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112713-92-5

Basic Information
CAS No.: 112713-92-5
Name: 1-Cyclopentene-1-heptanoic acid, 5-oxo-3-[(triethylsilyl)oxy]-, Methyl ester
Molecular Structure:
Molecular Structure of 112713-92-5 (1-Cyclopentene-1-heptanoic acid, 5-oxo-3-[(triethylsilyl)oxy]-, Methyl ester)
Formula: C19H34O4Si
Molecular Weight: 354.562
Synonyms: Methyl 7-(5-oxo-3-((triethylsilyl)oxy)cyclopent-1-en-1-yl)heptanoate;Methyl 5-oxo-3-<(triethylsilyl)oxy>-1-cyclopenteneheptanoate;methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate;(+-)-methyl 7-[(3-triethylsilyloxy) 5-oxocyclopenten 1-yl]heptanoate;methyl 5-oxo-3-[(triethylsilyl)oxy]-1-cyclopentene-1-heptanoate;
Density: 0.99±0.1 g/cm3(Predicted)
Boiling Point: 413.2±45.0 °C(Predicted)
PSA: 52.60000
LogP: 4.78960
Synthetic route
112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

(n-Bu)3CH=CHCH2C(Me)(OSiMe3)C4H9 (3)

(n-Bu)3CH=CHCH2C(Me)(OSiMe3)C4H9 (3)

59122-46-2

misoprostol

Conditions
ConditionsYield
With (lithium)2(CN)(methyl)2cuprate In tetrahydrofuran; water; acetic acid91%
112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

5-fluoro-1-(tributylstannyl)-4-(triethylsilyloxy)-4-methyl-1-octene

5-fluoro-1-(tributylstannyl)-4-(triethylsilyloxy)-4-methyl-1-octene

112713-97-0

7-[(1R,2R,3R)-2-((E)-5-Fluoro-4-methyl-4-trimethylsilanyloxy-oct-1-enyl)-5-oxo-3-trimethylsilanyloxy-cyclopentyl]-heptanoic acid methyl ester

Conditions
ConditionsYield
With (lithium)2(CN)(methyl)2cuprate In tetrahydrofuran68%
112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

1-propyl-1-<5-(tributylstannyl)-2-(triethylsilyloxy)-(E)-4-penten-2-yl>cyclobutane

1-propyl-1-<5-(tributylstannyl)-2-(triethylsilyloxy)-(E)-4-penten-2-yl>cyclobutane

112713-98-1

7-{(1R,2R,3R)-5-Oxo-2-[(E)-4-(1-propyl-cyclopropyl)-4-trimethylsilanyloxy-pent-1-enyl]-3-trimethylsilanyloxy-cyclopentyl}-heptanoic acid methyl ester

Conditions
ConditionsYield
With (lithium)2(CN)(methyl)2cuprate In tetrahydrofuran63%
66792-28-7

4-methyl-4-trimethylsilyloxyl-1-octyne

75-24-1

trimethylaluminum

112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

136424-56-1

7-[(1R,2R,3R)-2-((E)-2,4-Dimethyl-4-trimethylsilanyloxy-oct-1-enyl)-5-oxo-3-triethylsilanyloxy-cyclopentyl]-heptanoic acid methyl ester

Conditions
ConditionsYield
With zirconocene dichloride 1) CH2Cl2, 0 deg C to r.t. 2) THF, Et2O, 0 deg C; Yield given. Multistep reaction;
66792-28-7

4-methyl-4-trimethylsilyloxyl-1-octyne

112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

84024-39-5, 138456-65-2

7-[(1R,2R,3R)-2-((E)-4-Methyl-4-trimethylsilanyloxy-oct-1-enyl)-5-oxo-3-triethylsilanyloxy-cyclopentyl]-heptanoic acid methyl ester

Conditions
ConditionsYield
Yield given. Multistep reaction;
62555-05-9

(1E)-(4R)-4-trimethylsilyloxy-4-methyl-1-iodo-1octene

112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

84024-39-5, 138456-65-2

7-[(1R,2R,3R)-2-((E)-4-Methyl-4-trimethylsilanyloxy-oct-1-enyl)-5-oxo-3-triethylsilanyloxy-cyclopentyl]-heptanoic acid methyl ester

Conditions
ConditionsYield
With n-butyllithium; methyllithium 1.) THF, -78 deg C, 1 h, 2.) -78 deg C; Yield given. Multistep reaction;

(1-Ethynyl-pentyloxy)-trimethyl-silane

112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

128217-25-4

7-[(1R,2R,3R)-5-Oxo-3-triethylsilanyloxy-2-((E)-3-trimethylsilanyloxy-hept-1-enyl)-cyclopentyl]-heptanoic acid methyl ester

Conditions
ConditionsYield
Yield given. Multistep reaction;

(1,1-Dimethyl-butyl)-(1-ethynyl-pentyloxy)-dimethyl-silane

112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

128217-26-5

7-((1R,2R,3R)-2-{(E)-3-[(1,1-Dimethyl-butyl)-dimethyl-silanyloxy]-3-methyl-oct-1-enyl}-5-oxo-3-triethylsilanyloxy-cyclopentyl)-heptanoic acid methyl ester

Conditions
ConditionsYield
Yield given. Multistep reaction;
75-77-4

chloro-trimethyl-silane

5674-01-1

2-methylallylmagnesium chloride

112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

7-[(4R,5R)-5-(2-Methyl-allyl)-4-triethylsilanyloxy-2-trimethylsilanyloxy-cyclopent-1-enyl]-heptanoic acid methyl ester

Conditions
ConditionsYield
With copper(I) bromide dimethylsulfide complex; lithium chloride In tetrahydrofuran at -78℃; for 0.25h;
89487-33-2

prenylmagnesium bromide

112713-92-5

methyl 7-(5-oxo-3-[(triethylsilyl)-oxy]-1-cyclopenten-1-yl)-heptanoate

A

7-[2-(1,1-Dimethyl-allyl)-3-hydroxy-5-oxo-cyclopentyl]-heptanoic acid methyl ester

B

3-Hydroxy-2-(2-methyl-2-buten-4-yl)-5-oxo-1-cyclopenteneheptanoate

Conditions
ConditionsYield
With chloro-trimethyl-silane; copper(I) bromide dimethylsulfide complex; tetrabutyl ammonium fluoride; lithium chloride 1.) THF, -78 deg C, 5 min, 2. ) THF, 10 min; Yield given. Multistep reaction. Yields of byproduct given;
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    Product Name: 1-Cyclopentene-1-heptanoic acid, 5-oxo-3-[(triethylsilyl)oxy]-, Methyl ester Synonyms: 1-Cyclopentene-1-heptanoic acid, 5-oxo-3-[(triethylsilyl)oxy]-, Methyl ester;Methyl 7-(5-oxo-3-((triethylsilyl)oxy)-cyclopent-1-en-1-y

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    112713-92-5 CAS NO.112713-92-5

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