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13209-41-1

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Basic Information
CAS No.: 13209-41-1
Name: 17,21-dihydroxy-16alpha-methylpregna-1,4,9(11)-triene-3,20-dione
Article Data: 10
Molecular Structure:
Molecular Structure of 13209-41-1 (17,21-dihydroxy-16alpha-methylpregna-1,4,9(11)-triene-3,20-dione)
Formula: C22H28 O4
Molecular Weight: 356.462
Synonyms: Pregna-1,4,9(11)-triene-3,20-dione,17,21-dihydroxy-16a-methyl- (6CI,7CI,8CI); 17a,21-Dihydroxy-16a-methylpregna-1,4,9(11)-triene-3,20-dione
Density: 1.24g/cm3
Melting Point: 228-231 °C(Solv: acetone (67-64-1); hexane (110-54-3))
Boiling Point: 548.3°C at 760 mmHg
Flash Point: 299.4°C
PSA: 74.60000
LogP: 2.75290
Related products
Synthetic route

C25H36O4Si

13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

Conditions
ConditionsYield
With hydrogenchloride In pentan-1-ol80%

C25H36O2Si

13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
2: hydrogenchloride / pentan-1-ol
View Scheme
37413-91-5

2-((10S,13S,14S)-10,13-dimethyl-3-oxo-6,7,8,10,12,13,14,15-octahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxoethyl acetate

13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: dichloromethane; tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
1.2: 3 h / 20 °C / Inert atmosphere
1.3: -50 °C / Inert atmosphere
2.1: acetic acid; peracetic acid / toluene / 0.5 h / -10 °C / Inert atmosphere
3.1: potassium carbonate; water / methanol / 0 - 20 °C
View Scheme
10106-41-9

17α,21-dihydroxy-16α-methyl-1,4,9(11)-pregnatriene-3,20-dione 21-acetate

13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

Conditions
ConditionsYield
With water; potassium carbonate In methanol at 0 - 20℃;
124-63-0

methanesulfonyl chloride

13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

23776-75-2

Methanesulfonic acid 2-((8S,10S,13S,14S,16R,17R)-17-hydroxy-10,13,16-trimethyl-3-oxo-6,7,8,10,12,13,14,15,16,17-decahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxo-ethyl ester

Conditions
ConditionsYield
With pyridine at 0 - 2℃; for 1.5h;85%
50-00-0

formaldehyd

13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

14518-56-0

16α-methyl-17α,20;20,21-bismethylenedioxypregn-1,4,9(11)-triene-3-one

Conditions
ConditionsYield
With hydrogenchloride In dichloromethane Ambient temperature;74%
124-63-0

methanesulfonyl chloride

13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

A

21-chloro-17α-hydroxy-16α-methylpregna-1,4,9(11)-triene-3,20-dione

B

17α-hydroxy-17β-(4-(R)-hydroxy-2,2-dioxido-1,2-oxathiolan-4-yl)-16α-methylandrosta-1,4,9(11)-triene-3-one

Conditions
ConditionsYield
With dmap In dichloromethane for 4h; Heating;A 69%
B 1.1%
...Expand
13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

A

21-chloro-17α-hydroxy-16α-methylpregna-1,4,9(11)-triene-3,20-dione

B

17α-hydroxy-17β-(4-(R)-hydroxy-2,2-dioxido-1,2-oxathiolan-4-yl)-16α-methylandrosta-1,4,9(11)-triene-3-one

Conditions
ConditionsYield
With dmap; methanesulfonyl chloride In dichloromethane for 4h; Heating;A 69%
B 1.1%
13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

21-chloro-17α-hydroxy-16α-methylpregna-1,4,9(11)-triene-3,20-dione

Conditions
ConditionsYield
With Vilsmeier reagent; water 1.) toluene, from -3 deg C to 2 deg C, 3 h, 2.) toluene, 5 deg C; Yield given. Multistep reaction;
13209-41-1

(8S,10S,13S,14S,16R,17R)-17-hydroxy-17-(2-hydroxyacetyl)-10,13,16-trimethyl-7,8,12,14,15,16-hexahydro-6H-cyclopenta[a]phenanthren-3-one

83881-01-0

21-fluoro-17α-hydroxy-16α-methyl-1,4,9(11)-ppregnatriene-3,30-dione 17-(2'-furoate)

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 85 percent / pyridine / 1.5 h / 0 - 2 °C
2: 70 percent / KF / dimethylformamide / 4 h / 124 °C
3: 23 percent / 4-DMAP / CH2Cl2 / 27 h / 40 °C
View Scheme
Multi-step reaction with 3 steps
1: 85 percent / pyridine / 1.5 h / 0 - 2 °C
2: 70 percent / KF / dimethylformamide / 4 h / 124 °C
3: 58 percent / 4-DMAP / CH2Cl2 / 20 h / Ambient temperature
View Scheme
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    Business Type:Trading Company

    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

       Inquiry Now

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