CAS No.13497-18-2,Bis[3-(triethoxysilyl)propyl]amine Suppliers

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Basic Information

Molecular Structure:
CAS No.:	13497-18-2
Name:	Bis[3-(triethoxysilyl)propyl]amine
Article Data:	11

Formula:	C₁₈H₄₃NO₆Si₂
Molecular Weight:	425.714
Synonyms:	3,13-Dioxa-8-aza-4,12-disilapentadecane,4,4,12,12-tetraethoxy- (6CI,8CI);Silane, [iminobis(trimethylene)]bis[triethoxy-(8CI);3,3'-Bis(triethoxysilyl)propylamine;Bis(3-methoxysilylpropyl)amine;Bis(triethoxysilylpropyl)amine;Dynasylan1122;G 402;G 402 (coupling agent);Si 252;
EINECS:	236-818-1
Density:	0.958 g/cm³
Melting Point:	<0 °C
Boiling Point:	408 °C at 760 mmHg
Flash Point:	200.6 °C
Solubility:	23-1000000mg/L at 20℃
Appearance:	Yellowish clear liquid
Hazard Symbols:	C
Risk Codes:	34
Safety:	26-28-36/37/39-45
Transport Information:	UN 2735
PSA:	67.41000
LogP:	3.84390

Synthetic route

: 5089-70-3
(3-chloropropyl)triethoxysilane

A: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

B tris-<3-triethoxysilanyl-propyl>-amine and 3-triethoxysilanyl-propylamine: tris-<3-triethoxysilanyl-propyl>-amine and 3-triethoxysilanyl-propylamine

Conditions

Conditions	Yield
With ammonia

: 919-30-2
3-aminopropyltriethoxysilane

: 5089-70-3
(3-chloropropyl)triethoxysilane

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

Conditions

Conditions	Yield
at 70℃; for 5.5h; Inert atmosphere;	482 g

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: 109-70-6
1,3-chlorobromopropane

: 3-chloro-N,N-bis(3-(triethoxysilyl)propyl)propane-1-amine

Conditions

Conditions	Yield
With calcium hydride In N,N-dimethyl-formamide at 23℃; for 15h; Reagent/catalyst;	99%
With calcium hydride In N,N-dimethyl-formamide at 23℃; for 15h;	99%

: 3121-61-7
2-methoxyethyl acrylate

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: 2-methoxyethyl 3-(bis(3-triethoxysilylpropyl)amino)propanoate

Conditions

Conditions	Yield
In ethanol at 20℃; for 8h; Inert atmosphere;	97.3%

: 1003-10-7
Thiobutyrolactone

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: 1333386-63-2
4-mercapto-N,N-bis(3-(triethoxysilyl)propyl)butanamide

Conditions

Conditions	Yield
In toluene for 48h; Reflux; Inert atmosphere;	96%

: 50-00-0
formaldehyd

: 64-17-5
ethanol

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: 1440531-01-0
N-(ethoxymethyl)-N,N-bis(3-triethoxysilylpropyl)amine

Conditions

Conditions	Yield
at 80℃; for 0.0833333h; Inert atmosphere;	95%
at 80℃; for 0.0833333h; Inert atmosphere;	95 mg

...Expand

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: 106-96-7
propargyl bromide

: N,N-bis((3-triethoxysilyl)propyl)prop-2-yn-1-amine

Conditions

Conditions	Yield
With calcium hydride In tetrahydrofuran; water; toluene at 20℃; Inert atmosphere; Schlenk technique;	95%
In tetrahydrofuran; water; toluene at 20℃;	95%
With calcium hydride In tetrahydrofuran; water; toluene at 20℃; for 16h;	95%

: 42059-30-3
1-azido-2-iodoethane

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: N‐(2‐azidoethyl)‐3‐(triethoxysilyl)‐N‐(3‐(triethoxysilyl)propyl)propan‐1‐amine

Conditions

Conditions	Yield
With potassium carbonate In acetonitrile at 85℃; for 16h; Inert atmosphere; Schlenk technique; Sealed tube;	95%
With potassium carbonate In acetonitrile at 85℃; for 18h; Sealed tube; Inert atmosphere;

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: 71321-16-9
3-(trimethylsilyl)prop-2-yn-1-yl 4-methylbenzenesulfonate

: (3-trimethylsilylprop-2-ynyl)bis(3-triethoxysilylpropyl)amine

Conditions

Conditions	Yield
With potassium carbonate In acetonitrile at 85℃; for 15h;	94%

: 13497-18-2
bis-(3-triethoxysilylpropyl)amine

: phenoxy tetraethyleneglycol acrylate

: 2-(2-(2-(2-phenoxyethoxy)ethoxy)ethoxy)ethyl 3-(bis(3-(triethoxysilyl)propyl)amino)propanoate

Conditions

Conditions	Yield
In ethanol at 20℃; for 8h; Inert atmosphere;	93.7%

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Chemistry

IUPAC Name: 3-Triethoxysilyl-N-(3-triethoxysilylpropyl)propan-1-amine
Systematic of 1-Propanamine,3-(triethoxysilyl)-N-[3-(triethoxysilyl)propyl]- (CAS NO.13497-18-2): Bis(3-triethoxysilylpropyl)amine ; EINECS 236-818-1
CAS NO: 13497-18-2
Molecular Formula of 1-Propanamine,3-(triethoxysilyl)-N-[3-(triethoxysilyl)propyl]- (CAS NO.13497-18-2): C₁₈H₄₃NO₆Si₂
Molecular Weight: 425.7081
Molecular Structure:

Melting Point: <0°C
Polar Surface Area: 58.62 Å²
Index of Refraction: 1.439
Molar Refractivity: 116.94 cm³
Molar Volume: 444.1 cm³
Surface Tension: 27 dyne/cm
Density of 1-Propanamine,3-(triethoxysilyl)-N-[3-(triethoxysilyl)propyl]- (CAS NO.13497-18-2): 0.958 g/cm³
Flash Point: 200.6 °C
Enthalpy of Vaporization: 66 kJ/mol
Boiling Point: 408 °C at 760 mmHg
Vapour Pressure: 7.22E-07 mmHg at 25°C

Safety Profile

Hazard Codes: Corrosive C
Risk Statements: 34
R34: Causes burns.
Safety Statements: 26-28-36/37/39-45
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S28: After contact with skin, wash immediately with plenty of soap-suds.
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: 2735
TSCA: Yes