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Basic Information
CAS No.: 133627-45-9
Name: 3-Amino-2-chloro-4-methylpyridine
Molecular Structure:
Molecular Structure of 133627-45-9 (3-Amino-2-chloro-4-methylpyridine)
Formula: C6H7ClN2
Molecular Weight: 142.588
Synonyms: 2-Chloro-4-methyl-3-pyridinamine;2-Chloro-4-methylpyridin-3-amine;3-amino-2-chloro-4-methylpyridine;Capic;3-Amino-2-chloro-4-methyl pyridine;2-Chloro-3-amino-4-methylpyridine;
EINECS: -0
Density: 1.26 g/cm3
Melting Point: 61-64 °C
Boiling Point: 283.3 °C at 760 mmHg
Flash Point: 125.2 °C
Appearance: off white crystals
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37/39-36
PSA: 38.91000
LogP: 2.20680
Related products
Synthetic route
23056-39-5

2-chloro-3-nitro-4-methylpyridine

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
With hydrogenchloride; tin(ll) chloride In diethyl ether for 0.333333h; Ambient temperature;98%
Stage #1: 2-chloro-3-nitro-4-methylpyridine With iron; acetic acid at 70 - 80℃;
Stage #2: With sodium carbonate In water pH=8.0 - 8.5; Product distribution / selectivity;		90.79%
Stage #1: 2-chloro-3-nitro-4-methylpyridine With hydrogenchloride In methanol; water at 65℃;
Stage #2: With iron In methanol; water at 65℃; Product distribution / selectivity;		90.1%
152362-01-1

2-chloro-4-methyl-3-pyridinecarboxamide

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
With sodium hypobromide; bromine; sodium hydroxide In water at 65 - 75℃; for 4h; Hofmann Rearrangement;98%
With bromine; sodium hydroxide In water at 0 - 20℃; for 2h;97%
With bromine; sodium hydroxide In water; toluene at 0 - 60℃;96.9%

4-methylpiperidin-3-one

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
Stage #1: 4-methylpiperidin-3-one With hydrogenchloride; dihydrogen peroxide In chloroform; water at 30 - 40℃; for 5h; Green chemistry;
Stage #2: With ammonium hydroxide at 40 - 45℃; for 3h; Solvent; Reagent/catalyst; Green chemistry;		93.3%
3430-27-1

3-amino-4-methylpyridine

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
With hydrogenchloride; dihydrogen peroxide at 20℃; for 0.5h;89%
With hydrogenchloride; chlorine In water at 20℃; for 0.416667h;84%
Stage #1: 3-amino-4-methylpyridine With hydrogenchloride In water at 40℃; Cooling with ice;
Stage #2: With dihydrogen peroxide for 2h;		83.2%
5832-44-0

3-nitro-4-methylpyridine

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 97 percent / H2 / 5 percent Pd/C / methanol / 5 h / 20 °C / 3750.3 Torr
2: 89 percent / conc. aq. HCl; 35 percent aq. H2O2 / 0.5 h / 20 °C
View Scheme
50839-95-7

2-chloro-4-methylnicotinoylchloride

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NH3(g) / toluene / below 30 deg C
2: 93 percent / NaOH, Br2 / H2O / 1.) 5 deg C; 2.) 75 deg C, 90 min
View Scheme
50840-02-3

ethyl 2-chloro-4-methyl-3-pyridinecarboxylate

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 90 percent / NaOH / methanol; H2O / 75 °C
2: SOCl2 / toluene / 1.) 70 deg C, 1 h; 2.) reflux, 4 h
3: NH3(g) / toluene / below 30 deg C
4: 93 percent / NaOH, Br2 / H2O / 1.) 5 deg C; 2.) 75 deg C, 90 min
View Scheme
142266-63-5

2-chloro-4-methyl-3-pyridinecarboxylic acid

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: SOCl2 / toluene / 1.) 70 deg C, 1 h; 2.) reflux, 4 h
2: NH3(g) / toluene / below 30 deg C
3: 93 percent / NaOH, Br2 / H2O / 1.) 5 deg C; 2.) 75 deg C, 90 min
View Scheme
152362-00-0

ethyl 2-chloro-2-cyano-3-methyl-5-oxopentanoate

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 17 percent / PCl3, HCl(g) / dimethylformamide / 1.) 85 deg C; 2.) 90 deg C
2: 90 percent / NaOH / methanol; H2O / 75 °C
3: SOCl2 / toluene / 1.) 70 deg C, 1 h; 2.) reflux, 4 h
4: NH3(g) / toluene / below 30 deg C
5: 93 percent / NaOH, Br2 / H2O / 1.) 5 deg C; 2.) 75 deg C, 90 min
View Scheme
23056-39-5

2-chloro-3-nitro-4-methylpyridine

tin(IV) chloride dihydrate

133627-45-9

3-Amino-2-chloro-4-methylpyridine

Conditions
ConditionsYield
With sodium hydroxide; acetic acid In hydrogenchloride; water
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Chemistry

Molecular structure of 3-Amino-2-chloro-4-methyl pyridine (CAS NO.133627-45-9) is:

IUPAC: 2-Chloro-4-methylpyridin-3-amine
CAS Registry Number: 133627-45-9
Molecular Formula: C6H7ClN2
Molecular Weight: 142.59
Melting Point: 61-64°C
Surface Tension: 49.9 dyne/cm
Density: 1.26 g/cm3
Flash Point: 125.2 °C
Enthalpy of Vaporization: 52.23 kJ/mol
Boiling Point: 283.3 °C at 760 mmHg
Vapour Pressure: 0.00318 mmHg at 25°C
Product Categories: Pyridine;Amines and Anilines;Heterocycles;Pyridines, Pyrimidines, Purines and Pteredines;pharmacetical;Amines;Pyridines;Heterocyclic Compounds;(intermediate of nevirapine);Aromatics Compounds;Chloropyridines;Halopyridines;Aromatics;Bases & Related Reagents;Nucleotides

Uses

 3-Amino-2-chloro-4-methyl pyridine (CAS NO.133627-45-9) is the important intermediates .

Safety Profile

Safty information about 3-Amino-2-chloro-4-methyl pyridine (CAS NO.133627-45-9) is:
Hazard Codes: IrritantXi
Risk Statements: 36/37/38 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39-36 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection. 
S36:Wear suitable protective clothing.
RIDADR: UN2811
Hazard Note: Irritant
HazardClass: 6.1
PackingGroup: III

Specification

 3-Amino-2-chloro-4-methyl pyridine , its cas register number is 133627-45-9. It also can be called 2-Chloro-3-amino-4-picoline .It is a off white crystals.