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1334513-02-8

Basic Information
CAS No.: 1334513-02-8
Name: (S)-isopropyl 2-(((S)-(perfluorophenoxy)(phenoxy)phosphoryl)amino)propanoate
Article Data: 26
Cas Database
Molecular Structure:
Molecular Structure of 1334513-02-8 ((S)-isopropyl 2-(((S)-(perfluorophenoxy)(phenoxy)phosphoryl)amino)propanoate)
Formula: C18H17F5NO5P
Molecular Weight: 453.302
Synonyms: L-Alanine, N-[(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-, 1-methylethyl ester; N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)Phenoxyphosphinyl]-L-Alanine 1-Methylethyl Ester; N-[(S)-(2,3,4,5,6-Penta fluorophenoxy)phenoxy phosphinyl]-L-alanine 1-methylethyl ester; Sofosbuvir Side Chain; N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-phenoxyphosphinyl]-L-alanine 1-methylethyl ester; N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine1-Methylethyl ester; N-((S)-(2,3,4,5,6-Pentafluoro Phenoxy) Phenoxy Phosphinyl)-L--Alanine-1-Methyl Ethyl Ester; n-((s)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl)-l-alanine1-methylethylester; (2s)-isopropyl-2-((perfluorophenoxyl)(phenoxy)phosphorylamino)Propanoate
EINECS: 695-076-0
Density: 1.405
Melting Point: N/A
Boiling Point: 442.6±55.0 °C(Predicted)
Flash Point: N/A
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety:
Transport Information: N/A
PSA: 83.67000
LogP: 5.26860
Synthetic route
771-61-9

2,3,4,5,6-pentafluorophenol

770-12-7

O-phenyl phosphorodichloridate

39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Stage #1: 2,3,4,5,6-pentafluorophenol; O-phenyl phosphorodichloridate With triethylamine In chloroform at 0℃; under 11251.1 Torr;
Stage #2: alanine isopropyl ester hydrochloride In chloroform Temperature;
88%
Stage #1: alanine isopropyl ester hydrochloride With N-ethyl-N,N-diisopropylamine In dichloromethane at -68℃; for 0.5h;
Stage #2: O-phenyl phosphorodichloridate In dichloromethane at -10℃; for 0.5h;
Stage #3: 2,3,4,5,6-pentafluorophenol With N-ethyl-N,N-diisopropylamine In dichloromethane
78%
Stage #1: O-phenyl phosphorodichloridate; alanine isopropyl ester hydrochloride With triethylamine In dichloromethane at -78 - 20℃; for 2h;
Stage #2: 2,3,4,5,6-pentafluorophenol With triethylamine In dichloromethane at -78 - 20℃; for 3h;
61.6%
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

2263-53-8

sodium pentafluorophenolate

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Stage #1: phenyl(isopropoxy-L-alaninyl) phosphorochloridate; sodium pentafluorophenolate In tetrahydrofuran at -10℃;
Stage #2: With triethylamine In n-heptane; tert-butyl methyl ether pH=8;
66.81%
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

771-61-9

2,3,4,5,6-pentafluorophenol

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 4h;45.1%
With triethylamine In dichloromethane at 0℃; for 4h; Inert atmosphere;45.1%
17788-07-7

2,3,4,5,6-pentafluorophenyl dichlorophosphate

39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
Stage #1: 2,3,4,5,6-pentafluorophenyl dichlorophosphate With triethylamine; phenol In dichloromethane at 20℃; for 0.5h;
Stage #2: alanine isopropyl ester hydrochloride With triethylamine In dichloromethane at 0℃; for 1h;
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

771-61-9

2,3,4,5,6-pentafluorophenol

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;
With triethylamine In dichloromethane at -10 - 0℃; for 1.5h;A n/a
B n/a
With triethylamine In dichloromethane at -15 - 5℃; for 1h; Inert atmosphere;A n/a
B n/a
39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dichloromethane / 0.5 h / -10 °C / Inert atmosphere
2: triethylamine / dichloromethane / 1.5 h / -10 - 0 °C
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / tert-butyl methyl ether / 2 h / -65 - -50 °C / Inert atmosphere; Cooling with acetone-dry ice
2: triethylamine / dichloromethane / 1 h / -15 - 5 °C / Inert atmosphere
View Scheme
770-12-7

O-phenyl phosphorodichloridate

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dichloromethane / 0.5 h / -10 °C / Inert atmosphere
2: triethylamine / dichloromethane / 1.5 h / -10 - 0 °C
View Scheme
771-61-9

2,3,4,5,6-pentafluorophenol

770-12-7

O-phenyl phosphorodichloridate

39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

C18H17F5NO4P

Conditions
ConditionsYield
Stage #1: alanine isopropyl ester hydrochloride With triethylamine In dichloromethane at -70℃; for 0.75h;
Stage #2: O-phenyl phosphorodichloridate In dichloromethane at -70 - 0℃; for 8h;
Stage #3: 2,3,4,5,6-pentafluorophenol With triethylamine In dichloromethane at 0 - 20℃;
770-12-7

