HCl In tetrahydrofuran 25°C, 10 h, acidic hydrolysis;50%
16940-66-2

sodium tetrahydroborate

109-63-7

trifluoroborane diethyl ether

A

13755-29-8

sodium tetrafluoroborate

B

17702-41-9

nido-decaborane

C

60-29-7

diethyl ether

D

11113-50-1

boric acid

Conditions
ConditionsYield
With potassium permanganate; sulfuric acid In water; diethylene glycol; benzene byproducts: H2; NaBH4 in diglyme heated to 105°C and BF3*OEt2 added for 6 h and stirred for 1 h, mixt. cooled under N2 atm., water added, diglyme removed, H2SO4, benzene and KMnO4 added and react. mixt. stirred at 10°C; mixt. filtered, layers separated, benzene layer washed with water and dried over anhyd. MgSO4, evapd. and sublimed;A n/a
B 47%
C n/a
D n/a
With sulfuric acid; dihydrogen peroxide; iron(II) sulfate In hexane; water; diethylene glycol byproducts: H2; NaBH4 in diglyme heated to 105°C and BF3*OEt2 added for 6 h and stirred for 1 h, mixt. cooled under N2 atm., water added, diglyme removed, H2SO4, hexane and FeSO4, then H2O2 added and react. mixt. stirred at 35°C; mixt. filtered, layers separated, hexane layer washed with water and dried over anhyd. MgSO4;A n/a
B 44%
C n/a
D n/a
With sulfuric acid; dihydrogen peroxide In water; diethylene glycol; benzene byproducts: H2; NaBH4 in diglyme heated to 105°C and BF3*OEt2 added for 6 h and stirred for 1 h, mixt. cooled under N2 atm., water added, diglyme removed, H2SO4, benzene and then H2O2 added and react. mixt. stirred for 68 h; mixt. filtered, layers separated, benzene layer washed with water and dried over anhyd. MgSO4;A n/a
B 41.1%
C n/a
D n/a
396695-62-8

closo-1,12-bis(sulfonic acid)-1,12-dicarbadodecaborane(12)

7722-84-1

dihydrogen peroxide

A

396695-66-2

closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1-sulfonic acid-1,12-dicarbadodecaborane(12)

B

closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1,12-bis(sulfonicacid)-1,12-dicarbadodecaborane(12) hexahydrate

C

11113-50-1

boric acid

Conditions
ConditionsYield
In water excess of aq. 30% H2O2 added to B compd.; refluxed for 5 h; monitored by(11)B NMR spectra; concd. HBr added; stirred for 2 h at room temp.; kep t at 80°C for 8 h; Br2 removed by N2 steam; volatiles removed in vac.; triturated in MeOH; centrifuged; supernatant sepd.; repeated 5 times; residue dissolved in water; filtered; dried (mono-sulfonic acid compd.); MeOH washings evapd. slowly (bis-sulfonic acid compd.);A 15%
B 45%
C n/a
173788-87-9

2-phenoxy-4-methyl-1,3,2-dioxaborinane

98-88-4

benzoyl chloride

A

7647-01-0

hydrogenchloride

B

93-99-2

benzoic acid phenyl ester

C

11113-50-1

boric acid

Conditions
ConditionsYield
In benzene byproducts: 1,3-butanediol; acylchlorid dropwise addn. to soln. of B-compd., boiling (40 min), 1 d at room temperature, aq. HCl addn.;A n/a
B 43%
C n/a
75-18-3

dimethylsulfide

1179328-70-1

[closo-1-CB9H9-1-N2]

A

201339-68-6

(CH3)2SCB9H9

B

11113-50-1

boric acid

Conditions
ConditionsYield
A 40%
B n/a

[(Pt(Ph)(1,5-cyclooctadiene))2(μ-OH)](BF4)

182482-25-3

2,4,6-trifluorophenylboronic acid

899439-56-6

Pt(C6H2F3-2,4,6)(Ph)(1,5-cyclooctadiene)

94352-68-8

Pt(C6H2F3-2,4,6)2(cod)

C

11113-50-1

boric acid

Conditions
ConditionsYield
In toluene room temp., 1 h;A 36%
B 1%
C n/a
396695-64-0

closo-1,12-bis(sulfinic acid)-1,12-dicarbadodecaborane(12)

7722-84-1

dihydrogen peroxide

A

396695-66-2

closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1-sulfonic acid-1,12-dicarbadodecaborane(12)

