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121-97-1

Basic Information
CAS No.: 121-97-1
Name: Methoxypropiophenone
Article Data: 223
Molecular Structure:
Molecular Structure of 121-97-1 (Methoxypropiophenone)
Formula: C10H12O2
Molecular Weight: 164.204
Synonyms: p-Methoxypropiophenone;4-Methoxypropiophenone;Propiophenone,4'-methoxy- (6CI,7CI,8CI);Propiophenone, p-methoxy- (4CI);1-(4-Methoxyphenyl)-1-propanone;1-Methoxy-4-propanoylbenzene;4-Propanoylanisole;4'-Methoxypropiophenone;Ethyl 4-methoxyphenyl ketone;Ethyl p-methoxyphenyl ketone;NSC 11834;
EINECS: 204-512-7
Density: 1.071 g/cm3
Melting Point: 27-29 °C(lit.)
Boiling Point: 272.316 °C at 760 mmHg
Flash Point: 118.806 °C
Appearance: Clear colourless to amber liquid
Hazard Symbols: IrritantXi
Safety: 24/25
Transport Information: UN 1993
PSA: 26.30000
LogP: 2.28790
Synthetic route
79-03-8

propionyl chloride

100-66-3

methoxybenzene

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With Noccaea caerulescens extract supported in montmorillonite K10 at 60℃; for 6h; Friedel Crafts acylation; Inert atmosphere; regioselective reaction;100%
With aluminum (III) chloride In dichloromethane at 5 - 20℃; for 2.5h;98%
With benzyltributylammonium tetrachloroferrate at 50℃; for 0.1h; Friedel-Crafts reaction;93%
100-66-3

methoxybenzene

123-62-6

propionic acid anhydride

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With lithium perchlorate at 60℃; for 1h;99%
Stage #1: methoxybenzene; propionic acid anhydride With modified ZSM-5 zeolite at 100℃; for 5h;
Stage #2: at 500℃; for 2h; Temperature; Calcination;
97.6%
With hafnium(IV) trifluoromethanesulfonate; lithium perchlorate In nitromethane for 6h; Ambient temperature;93%
51410-44-7

1-(4-methoxylphenyl)-2-propen-1-ol

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate; potassium carbonate In acetonitrile for 1h; Inert atmosphere; Reflux;99%
With [Ru(η(3):η(3)-C10H16)Cl(O2CCH3)] In aq. phosphate buffer at 50℃; for 1h; pH=7; Sealed tube; Inert atmosphere;99%
With Fe(II)(bis(2-(diisopropylphosphino)ethyl)amine)(CO)(H)(Cl); potassium tert-butylate In toluene at 80℃; for 1h; Inert atmosphere;98%
97-94-9

triethyl borane

4-methoxy-N-phenyl-N-tosylbenzamide

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium carbonate In tetrahydrofuran; tert-butyl methyl ether at 20℃; for 24h; Inert atmosphere; Schlenk technique;99%
75-57-0

tetramethlyammonium chloride

70-70-2

4-hydroxypropiophenone

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With potassium carbonate In 1,2-dimethoxyethane at 145℃; for 0.416667h; Microwave irradiation; Inert atmosphere; Sealed vessel;98%
With potassium carbonate at 150 - 160℃; for 4h;81%
92409-14-8

C17H20O4

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With 5%-palladium/activated carbon; ammonium formate In ethanol; water at 80℃; for 1h;98%
5349-60-0

1-(4-methoxyphenyl)-1-propanol

A

623-12-1

4-chloromethoxybenzene

B

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With dichloromethane extract derived from 6percent aqueous hypochlorite/tetra-n-butylammonium bisulfate solution with pH value to 8-9 In dichloromethane at 20℃;A 92%
B 6%
77-78-1

dimethyl sulfate

70-70-2

4-hydroxypropiophenone

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 20.5h; Heating / reflux;89%
With sodium hydroxide
With hydroxide
94607-41-7

(E)-1-(4-methoxyphenyl)-3-chloropropene

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With potassium carbonate; phenylboronic acid; [Ru(cyclopentadienyl)(MeCN)3]PF6 In acetonitrile at 20℃; for 16h;89%
With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; potassium carbonate; phenylboronic acid In acetonitrile at 20℃; for 24h; Inert atmosphere; regioselective reaction;89%
52898-49-4

4,N-dimethoxy-N-methylbenzamide

925-90-6

ethylmagnesium bromide

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 5℃; for 1h; Weinreb Ketone Synthesis; Inert atmosphere;89%
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    Product Name: Methoxypropiophenone CAS: 121-97-1 MF: C10H12O2 MW: 164.2 EINECS: 204-512-7 Mol File: 121-97-1.mol Methoxypropiophenone Structure Methoxypropiophenone Chemical Properties Melting point 27-29 °C(lit.) Boiling

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Chemistry

IUPAC Name: 1-(4-Methoxyphenyl)propan-1-one
Systematic of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): 4'-Methoxypropiophenone ; AI3-04094 ; EINECS 204-512-7 ; Ethyl 4-methoxyphenyl ketone ; NSC 11834 ; p-Methoxypropiophenone ; Propiophenone, 4'-methoxy- (8CI)
CAS NO: 121-97-1
Molecular Formula of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): C10H12O2
Molecular Weight: 164.2011
Molecular Structure:

Melting Point: 27-29 °C 
H bond acceptors: 2
Freely Rotating Bonds: 3
Polar Surface Area: 26.3 Å2
Index of Refraction: 1.501
Molar Refractivity: 47.59 cm3
Molar Volume: 161.4 cm3
Surface Tension: 33.6 dyne/cm
Density of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): 1.016 g/cm3
Flash Point: 118.8 °C
Enthalpy of Vaporization: 51.06 kJ/mol
Boiling Point: 272.3 °C at 760 mmHg
Vapour Pressure: 0.00612 mmHg at 25°C

Safety Profile

Hazard Codes: IrritantXi
Safety Statements: 24/25 
S24/25: Avoid contact with skin and eyes.
RIDADR: 1993
WGK Germany: 3
Hazard Note: Irritant