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13139-86-1

Basic Information
CAS No.: 13139-86-1
Name: 4-Methoxyphenylmagnesium bromide
Article Data: 38
Molecular Structure:
Molecular Structure of 13139-86-1 (4-Methoxyphenylmagnesium bromide)
Formula: C7H7BrMgO
Molecular Weight: 211.341
Synonyms: Magnesium,bromo(p-methoxyphenyl)- (7CI,8CI);p-Methoxyphenylmagnesium bromide (6CI);(4-Methoxyphenyl)magnesium bromide;(p-Anisyl)bromomagnesium;4-Anisylmagnesiumbromide;Bromo(4-methoxyphenyl)magnesium;Bromo(p-methoxyphenyl)magnesium;p-Anisylmagnesium bromide;
Density: 0.955 g/mL at 25 °C
Boiling Point: 65-67 °C
Flash Point: -4 °F
Solubility: Severe reaction
Appearance: Clear to brown solution when properly stored
Hazard Symbols: FlammableF,CorrosiveC
Risk Codes: 11-14/15-19-34
Safety: 16-26-36/37/39-43B-43-45-6A
Transport Information: UN 2924 3/PG 2
PSA: 9.23000
LogP: 2.34100
Synthetic route
104-92-7

1-bromo-4-methoxy-benzene

13139-86-1

4-methoxyphenyl magnesium bromide

Conditions
ConditionsYield
With magnesium; bromine In diethyl ether
With magnesium; copper(l) iodide In diethyl ether at -78℃; for 0.5h; Grignard reaction; Title compound not separated from byproducts;
With magnesium In tetrahydrofuran at 80℃; for 0.333333h; microwave irradiation;
104-92-7

1-bromo-4-methoxy-benzene

173433-59-5

7-chloro-1,2,3,4,4a,9b-hexahydro-2-methyl-5H-1,3-ethanoindeno-[1,2-c]pyridin-5-one

A

173434-18-9

7-Chloro-5-(p-methoxyphenyl)-2-methyl-1,3-ethano-1,2,3,4,4a,9b-hexahydro-5H-indeno[1,2-c]pyridin-5-ol

B

13139-86-1

4-methoxyphenyl magnesium bromide

Conditions
ConditionsYield
With magnesium In tetrahydrofuran; dichloromethane
104-92-7

1-bromo-4-methoxy-benzene

66-71-7

1,10-Phenanthroline

106-93-4

ethylene dibromide

13139-86-1

4-methoxyphenyl magnesium bromide

Conditions
ConditionsYield
With iodine; magnesium In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; iso-butanol
104-92-7

1-bromo-4-methoxy-benzene

52498-02-9

3-(p-methoxyphenyl)cyclobutanone

A

52498-11-0

1,3-bis(p-methoxyphenyl)cyclobutanol

B

13139-86-1

4-methoxyphenyl magnesium bromide

Conditions
ConditionsYield
In tetrahydrofuran
104-92-7

1-bromo-4-methoxy-benzene

7439-95-4

magnesium

13139-86-1

4-methoxyphenyl magnesium bromide

Conditions
ConditionsYield
With 1,2-dibromomethane In tetrahydrofuran at 40℃; for 1.5h;
In tetrahydrofuran at 20℃; for 2h;
In tetrahydrofuran
In tetrahydrofuran Inert atmosphere;
With lithium chloride In tetrahydrofuran at 0 - 25℃; for 0.5h; Inert atmosphere; Schlenk technique;
104-92-7

1-bromo-4-methoxy-benzene

magnesium

magnesium

13139-86-1

4-methoxyphenyl magnesium bromide

Conditions
ConditionsYield
With diethyl ether; iodine
With diethyl ether; iodine; benzene
24759-97-5

2-adamantanespiroxirane

13139-86-1

4-methoxyphenyl magnesium bromide

109610-24-4

2-(p-methoxy)benzyl-2-adamantanol

Conditions
ConditionsYield
In diethyl ether for 2h; Ambient temperature;100%

Benzoic acid (2S,3S)-2-formyl-1-(4-methoxy-phenyl)-4-oxo-azetidin-3-yl ester

13139-86-1

4-methoxyphenyl magnesium bromide

Benzoic acid (2R,3S)-2-[hydroxy-(4-methoxy-phenyl)-methyl]-1-(4-methoxy-phenyl)-4-oxo-azetidin-3-yl ester

Conditions
ConditionsYield
In tetrahydrofuran at -45℃;100%
134869-78-6

(2S,3S)-3-cyano-2,3-epoxy-1-propanol TBS ether

13139-86-1

4-methoxyphenyl magnesium bromide

139058-52-9

[(2R,3S)-3-(tert-Butyl-dimethyl-silanyloxymethyl)-oxiranyl]-(4-methoxy-phenyl)-methanone

Conditions
ConditionsYield
In toluene at -30℃;100%
141334-25-0

2,2,2-trifluoro-1-triphenylsilylethanone

13139-86-1

4-methoxyphenyl magnesium bromide

1,1-difluoro-2-(4-methoxyphenyl)-2-triphenylsilyloxyethene

Conditions
ConditionsYield
In tetrahydrofuran 1) -30 deg C, 15 min, 2) rt, 1 h;100%
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Chemistry

Molecular Structure of 4-Methoxyphenylmagnesium bromide (CAS No.13139-86-1):

Molecular Formula: C7H7BrMgO
Molecular Weight: 211.3389
CAS No: 13139-86-1
H bond acceptors: 1
H bond donors: 0
Freely Rotating Bonds: 2
Polar Surface Area: 9.23 Å2
Systematic Name: Bromo(4-methoxyphenyl)magnesium
InChI: InChI=1/C7H7O.BrH.Mg/c1-8-7-5-3-2-4-6-7;;/h3-6H,1H3;1H;/q;;+1/p-1/rC7H7BrMgO/c1-10-7-4-2-6(9-8)3-5-7/h2-5H,1H3
InChIKey: JKXAZEXIOPFJSC-DZVGZYEUAY
Std. InChI: InChI=1S/C7H7O.BrH.Mg/c1-8-7-5-3-2-4-6-7;;/h3-6H,1H3;1H;/q;;+1/p-1
Std. InChIKey: JKXAZEXIOPFJSC-UHFFFAOYSA-M
Product Categories: Aryl;Grignard Reagents;Organometallic Reagents

Safety Profile

Hazard Codes: FlammableF,CorrosiveC
Risk Statements: 11-14-19-22-34-14/15
R11:Highly flammable. 
R14 :Reacts violently with water. 
R22:Harmful if swallowed. 
R34:Causes burns. 
R15:Contact with water liberates extremely flammable gases.
Safety Statements: 16-26-33-36/37/39-45-6A-43B
S16:Keep away from sources of ignition. 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S33:Take precautionary measures against static discharges. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection. 
S45:In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) 
S6:Keep under ... (there follows the name of an inert gas).
S43:In case of fire use ... (there follows the type of fire-fighting equipment to be used.)
RIDADR: UN 2924 3/PG 2
HazardClass: 4.3
PackingGroup: II

Specification

  4-Methoxyphenylmagnesium bromide (CAS No.13139-86-1), its synonyms are p-Anisylmagnesium bromide ; Bromo(4-methoxyphenyl)magnesium ; Magnesium, bromo(4-methoxyphenyl)- .