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CAS No.: | 13633-25-5 |
---|---|
Name: | 1-Bromo-4-phenylbutane |
Article Data: | 71 |
Molecular Structure: | |
Formula: | C10H13Br |
Molecular Weight: | 213.117 |
Synonyms: | (4-Bromobutyl)benzene;1-Phenyl-4-bromobutane;4-Bromo-1-phenylbutane;4-Phenyl-1-bromobutane;4-Phenylbutyl bromide;NSC 89816; |
Density: | 1.265 g/cm3 |
Melting Point: | 52 °C |
Boiling Point: | 265.2 °C at 760 mmHg |
Flash Point: | 142.5 °C |
Solubility: | Slightly soluble in water. |
Appearance: | cream |
Hazard Symbols: | Xi |
Risk Codes: | 36/37/38 |
Safety: | 26-36 |
PSA: | 0.00000 |
LogP: | 3.40420 |
Conditions | Yield |
---|---|
With triphenylphosphine In dichloromethane; hexane-diethyl ether | 100% |
4-phenyl-butan-1-ol
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With hydrogen bromide for 12h; Reagent/catalyst; Irradiation; Reflux; | 99.6% |
With allyl bromide; 1,1'-carbonyldiimidazole In acetonitrile for 1h; Heating; | 98% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 25℃; | 95% |
N-methyl-N-[4-(diphenylphosphino)benzyl]pyrrolidinium bromide
4-phenyl-butan-1-ol
A
Br(1-)*C24H27NOP(1+)
B
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With carbon tetrabromide In 1,2-dichloro-ethane at 40℃; for 2h; | A n/a B 97% |
4-Phenylbutyric acid
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With trimethylsilyl bromide; 1,1,3,3-Tetramethyldisiloxane; indium tribromide In chloroform at 60℃; for 4h; Sealed tube; Inert atmosphere; | 97% |
With indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane; trimethylsilyl cyanide In chloroform at 60℃; Inert atmosphere; | |
Multi-step reaction with 2 steps 1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere 2: triphenylphosphine; carbon tetrabromide / acetonitrile / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 20 °C 2: triphenylphosphine; carbon tetrabromide / acetonitrile / 3 h / 20 °C View Scheme |
(4-bromo-1-buten-1-yl)benzene
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethanol; water under 225.023 Torr; for 5h; | 93% |
4-(diphenylphosphino)-benzyltrimethylammonium bromide
4-phenyl-butan-1-ol
A
Br(1-)*C22H25NOP(1+)
B
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With carbon tetrabromide In 1,2-dichloro-ethane at 60℃; for 2h; | A n/a B 91% |
Conditions | Yield |
---|---|
at 5℃; for 2h; Temperature; | 85.8% |
Conditions | Yield |
---|---|
With copper(I) bromide; lithium bromide In tetrahydrofuran at 50 - 55℃; for 1h; | 85% |
benzenediazonium tetrafluoroborate
4-bromo-1-butylboronic acid catechol ester
1-Bromo-4-phenylbutane
Conditions | Yield |
---|---|
With 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; palladium diacetate In tetrahydrofuran at 20℃; for 4.5h; Sizuki-Miyaura cross coupling; | 61% |
4-phenyl-butan-1-ol
triphenylphosphine
A
1-Bromo-4-phenylbutane
B
Triphenylphosphine oxide
Conditions | Yield |
---|---|
With carbon tetrabromide In 1,2-dichloro-ethane | A 53% B n/a |
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