B

closo-2,3,4,5,6,7,8,9,10,11-decahydroxy-1,12-bis(sulfonicacid)-1,12-dicarbadodecaborane(12) hexahydrate

C

11113-50-1

boric acid

Conditions
ConditionsYield
In water excess of aq. 30% H2O2 added to B compd.; refluxed for 5 h; monitored by(11)B NMR spectra; concd. HBr added; stirred for 2 h at room temp.; kep t at 80°C for 8 h; Br2 removed by N2 steam; volatiles removed in vac.; triturated in MeOH; centrifuged; supernatant sepd.; repeated 5 times; residue dissolved in water; filtered; dried (mono-sulfonic acid compd.); MeOH washings evapd. slowly (bis-sulfonic acid compd.);A 25%
B 35%
C n/a
79193-50-3

2-(1-adamantyl)-1,3,2-dioxaborinane

11113-50-1

boric acid

Conditions
ConditionsYield
With water In neat (no solvent) (N2), boiled with reflux condenser for 30 min; extd. (ether);29%
With hydrogenchloride; water In diethyl ether Kinetics; byproducts: adamantane, adamantanol; (N2), C10H15B02C3H6 hydrolysed by 5% HCl (stirred at 20°C for several days); GLC;
With water In diethyl ether Kinetics; byproducts: adamantane, adamantanol; (N2), soln. of C10H15B02C3H6 added to water and stirred at 20°C for several days; aq. layer removed, washed (ether); GLC;
84633-96-5

bis-9-M-carboranylbromonium borofluoride

11113-50-1

boric acid

Conditions
ConditionsYield
With water soln. of bis(9-m-carboranyl)bromonium borofluoride in water boiled for 4h; diluted with acetone, extn. with CH2Cl2, distn. in vac., addn. of etherpptn. of unreacted carborane, evapn. of aq. ext. left boric acid;25%

rubidium chloride

11113-50-1

boric acid

rubidium pentaborate

Conditions
ConditionsYield
With steam In neat (no solvent) heating of a mixt. of RbCl and boric acid in a stream of water-vapour at 100-150°C;;100%
With steam In neat (no solvent) heating of a mixt. of RbCl and boric acid in a stream of water-vapour at 100-150°C;;100%
With water byproducts: HCl; 100-150°C with steam;
With H2O byproducts: HCl; 100-150°C with steam;
71-23-8

propan-1-ol

69-65-8

mannitol

11113-50-1

boric acid

1,2,3,4,5,6-hexakis-O-dipropoxyboryl-D-mannitol

Conditions
ConditionsYield
In toluene boiling a mixt. of D-mannitol, H3BO3, and n-propanol in toluene on a Dean-Stark apparatus (azeotropic removal of H2O);; removal of toluene and propanol; elem. anal.;;100%
90-01-7

salicylic alcohol

11113-50-1

boric acid

791-31-1

triphenylhydroxysilane

82172-56-3

2-triphenylsiloxy-4H-1,3,2-benzodioxaborin

Conditions
ConditionsYield
In benzene byproducts: H2O; azeotropic removal of water; elem. anal.;100%
11113-50-1

boric acid

120-80-9

benzene-1,2-diol

791-31-1

triphenylhydroxysilane

82172-55-2

2-triphenylsiloxy-1,3,2-benzodioxaborole

Conditions
ConditionsYield
In benzene byproducts: H2O; azeotropic removal of water; elem. anal.;100%
11113-50-1

boric acid

107-21-1

ethylene glycol

791-31-1

triphenylhydroxysilane

82172-50-7

2-triphenylsiloxy-1,3,2-dioxaborolane

Conditions
ConditionsYield
In benzene byproducts: H2O; azeotropic removal of water; distd. in vac., elem. anal.;100%
739319-89-2

cadmium(II) carbonate

cadmium(II) fluoride

11113-50-1

boric acid

cadmium fluoroborate

Conditions
ConditionsYield
With lead(II) fluoride In neat (no solvent, solid phase) at 450 - 800℃; for 48h;100%
11113-50-1

boric acid

120-80-9

benzene-1,2-diol

37737-62-5

tris(catecholato)diboron

Conditions
ConditionsYield
In toluene Dean-Stark; Reflux;100%

antimony pentoxide

11113-50-1

boric acid

497-19-8

sodium carbonate

Na2SbB3O8

Conditions
ConditionsYield
at 750℃; for 72h;100%

antimony pentoxide

11113-50-1

boric acid

584-08-7

potassium carbonate

K2SbB3O8

Conditions
ConditionsYield
at 750℃; for 72h;100%

rubidium carbonate

antimony pentoxide

11113-50-1

boric acid

Rb2SbB3O8

Conditions
ConditionsYield
at 750℃; for 72h;100%

ytterbium(III) oxide

739319-89-2

cadmium(II) carbonate

11113-50-1

boric acid

3BO3(3-)*4Cd(2+)*Yb(3+)*O(2-)

