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111982-45-7

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Basic Information
CAS No.: 111982-45-7
Name: 2-FLUOROPHENYL CYCLOPENTYL KETONE
Article Data: 3
Molecular Structure:
Molecular Structure of 111982-45-7 (2-FLUOROPHENYL CYCLOPENTYL KETONE)
Formula: C12H13FO
Molecular Weight: 192.233
Synonyms: cyclopentyl-(2-fluoro-phenyl)-methanone;2-FLUOROPHENYL CYCLOPENTYL KETONE;Methanone,cyclopentyl(2-fluorophenyl);
Density: 1.131g/cm3
Boiling Point: 275.8oC at 760 mmHg
Flash Point: 110.9oC
PSA: 17.07000
LogP: 3.19860
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Synthetic route
137-43-9

Cyclopentyl bromide

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111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

Conditions
ConditionsYield
Stage #1: Cyclopentyl bromide With iodine; magnesium In tetrahydrofuran at 20℃; Reflux;
Stage #2: 2-fluorobenzonitrile With copper(I) bromide dimethylsulfide complex In tetrahydrofuran for 4h; Inert atmosphere; Reflux;
Stage #3: With sulfuric acid; water In tetrahydrofuran for 4h; Reagent/catalyst; Solvent; Time;		90%
394-47-8

2-fluorobenzonitrile

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cyclopentylmagnesium bromide

111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

Conditions
ConditionsYield
Stage #1: 2-fluorobenzonitrile; cyclopentylmagnesium bromide With copper(I) bromide In tetrahydrofuran at 60℃; for 15h;
Stage #2: With sulfuric acid; water In tetrahydrofuran at 0℃; for 15h;		40%
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

1616657-67-0

α-bromocyclopentyl-(2-fluorophenyl)ketone

Conditions
ConditionsYield
Stage #1: cyclopentyl-(2-fluorophenyl)ketone With hydrogen bromide In water at 20℃; for 0.0833333h; Darkness;
Stage #2: With lithium chloride In water at 20℃; for 0.0166667h; Darkness;
Stage #3: With dihydrogen peroxide In water at 70℃; for 1.5h; Darkness;		96%
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

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3-cyclopentyl-1H-indazole

Conditions
ConditionsYield
With hydrazine In water at 130℃; for 72h;89%
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

1372151-92-2

C14H16OS

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C
1.2: 18 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 °C
View Scheme
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

C14H15BrS

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C
1.2: 18 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 °C
3.1: phosphorus tribromide / diethyl ether / 1 h / 20 °C
View Scheme
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

C18H25O3PS

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C
1.2: 18 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 °C
3.1: phosphorus tribromide / diethyl ether / 1 h / 20 °C
4.1: toluene / 18 h / Reflux
View Scheme
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

C25H29F2O3PS

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C
1.2: 18 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 5 °C
3.1: phosphorus tribromide / diethyl ether / 1 h / 20 °C
4.1: toluene / 18 h / Reflux
5.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -70 °C
5.2: 0.5 h / -70 - 20 °C
View Scheme
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

623-51-8

ethyl 2-sulfanylacetate

1372151-88-6

C16H18O2S

Conditions
ConditionsYield
Stage #1: ethyl 2-sulfanylacetate With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: cyclopentyl-(2-fluorophenyl)ketone In N,N-dimethyl-formamide for 18h; Reflux;
111982-45-7

cyclopentyl-(2-fluorophenyl)ketone

A

111982-48-0

α-hydroxycyclopentyl-(2-flourophenyl)-N-methylamine

B

1616657-68-1

(2-fluorophenyl)(1-hydroxycyclopentyl)methanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: hydrogen bromide / water / 0.08 h / 20 °C / Darkness
1.2: 0.02 h / 20 °C / Darkness
1.3: 1.5 h / 70 °C / Darkness
2.1: 6 h / -40 °C
View Scheme
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    yierdechem is a young and potential team, with about ten years experiences in the field of pharmaceutical intermediate and fine chemicals, yierdechem has established solid business

  • Hangzhou Yierdechem Co. Ltd

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-571-86904883

    Address:903,zhijiang Minglou, Xiasha EDA, Hangzhou City 310018,P.R.China

       Inquiry Now

  • 2-FLUOROPHENYL CYCLOPENTYL KETONE CAS 111982-45-7

  • Casno:

    111982-45-7

    2-FLUOROPHENYL CYCLOPENTYL KETONE CAS 111982-45-7

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    high quality, in stock,fast and safe deliveryAppearance:White crystalline powder Package:1kg/bag,25kg/drum Application:Pharmaceutical Intermediates Transportation:Air/Sea/Land Port:Shanghai/Qingdao

    Our company is a high-tech modern chemical enterprise with research & development, production and sales. Based on the best quality and pretty competitive price, our products are so

  • Shanghai Zhenrui Biotechnology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-13166310959 15032669666

    Address:Shijiazhuang City

       Inquiry Now

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