O-phenyl phosphorodichloridate

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: triethylamine / ethyl acetate / 1 h / -10 °C / Enzymatic reaction
1.2: 2.5 h / -5 - 25 °C
2.1: triethylamine / ethyl acetate; n-heptane / 4 - 8 h / Resolution of racemate
View Scheme
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 1.5 h / -60 - 25 °C / Inert atmosphere
2.1: tetrahydrofuran / -10 °C
2.2: pH 8
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 20 h / -70 - 20 °C
2: triethylamine / dichloromethane / 20 h / -5 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 1 h / -78 - 20 °C
2: triethylamine / dichloromethane / 4 h / 0 °C
View Scheme
39825-33-7

isopropyl L-alanine

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: triethylamine / ethyl acetate / 1 h / -10 °C / Enzymatic reaction
1.2: 2.5 h / -5 - 25 °C
2.1: triethylamine / ethyl acetate; n-heptane / 4 - 8 h / Resolution of racemate
View Scheme
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    N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-Methylethyl ester

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    Isopropyl N-[(pentafluorophenoxy)(phenoxy)phosphoryl]-L-alaninate 1334513-02-8

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  • Isopropyl N-[(pentafluorophenoxy)(phenoxy)phosphoryl]-L-alaninate

  • Casno:

    1334513-02-8

    Isopropyl N-[(pentafluorophenoxy)(phenoxy)phosphoryl]-L-alaninate

    Min.Order: 100 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

    Our Service 1.Own made fine chemical products 2.Out sourcing and quality controlling service in China 3. COM for Chemical synthesis 4.Lab custom synthesis of API and intermadiates Quality Assurance 1. NMR,HPLC and COA can b

    Triumph International Development Limilted is engaged in the API, pharmaceutical intermediates research and developmen.Adhering to the "customer first" business philosophy,we suppl

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-536-7971999

    Address:Yinhai Road,Shouguang

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  • SF-1.2

  • Casno:

    1334513-02-8

    SF-1.2

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

    Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

  •  Afine Chemicals Limited

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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  • (S)-isopropyl 2-(((S)-(perfluorophenoxy)(phenoxy)phosphoryl)amino)propanoate

  • Casno:

    1334513-02-8

    (S)-isopropyl 2-(((S)-(perfluorophenoxy)(phenoxy)phosphoryl)amino)propanoate

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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  • Featured products N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-Methylethyl ester

  • Casno:

    1334513-02-8

    Featured products N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-Methylethyl ester

    Min.Order: 100 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

    Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

    We are a team of industry experts, dedicated to delivering the best chemical solutions from quality suppliers across China. Putting our customers first, we take a holistic approach

  •  Chemlyte Solutions

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-189 8945 5137

    Address:Jian Qiao Community, 789 Shenhua Road, Xihu District, Hangzhou, China, 310000

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  • N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-methylethyl ester

  • Casno:

    1334513-02-8

    N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-methylethyl ester

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 100.0-100.0/Kilogram

    HangYu Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. HangYu Chemical consis

    Zibo HangYu Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals

  •  Zibo Hangyu Import&Export Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15988566987

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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  • CAS 1334513-02-8 (2S)-Isopropyl-2-((perfluorophexyl) (phenoxy)phosphorylamino Propanoate

  • Casno:

    1334513-02-8

    CAS 1334513-02-8 (2S)-Isopropyl-2-((perfluorophexyl) (phenoxy)phosphorylamino Propanoate

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 1.0-1.0/Kilogram

    We promise our customer following items 1.Reasonable price: We provide high quality products with competitive price in china, 2.Low moq: No worry about the low moq, our moq is 1 gram or lower. 3.Good and efficient service,Fast Delivery Fast respond

    Xi’an JunYuan Biotech Co., Ltd., which is specialized in fine chemicals research, production and sales. It has strong professional research and development team, talented personne

  •  XI'AN JUNYUAN BIO-TECH CO., LTD.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-29-86106815

    Address:Block C of XINJIE, No. 398, Fengcheng 6 Road, Xi'an Economic & Technological Development Zone

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  • Lower Price N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-Phenoxy-Phosphinyl]-1-Methylethyl Ester

  • Casno:

    1334513-02-8

    Lower Price N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-Phenoxy-Phosphinyl]-1-Methylethyl Ester

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0/Kilogram

    Product name: N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-Phenoxy-Phosphinyl]-1-Methylethyl Ester CAS No.: 1334513-02-8 Molecule Formula:C18H17F5NO5P Molecule Weight:453.30 Purity: 99.0% Package: 25kg/drum Description:White powder Manufactu

    Siwei Development Group Ltd. is a reputed professional enterprise in China dedicated to the Amino Acids production and sales of fine chemical products.Over the years we have been m

  •  Siwei Development Group Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-571-82881840

    Address:Rm2-2-503 Zhongdingyuan, Xianghurenjia Wenyan Xiaoshan, Hangzhou China

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