Conditions
ConditionsYield
at 950℃; for 120h;100%
86119-84-8, 7664-38-2

phosphoric acid

11113-50-1

boric acid

magnesium oxide

luneburgite

Conditions
ConditionsYield
for 0.166667h; Heating;100%
107641-99-6

2,5-Bis(2-hydroxypropylthio)-1,3,4-thiadiazole

10213-78-2

N,N-diethanolstearylamine

11113-50-1

boric acid

C52H102B2N4O6S3

Conditions
ConditionsYield
for 8h;100%

C60H48N4O6

11113-50-1

boric acid

C60H42B2N4O6

Conditions
ConditionsYield
In chloroform for 66h; Reflux;100%

fuming sulphuric acid

11113-50-1

boric acid

lead dioxide

lead(II) borosulfate

Conditions
ConditionsYield
at 119.84℃; for 24h; Sealed tube;100%
106-31-0

butanoic acid anhydride

C14H11F2NO4

11113-50-1

boric acid

C21H22BF2NO8

Conditions
ConditionsYield
Stage #1: butanoic acid anhydride; boric acid at 90 - 120℃; for 3h; Inert atmosphere;
Stage #2: C14H11F2NO4 at 115℃; for 2h;
100%

rubidium carbonate

neodymium(III) oxide

11113-50-1

boric acid

germanium dioxide

RbNdGe2O6

Conditions
ConditionsYield
Stage #1: rubidium carbonate; neodymium(III) oxide; boric acid; germanium dioxide at 1050℃; for 48h;
Stage #2: at 950℃;
100%

ammonium sulfate

7664-93-9

sulfuric acid

7446-11-9

sulfur trioxide

11113-50-1

boric acid

3H3N*3H(1+)*B(SO4)3(3-)

Conditions
ConditionsYield
at 300℃; for 3h;100%
1633-05-2

strontium(II) carbonate

7664-93-9

sulfuric acid

7446-11-9

sulfur trioxide

11113-50-1

boric acid

Sr(2+)*2{B(SO4)2}(1-)=Sr{B(SO4)2}2

Conditions
ConditionsYield
at 180℃; for 24h;100%
11113-50-1

boric acid

55478-53-0

pyroglutamoyl chloride

Li(1+)*C10H10BN2O6(1-)

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 10℃; under 750.075 Torr; for 12h; Flow reactor;99.1%
488-86-8

croconic acid

11113-50-1

boric acid

213967-57-8

1,4-Dioxane-2,3,5,6-tetrone

Li(1+)*C7BO9(1-)

Conditions
ConditionsYield
In water at 20℃; under 0 Torr; for 8h; Flow reactor;99.1%
11113-50-1

boric acid

56-35-9

bis(tri-n-butyltin)oxide

57754-92-4

(C4H9)3SnOB(OH)2

Conditions
ConditionsYield
byproducts: H2O; B(OH)3 excess; 160°C;99%
byproducts: H2O; B(OH)3 excess; 160°C;99%
11113-50-1

boric acid

vanadia

107-15-3

ethylenediamine

4H3NC2H4NH3(2+)*V6B20O50H8(8-)*5H2O=(H3NC2H4NH3)4V6B20O50H8*5H2O

Conditions
ConditionsYield
In melt heating at 180°C for 3 days;99%
7664-41-7

ammonia

11113-50-1

boric acid

10043-11-5

boron nitride

Conditions
ConditionsYield
With multi-walled carbon nanotubes In solid byproducts: CO, H2, H2O; mixt. of multi-walled carbon nanotubes and H3BO3 taken in quartz tube, NH3 gas passed through with 10 sccm flow rate at 200 °C 2 h, temp.slowly raised to 1000 °C for 3 h;99%
With pyrographite; iron In neat (no solvent) byproducts: CO, H2, H2O; mixt. of activated carbon, H3BO3 and ferric nitrate (mole ratio of 3:1:0.1) taken in quartz tube, dried in oven at 60 °C 6 h, NH3 gas passed through with 10 sccm flow rate, heating at 1300 °C for 4 h;
byproducts: H2O; synthesis of BN coating on the surfaces of carbon nanotubes and nanofibers around 1150°C using infiltration of nanotubes with boric acid and nitridation in ammonia;
11113-50-1

