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1341224-83-6

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Basic Information
CAS No.: 1341224-83-6
Name: INCB8761(PF-4136309)
Article Data: 1
Molecular Structure:
Molecular Structure of 1341224-83-6 (INCB8761(PF-4136309))
Formula: C29H31F3N6O3
Molecular Weight: 568.599
Synonyms: INCB 8761(PF-4136309);(S)-N-(2-(3-((4-hydroxy-4-(5-(pyrimidin-2-yl)pyridin-2-yl)cyclohexyl)amino)pyrrolidin-1-yl)-2-oxoethyl)-3-(trifluoromethyl)benzamide;(S)-N-[2-(3-{trans-4-hydroxy-4-[5-(pyrimidin-2-yl)pyridin-2-yl]cyclohexylamino}pyrrolidin-1-yl)-2-oxoethyl]-3-(trifluoromethyl)benzamide;INCB8761(PF-4136309);
Density: 1.40±0.1 g/cm3(Predicted)
Boiling Point: 712.2±60.0 °C(Predicted)
Appearance: Off-white to light yellow solid
PSA: 120.34000
LogP: 4.02780
Synthetic route
857651-06-0

4-hydroxy-4-(5-(pyrimidin-2-yl)pyridin-2-yl)cyclohexanone

857651-01-5

(S)-N-{2-[3-aminopyrrolidin-1-yl]-2-oxoethyl}-3-(trifluoromethyl)benzamide hydrochloride

1341224-83-6

PF-4136309

Conditions
ConditionsYield
Stage #1: 4-hydroxy-4-(5-(pyrimidin-2-yl)pyridin-2-yl)cyclohexanone; (S)-N-{2-[3-aminopyrrolidin-1-yl]-2-oxoethyl}-3-(trifluoromethyl)benzamide hydrochloride With triethylamine In 2-methyl-propan-1-ol for 0.5h; Cooling with ice;
Stage #2: With sodium tris(acetoxy)borohydride In 2-methyl-propan-1-ol at 20℃; for 4h;
66%
624-28-2

2,5-dibromopyridine

1341224-83-6

PF-4136309

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: n-butyllithium / toluene / 2.5 h / -78 °C
1.2: -78 - 20 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 3.67 h / 25 °C / Inert atmosphere
2.2: 25 °C / Inert atmosphere
3.1: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 - 25 °C
4.1: triethylamine / 2-methyl-propan-1-ol / 0.5 h / Cooling with ice
4.2: 4 h / 20 °C
View Scheme
4746-97-8

cyclohexanedione monoethylene ketal

1341224-83-6

PF-4136309

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: n-butyllithium / toluene / 2.5 h / -78 °C
1.2: -78 - 20 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 3.67 h / 25 °C / Inert atmosphere
2.2: 25 °C / Inert atmosphere
3.1: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 - 25 °C
4.1: triethylamine / 2-methyl-propan-1-ol / 0.5 h / Cooling with ice
4.2: 4 h / 20 °C
View Scheme
708274-37-7

8-(5-bromopyridin-2-yl)-1,4-dioxaspiro[4.5]decan-8-ol

1341224-83-6

PF-4136309

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 3.67 h / 25 °C / Inert atmosphere
1.2: 25 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 - 25 °C
3.1: triethylamine / 2-methyl-propan-1-ol / 0.5 h / Cooling with ice
3.2: 4 h / 20 °C
View Scheme
857651-05-9

8-(5-pyrimidin-2-ylpyridin-2-yl)-1,4-dioxaspiro[4.5]decan-8-ol

1341224-83-6

PF-4136309

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 - 25 °C
2.1: triethylamine / 2-methyl-propan-1-ol / 0.5 h / Cooling with ice
2.2: 4 h / 20 °C
View Scheme
17794-48-8

m-trifluoromethylhippuric acid

1341224-83-6

PF-4136309

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 20 °C / Cooling with ice
2.1: hydrogenchloride / 1,4-dioxane; methanol / 1 h / 20 °C
3.1: triethylamine / 2-methyl-propan-1-ol / 0.5 h / Cooling with ice
3.2: 4 h / 20 °C
View Scheme
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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0852-0755-61104662

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    1341224-83-6

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    Todachem specialize in exporting chemicals for 10 years, we manufacture and distribute high quality pharmaceutical APIs, intermediates, special chemicals, active molecule and other fine chemicals. We have our research laboratory and more than 100 n

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    1.Custom synthetic service could be provided and COA/HPLC/HNMR is available. 2.Professional synthesis laboratory and production base. 3.Strong synthesis team and service team.4.Professional data management system.5.We provide the professional test da

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    China (Mainland)  |  Contact Details

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  • INCB8761(PF-4136309)

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    1341224-83-6

    INCB8761(PF-4136309)

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    United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    1,Best Quality: Our products have exported to Germany, Spain, UK, USA, Australia, Middle East, and so on other countries, and we have got very good feedback from our customers.so

    Hubei Jusheng Technology Co., Ltd., is a large group corporation which engaged in the R&D and manufacture of chemicals, Pharmaceuticals and intermediates. We have earned ourselves

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • PF-4136309,1341224-83-6

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    1341224-83-6

    PF-4136309,1341224-83-6

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    Superiority: 1. Quality: High purity, strict quality control, 10 years experience in chemical industry. 2. Price: Moderate price, more QTY more discount. 3. MOQ: Sample order is welcome to test quality. 4. Shipping time: In Stock, can be sh

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:13545198479

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    1341224-83-6

    PF-4136309 (INCB-8761) with approved quality

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    Wuhan Prominence Bio-technology Co., Ltd is a leading provider and manufacturer of pharmaceutical and chemical products. Mainly involves API, pharmaceutical intermediates peditides and natural extract etc. We are capable to supply you with any quanti

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • INCB-8761/1341224-83-6  high purity

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    1341224-83-6

    INCB-8761/1341224-83-6 high purity

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    INCB-8761/1341224-83-6 high purityAppearance:Yellow crystalline powder Storage:Room temperature,protect from light Package:bottle Application:pharma research Transportation:By Courier or by air

    Locating in Changchun bonded area, which has absolute advantage of importing and exporting, with the R&D team having more than 10 years experience of OLED material and intermediate

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • INCB-8761/1341224-83-6  high purity

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    1341224-83-6

    INCB-8761/1341224-83-6 high purity

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    We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

    Our company has been engaged in the Pharmaceutical raw material and pharmaceutical intermediates medicine material intermediates and related chemical industry for more than ten ye

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-576-88869393

    Address:Jiaojiang District, Taizhou, Zhejiang, China.

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  • 1341224-83-6

  • Casno:

    1341224-83-6

    1341224-83-6

    Min.Order: 0

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    INCB-8761/1341224-83-6 high purity Application:pharma research

    We are Hebei minshang biotechnology co. LTD., mainly deal in pharmaceutical intermediates and various chemicals. We are manufacturers and have our own factory. Products & Usage Ph

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18032092709

    Address:hebei

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  • INCB-8761/1341224-83-6  high purity

  • Casno:

    1341224-83-6

    INCB-8761/1341224-83-6 high purity

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    INCB-8761/1341224-83-6 high purityAppearance:Yellow crystalline powder Storage:Room temperature,protect from light Package:bottle Application:pharma research Transportation:By Courier or by air

    Shanghai PengMo Biotechnology Co., Ltd. is engaging in researching, developing, manufacturing and exporting advanced pharmaceutical intermediates and other fine chemicals. Our comp

  • Shanghai PengMo Biotechnology Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-13052359378

    Address:No.218 Hai Qu Road.Shanghai.China

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