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Basic Information
CAS No.: 1228779-96-1
Name: 3-nitro-4-((tetrahydro-2H-pyran-4-yl)MethylaMino)benzenesulfonaMide
Article Data: 21
Molecular Structure:
Molecular Structure of 1228779-96-1 (3-nitro-4-((tetrahydro-2H-pyran-4-yl)MethylaMino)benzenesulfonaMide)
Formula: N/A
Molecular Weight: 315.35
Synonyms: 3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide
Density: 1.412±0.06 g/cm3(Predicted)
Melting Point: 188 - 191°C
Boiling Point: 542.0±60.0 °C(Predicted)
Related products
Synthetic route
130290-79-8

4-tetrahydropyranmethylamine

406233-31-6

4-fluoro-3-nitrobenzenesulfonamide

1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 5h;97%
With triethylamine In tetrahydrofuran at 0 - 20℃; for 16h;95%
With sodium carbonate In isopropyl alcohol at 55 - 65℃; for 4h;94%
130290-79-8

4-tetrahydropyranmethylamine

97-09-6

4-Chloro-3-nitrobenzenesulfonamide

1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃; for 12h;91%
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃; for 24h; Inert atmosphere; Large scale;88%
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃;78%
4295-99-2

tetrahydro-2H-pyran-4-carbonitrile

1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogen; ammonia / methanol / 12 h / 40 - 45 °C / 3000.3 - 3750.38 Torr
2: N-ethyl-N,N-diisopropylamine / acetonitrile / 25 h / 55 - 70 °C
View Scheme
88-73-3

2-Chloronitrobenzene

1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: chlorosulfonic acid / 18 h / 20 - 100 °C
1.2: 5 h / -10 - 23 °C
2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 25 h / 55 - 70 °C
View Scheme
362703-30-8

methyl 4-cyanotetrahydro-2H-pyran-4-carboxylate

1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium hydroxide; water / N,N-dimethyl-formamide / 7 h / pH 9 - 11
2: copper(I) oxide / toluene / 7 h / 107 °C
3: hydrogen; ammonia / methanol / 12 h / 40 - 45 °C / 3000.3 - 3750.38 Torr
4: N-ethyl-N,N-diisopropylamine / acetonitrile / 25 h / 55 - 70 °C
View Scheme

4-cyanotetrahydro-2H-pyran-4-carboxylic acid

1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: copper(I) oxide / toluene / 7 h / 107 °C
2: hydrogen; ammonia / methanol / 12 h / 40 - 45 °C / 3000.3 - 3750.38 Torr
3: N-ethyl-N,N-diisopropylamine / acetonitrile / 25 h / 55 - 70 °C
View Scheme
1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

2-((1H-pyrrolo[2,3-b]pyridin-5-yl)oxy)-4-bromobenzoic acid

2-((1H-pyrrolo[2,3-b]pyridin-5-yl)oxy)-4-bromo-N-((3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)phenyl)sulfonyl)benzamide

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 15h; Inert atmosphere;100%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 48h;61.3%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 24h;80 mg
1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

2-bromo-4-(4-((2-(4-chlorophenyl)-4,4-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoic acid

2-bromo-4-(4-((2-(4-chlorophenyl)-4,4-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)-N-(3-nitro-4-((tetrahydro-2H-pyran-4-yl)methylamino)phenylsulfonyl)benzamide

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 25℃;93%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 25℃;93%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 25℃;93%
1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

1235865-77-6

[2-((1H-pyrrolo [2,3-b]pyridin-5-yl)oxy)-4-(4-((4’-chloro-5,5-dimethyl-3,4,5,6-tetrahydro-[1,1’-biphenyl]-2-yl)methyl)piperazin-1-yl)benzoic acid]

1257044-40-8

2-((1H-pyrrolo[2,3-b]pyridin-5-yl)oxy)-4-(4-((4'-chloro-5,5-dimethyl-3,4,5,6-tetrahydro-[1,1-biphenyl]-2-yl)methyl)piperazin-1-yl)-N-((3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)phenyl)sulfonyl)benzamide

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 3h; Reagent/catalyst; Temperature;91.4%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 25℃; for 12h; Inert atmosphere; Large scale;86%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 25℃;84%
1228779-96-1

3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide

C40H40ClN5O7S

C51H53ClN8O11S2

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 30 - 35℃;89%
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    Product name: 3-Nitro-4-(((Tetrahydro-1H-Pyran-4-yl)methyl)amino)benzenesulfonamide CAS No.：1228779-96-1 Molecule Formula：C12H17N3O5S Molecule Weight：315.35 Purity: 99.0% Package: 25kg/drum Description：White powder Manufacture Standar

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    Name: 3-nitro-4-(((tetrahydro-2H-pyran-4-yl)methyl)amino)benzenesulfonamide CAS No.: 1228779-96-1 Other name: THP-sulfonamide;3-nitro-4-[(oxan-4-ylmethyl)amino]benzene-1-sulfonamide;abt-1－199;3-Nitro-4-[[(tetrahydropyran-4-yl)methyl]amino]benzenes

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    In stock Storage:200kg Package:1kg/Box, 25kg/Drum Application:Pharmaceutical and Cosmetic Transportation:By Sea/Air/Courier Port:Any port of China

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    1228779-96-1

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    good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg，customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

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    Business Type:Lab/Research institutions

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    Address:Room 02-31, 13 / F, Building 9, Guannan Fuxing Medical Park Phase II, No.58, Guanggu Avenue, East Lake New Technology Development Zone, Wuhan, Hubei, China (Wuhan Area, Free Trade Zone)

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  • 1228779-96-1 CAS No.1228779-96-1

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    1228779-96-1

    1228779-96-1 CAS No.1228779-96-1

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    Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

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