boric acid

92-44-4

2,3-naphthalenediol

1071759-34-6

cinchonidine

cinchonidinium (bis-2,3-naphthalenediyl)orthoborate salt

Conditions
ConditionsYield
In acetone mixt. of alkaloid, boric acid and 2,3-dihydroxynaphthalene (molar ratio 1:1:2) dissolved in hot acetone, warmed; evapd., noncryst. solid product;99%

tri(ethylenediamine) cobalt(III) chloride dihydrate

86119-84-8, 7664-38-2

phosphoric acid

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boric acid

boron trifluoride monoethylamine

C2H10N2(2+)*CoB2P3O12(OH)(2-) = [C2H10N2][CoB2P3O12(OH)]

Conditions
ConditionsYield
In water hydrothermal synthesis (180°C, 5 d); elem. anal.;99%
636-61-3

D-Malic acid

11113-50-1

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1310-73-2

sodium hydroxide

sodium (S,S,S)-dimalatoborate

Conditions
ConditionsYield
In water malic acid dissolved in H2O, treated with boric acid, aq. NaOH added, stirred in open flask at 100 °C for ca. 4 h; mixt. evapd.; detd. by NMR, XRD;99%
11113-50-1

boric acid

6-methyl-5-hepten-3-yn-1-ol

tris(6-methyl-5-hepten-3-yn-1-oxy)borane

Conditions
ConditionsYield
In toluene byproducts: H2O; (N2); stirring of mixt. of boric acid and 6-methyl-5-hepten-3-yn-1-ol intoluene under reflux for 12 h with removal of water by a Dean-Stark tra p; evapn. of solvent by distn. (180-230°C/0.5 mmHg);99%
1073-72-9

4-hydroxythioanisole

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24676-71-9

sodium 4-methylthio-phenolate

sodium tetrakis(4-methylthiophenoxy)borate

Conditions
ConditionsYield
In toluene phenol (excess) and acid heated for 2 h (Dean-Stark trape), volatiles removed (vac.), dissolved (THF), added dropwise to a soln. of Na compd. (THF), stirred for 1-12 h; ppt. filtered, washed (diethyl ether, pentane), dried (high vac.); elem.anal.;99%
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  • Casno:

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  • Boric acid

  • Casno:

    11113-50-1

    Boric acid

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Specification

The Boric acid, with the CAS registry number 11113-50-1, is also known as UNII-R57ZHV85D4 .It belongs to the product categories of UVCBs-inorganic.Its EINECS number is 234-343-4.This chemical's molecular formula is H3BO3 and molecular weight is 61.83. What's more,Its systematic name is Boric acid.

The Boric acid has many various application, such as in personal care products, food additives, biological insecticides & antiputrefactiva. Except these, it is also used in the glass, ceramics, rubber, fertilisers, flame retardants, paints, industrial fluids, brake fluids, soldering products, film developers and so on.And it is among one kind of 8 Substances of Very High Concern which is issued by the ECHA, as this chemical could cause very serious danger to people's health, including being carcinogenic, inducing the organism's mutation, damage to genital system and so on.

Physical properties about Boric acid are:(1)ACD/LogP: -0.61; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -0.61; (4)ACD/LogD (pH 7.4): -0.62; (5)ACD/BCF (pH 5.5): 1.00; (6)ACD/BCF (pH 7.4): 1.00; (7)#H bond acceptors: 3; (8)#H bond donors: 3; (9)#Freely Rotating Bonds: 3; (10)Index of Refraction: 1.385; (11)Molar Refractivity: 10.083 cm3; (12)Molar Volume: 43.003 cm3; (13)Surface Tension: 59.1980018615723 dyne/cm; (14)Density: 1.438 g/cm3.

You can still convert the following datas into molecular structure:
(1)SMILES:B(O)(O)O;
(2)Std. InChI:InChI=1S/BH3O3/c2-1(3)4/h2-4H;
(3)Std. InChIKey:KGBXLFKZBHKPEV-UHFFFAOYSA-N.