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133051-88-4

Basic Information
CAS No.: 133051-88-4
Name: 5-[4'-(Bromomethyl)-[1,1'-biphenyl]-2-yl]-2-(triphenylmethyl)-2H-tetrazole
Article Data: 13
Molecular Structure:
Molecular Structure of 133051-88-4 (5-[4'-(Bromomethyl)-[1,1'-biphenyl]-2-yl]-2-(triphenylmethyl)-2H-tetrazole)
Formula: C33H25 Br N4
Molecular Weight: 557.492
Synonyms: 5-[4'-(Bromomethyl)[1,1'-biphenyl]-2-yl]-2-(triphenylmethyl)-2H-tetrazole;5-[4'-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole
Density: 1.28±0.1 g/cm3(Predicted)
Melting Point: 135-137 °C(Solv: ethyl ether (60-29-7))
Boiling Point: 718.4±70.0 °C(Predicted)
PSA: 43.60000
LogP: 7.74220
Synthetic route
133909-97-4

N-(trityl)-5-[4΄-(methyl)biphenyl-2-yl]-2H-tetrazole

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane for 3h; Heating;92%
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane for 8h; Heating;92%
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile) In dichloromethane at 28℃; Reflux;85%
114772-53-1

2-Cyano-4'-methylbiphenyl

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: zinc chloride; sodium azide / dimethylformamide / 36 h / Heating
1.2: 96 percent / aq. HCl / dimethylformamide / 1 h / cooling
2.1: 91 percent / aq. NaOH / toluene / 3 h / 20 °C
3.1: 92 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl4 / 8 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: 96 percent / ZnCl2; NaN3 / dimethylformamide / 36 h / Heating
2: 91 percent / aq. NaOH / toluene / 3 h / 20 °C
3: 92 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl4 / 8 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: trimethyltin azide / toluene / Heating
2: Et3N / CHCl3
3: NBS, AIBN / CCl4 / Heating
View Scheme
120568-11-8

5-<4'-Methyl-1,1'-biphenyl-2-yl>-1H-tetrazole

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 91 percent / aq. NaOH / toluene / 3 h / 20 °C
2: 92 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl4 / 8 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: Et3N / CHCl3
2: NBS, AIBN / CCl4 / Heating
View Scheme
Multi-step reaction with 2 steps
1: Et3N / CH2Cl2 / 1.5 h / Heating
2: N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 2 h / Heating
View Scheme
120568-11-8

2-(tetrazol-5-yl)-4'-methyl-1,1'-biphenyl

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 91 percent / aq. NaOH / toluene / 3 h / 20 °C
2: 92 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl4 / 8 h / Heating
View Scheme
106-38-7

para-bromotoluene

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 4 steps
2: 1.) Me3SnN3, 2.) aq. HCl / 1.) toluene, reflux, 24 h, 2.) 25 deg C
3: Et3N / CH2Cl2 / 1.5 h / Heating
4: N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 2 h / Heating
View Scheme
Multi-step reaction with 7 steps
1: magnesium / tetrahydrofuran / 2 h / 20 °C
2: tetrahydrofuran / 3 h / 20 °C
3: pyridine; trichlorophosphate / 3 h / 10 - 100 °C
4: sodium azide / toluene / 96 h / 110 °C
5: hydrogenchloride / tetrahydrofuran; water / 16 h / 20 °C
6: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C
7: N-Bromosuccinimide; Phthalic acid dibutyl ester / tetrachloromethane / 6 h / Reflux
View Scheme
2042-37-7

o-cyanobromobenzene

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 4 steps
2: 1.) Me3SnN3, 2.) aq. HCl / 1.) toluene, reflux, 24 h, 2.) 25 deg C
3: Et3N / CH2Cl2 / 1.5 h / Heating
4: N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 2 h / Heating
View Scheme
Multi-step reaction with 5 steps
1: nickel
2: sodium azide / toluene / 96 h / 110 °C
3: hydrogenchloride / tetrahydrofuran; water / 16 h / 20 °C
4: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C
5: N-Bromosuccinimide; Phthalic acid dibutyl ester / tetrachloromethane / 6 h / Reflux
View Scheme
57598-33-1

2-(2-methoxyphenyl)-4,4-dimethyl-2-oxazoline

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: tetrahydrofuran / 2 h / 20 °C
2: 96 percent / pyridine, phosphorus oxychloride / 3 h / 100 °C
3: 1.) tributyltin chloride, sodium azide, 2.) 10 N aq. sodium hydroxide / 1.) toluene, reflux, 70 h, 20 deg C, 3 h
4: 92 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 3 h / Heating
View Scheme
74201-13-1

N-(2-hydroxy-1,1-dimethyl)-2-methoxybenzamide

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: thionyl chloride / 1 h / 25 °C
2: tetrahydrofuran / 2 h / 20 °C
3: 96 percent / pyridine, phosphorus oxychloride / 3 h / 100 °C
4: 1.) tributyltin chloride, sodium azide, 2.) 10 N aq. sodium hydroxide / 1.) toluene, reflux, 70 h, 20 deg C, 3 h
5: 92 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 3 h / Heating
View Scheme
84392-32-5

4,4-dimethyl-2-(4'-methyl-biphenyl-2-yl)-4,5-dihydrooxazole

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 96 percent / pyridine, phosphorus oxychloride / 3 h / 100 °C
2: 1.) tributyltin chloride, sodium azide, 2.) 10 N aq. sodium hydroxide / 1.) toluene, reflux, 70 h, 20 deg C, 3 h
3: 92 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 3 h / Heating
View Scheme
Multi-step reaction with 5 steps
1: pyridine; trichlorophosphate / 3 h / 10 - 100 °C
2: sodium azide / toluene / 96 h / 110 °C
3: hydrogenchloride / tetrahydrofuran; water / 16 h / 20 °C
4: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C
5: N-Bromosuccinimide; Phthalic acid dibutyl ester / tetrachloromethane / 6 h / Reflux
View Scheme
579-75-9

2-Methoxybenzoic acid

133051-88-4

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 95 percent / thionyl chloride / 18 h / 20 °C
2: CH2Cl2 / 2 h / 20 °C
3: thionyl chloride / 1 h / 25 °C
4: tetrahydrofuran / 2 h / 20 °C
5: 96 percent / pyridine, phosphorus oxychloride / 3 h / 100 °C
6: 1.) tributyltin chloride, sodium azide, 2.) 10 N aq. sodium hydroxide / 1.) toluene, reflux, 70 h, 20 deg C, 3 h
7: 92 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 3 h / Heating
View Scheme
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Chemistry

Molecular Structure:

Molecular Formula: C33H25BrN4
Molecular Weight: 557.48 
Product Name: 5-[4'-(Bromomethyl)-[1,1'-biphenyl]-2-yl]-2-(triphenylmethyl)-2H-tetrazole
Synonyms of 5-[4'-(Bromomethyl)-[1,1'-biphenyl]-2-yl]-2-(triphenylmethyl)-2H-tetrazole (CAS NO.133051-88-4): 4-Bromomethyl-[2'-(2-Trityl-2H
CAS NO: 133051-88-4