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13569-63-6

Basic Information
CAS No.: 13569-63-6
Name: RHENIUM(III) CHLORIDE
Molecular Structure:
Molecular Structure of 13569-63-6 (RHENIUM(III) CHLORIDE)
Formula: Cl3Re
Molecular Weight: 292.566
Synonyms: Rheniumchloride; Rhenium trichloride
EINECS: 236-987-1
Density: 4800 kg/m3
Melting Point: decomposes at 500℃ [LID94]
Boiling Point: 500 °C (decomposes)
Flash Point: °C
Solubility: Soluble in water.
Appearance: red, crystalline, nonvolatile solid
Hazard Symbols: IrritantXiCorrosiveC
Risk Codes: 36/37/38
Safety: 26-37/39
PSA: 0.00000
LogP: 2.06850
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Chemistry

IUPAC Name: Trichlororhenium
Synonyms: Rhenium trichloride ; Rhenium(iii) chloride ; Rhenium chloride ; Rhenium(+3)chloride ; Rheniumchloride(recl3) ; Rheniumchloridemeshredblackpowder ; Rhenium(III) chloride, 99.8+% (metals basis) ; Rhenium(III) trichloride
Product Categories: Catalysis and Inorganic Chemistry;Chemical Synthesis;Rhenium Salts;RheniumMetal and Ceramic Science;Salts
CAS NO: 13569-63-6
Molecular Formula: Cl3Re
Molecular Weight: 292.57
Molecular Structure:
EINECS: 236-987-1
Mol File: 13569-63-6.mol
Boiling Point: >550°C
Sensitive: Rhenium trichloride (CAS NO.13569-63-6) is moisture sensitive .

Uses

  Rhenium trichloride (CAS NO.13569-63-6) is used as a starting material for synthesis of rhenium complexes. ReCl3 can react with peralkylated benzene-metal complexes that act as electron reservoirs.

Production

 Rhenium trichloride (CAS NO.13569-63-6) is most efficiently prepared by the thermal decomposition of rhenium pentachloride in nitrogen. Other methods include reacting sulphuryl chloride with rhenium powder with or without the addition of aluminium chloride, the thermal decomposition of salts of hexachlororhenic(IV) acid, or the heating of Re2(O2CCH3)4Cl2 under HCl gas.

 

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
cat LDLo intravenous 20mg/kg (20mg/kg) VASCULAR: BP ELEVATION NOT CHARACTERIZED IN AUTONOMIC SECTION Journal of Pharmaceutical Sciences. Vol. 57, Pg. 321, 1968.
mouse LD50 intraperitoneal 280mg/kg (280mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

BEHAVIORAL: EXCITEMENT
Journal of Pharmaceutical Sciences. Vol. 57, Pg. 321, 1968.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intraperitoneal route. When heated to decomposition it emits toxic fumes of Cl. See also RHENIUM and CHLORIDES.
Hazard Codes IrritantXi
Risk Statements 36/37/38 
R36/37/38: Rhenium trichloride (CAS NO.13569-63-6) is irritating to eyes, respiratory system and skin.
Safety Statements 26-37/39 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S37/39: When Rhenium trichloride (CAS NO.13569-63-6) is used ,wear suitable gloves and eye/face protection.
WGK Germany 3
RTECS VI0875000
 

 

Specification

Rhenium trichloride prepared from rhenium pentachloride without further treatment is chemically reactive, but if it is vacuum sublimed at 500oC, then it becomes comparatively unreactive. However, x-ray diffraction tests show no observable difference in structure between the untreated and vacuum sublimed material.
The heat of oxidation according to the equation,
ReCl3(s) + 4OH- + 2OCl- → ReO4- + 2H2O + 5Cl-
is 190.7 ± 0.2 kcal/mol.