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13478-20-1

Basic Information
CAS No.: 13478-20-1
Name: PHOSPHORYL FLUORIDE
Article Data: 144
Molecular Structure:
Molecular Structure of 13478-20-1 (PHOSPHORYL FLUORIDE)
Formula: F3O P
Molecular Weight: 103.968
Synonyms: Phosphorylfluoride (6CI,8CI); Phosphorus fluoride oxide (PF3O); Phosphorus fluoride oxide(POF3); Phosphorus oxyfluoride; Phosphorus oxyfluoride (POF3); Phosphorustrifluoride oxide; Phosphoryl trifluoride; Trifluorophosphine oxide;Trifluorophosphorus oxide
Density: 1.506g/cm3
Melting Point: -39.1℃ [KIR78]
Boiling Point: °Cat760mmHg
Flash Point: °C
Solubility: hydrolyzes [KIR78]
Risk Codes: 14-34-36/37/38
Safety:
Risk Statements 14-34-36/37/38
Safety Statements 7/9-26-36/37/39-45
RIDADR 3308
PSA: 26.88000
LogP: 2.00300
Synthetic route

POF3*(CH3)3NO*BF3

A

13478-20-1

trifluorophosphoric acid

B

trimethyl amine oxyde boron trifluoride

Conditions
ConditionsYield
In neat (no solvent) at -78°C during 17 h;;A 100%
B n/a
16752-60-6

phosphorus pentoxide

7647-19-0, 874483-74-6

phosphorus pentafluoride

13478-20-1

trifluorophosphoric acid

Conditions
ConditionsYield
In neat (no solvent) N2-atmosphere; heating at 250°C for 3 d;99%

phosphorous

7782-41-4

fluorine

A

13478-20-1

trifluorophosphoric acid

7647-19-0, 874483-74-6

phosphorus pentafluoride

Conditions
ConditionsYield
In further solvent(s) fluorination (N2 carrier gas (ratio F/N2 1:5), -50°C) in freon-11;A n/a
B 90%

(C6F5)3B-O-Ti(acac)2

429-07-2

tetraethylammonium hexafluorophosphate

A

13478-20-1

trifluorophosphoric acid

16986-93-9

Ti(CH3COCHCOCH3)2F2

C

C19H3BF15(2-)

Conditions
ConditionsYield
In chloroform-d1; benzene for 3h; Schlenk technique; Inert atmosphere;A n/a
B 88%
C n/a
7664-39-3

hydrogen fluoride

A

13478-20-1

trifluorophosphoric acid

B

13769-76-1

phosphoryl dichloride fluoride

C

13769-75-0

phosphorus oxydifluorochloride

Conditions
ConditionsYield
50-70°C;A n/a
B 80%
C n/a
In neat (no solvent) react. of boiling POCl3 with HF;; fractionation of formed mixt.;;
7789-21-1

fluorosulphonic acid

phosphorus pentoxide

13478-20-1

trifluorophosphoric acid

Conditions
ConditionsYield
In neat (no solvent) byproducts: HPO3, SO3, H2SO4; droping HSO3F on P2O5 in excess;;80%
In neat (no solvent) byproducts: HPO3, SO3, H2SO4; droping HSO3F on P2O5 in excess;;80%

K(1+)*PO2F2AsF5(1-)=KPO2F2AsF5

A

potassium fluoride

B

13478-20-1

trifluorophosphoric acid

Conditions
ConditionsYield
N2-atmosphere; stay at room temp. for 170 h; can be accelerated by heating at 110°C;A n/a
B 47%

(C6F5)3B-O-V(acac)2

429-07-2

tetraethylammonium hexafluorophosphate

A

13478-20-1

trifluorophosphoric acid

B

[V(acac)3]+

C

C19H3BF15(2-)

Conditions
ConditionsYield
In chloroform-d1; benzene for 3h; Solvent; Time; Schlenk technique; Inert atmosphere;A n/a
B 40%
C n/a

aluminum cyclophosphate

aluminium fluoride

A

13478-20-1

trifluorophosphoric acid

879634-80-7

aluminium phosphate

Conditions
ConditionsYield
In neat (no solvent, solid phase) byproducts: AlPO4 (cristobalite-like); heated to 500°C, 1 h;A n/a
B 4%

phosphorous

13465-66-2, 271781-78-3

selenium(IV) fluoride

A

7446-08-4

selenium(IV) oxide

B

13478-20-1

trifluorophosphoric acid

C

1087413-67-9

nitrosylsulfuric acid fluoride

D

7783-55-3

trifluorophosphane

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