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13811-71-7

Basic Information
CAS No.: 13811-71-7
Name: (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester
Article Data: 16
Molecular Structure:
Molecular Structure of 13811-71-7 ((2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester)
Formula: C8H14O6
Molecular Weight: 206.196
Synonyms: Butanedioicacid, 2,3-dihydroxy-, diethyl ester, [S-(R*,R*)]- (9CI);Tartaric acid, diethylester, (-)- (8CI);(2S,3S)-Diethyl tartrate;(S,S)-Diethyl tartrate;D-(-)-Diethyl tartrate;D-Tartaric acid diethyl ester;Diethyl (-)-D-tartrate;Diethyl (2S,3S)-(-)-tartrate;Diethyl(S,S)-(-)-tartrate;
EINECS: 237-458-8
Density: 1.262 g/cm3
Melting Point: 17 °C
Boiling Point: 280 °C at 760 mmHg
Flash Point: 93.3 °C
Solubility: insoluble in water
Appearance: Colorless to light yellow liquid
Hazard Symbols: IrritantXiIrritantXi
Risk Codes: 36/37/38
Safety: 24/25-36-26
PSA: 93.06000
LogP: -1.16560
Synthetic route
64-17-5

ethanol

147-71-7

D-tartaric acid

13811-71-7

diethyl (2S,3S)-tartrate

Conditions
ConditionsYield
With thionyl chloride at 20℃;100%
With thionyl chloride at 20℃;100%
With hydrogenchloride In chloroform; water for 60h; Catalytic behavior; Reflux; enantioselective reaction;99.6%

(2S,3S)-2,3-Bis-(2,2,2-trichloro-acetoxy)-succinic acid diethyl ester

13811-71-7

diethyl (2S,3S)-tartrate

Conditions
ConditionsYield
With indium; water; ammonium chloride In methanol for 1h; Heating;89%

(2S,3S)-2,3-Bis-(2,2,2-trichloro-ethoxycarbonyloxy)-succinic acid diethyl ester

13811-71-7

diethyl (2S,3S)-tartrate

Conditions
ConditionsYield
With indium; water; ammonium chloride In methanol for 2h; Heating;85%
136087-36-0

diethyl (4R,5R)-1,3,2-dioxathiolane-4,5-dicarboxylate 2-oxide

13811-71-7

diethyl (2S,3S)-tartrate

Conditions
ConditionsYield
With sodium azide In ethanol; water at 20℃; for 14h;
136087-36-0

diethyl (4R,5R)-1,3,2-dioxathiolane-4,5-dicarboxylate 2-oxide

A

13811-71-7

diethyl (2S,3S)-tartrate

B

101924-53-2

diethyl (2S,3R)-2-azido-3-hydroxysuccinate

C

diethyl (2R,3R)-2-azido-3-hydroxysuccinate

Conditions
ConditionsYield
With sodium azide In water; N,N-dimethyl-formamide at 20℃; for 14h;
57968-71-5

(+/-)-diethyl tartrate

A

13811-71-7

diethyl (2S,3S)-tartrate

B

87-91-2

diethyl (2R,3R)-tartrate

Conditions
ConditionsYield
With (S)-aminopropyl alcohol(at)silica 1 In hexane; isopropyl alcohol at 20℃; for 1h; Purification / work up; Resolution of racemate; Inert atmosphere;A n/a
B n/a
13811-71-7

diethyl (2S,3S)-tartrate

35506-91-3, 133522-25-5, 136087-36-0

diethyl (4S,5S)-1,3,2-dioxathiolane-4,5-dicarboxylate 2-oxide

Conditions
ConditionsYield
With thionyl chloride In tetrachloromethane Heating;100%
With thionyl chloride; triethylamine In dichloromethane for 3h;100%
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 0 - 50℃; for 2.5h;95%
109-87-5

Dimethoxymethane

13811-71-7

diethyl (2S,3S)-tartrate

159593-22-3

diethyl (2S,3S)-2,3-di-O-methoxymethyl-tartrate

Conditions
ConditionsYield
With phosphorus pentoxide In dichloromethane100%
With phosphorus pentoxide In dichloromethane for 3h;100%
With phosphorus pentoxide In chloroform for 2h; Alkylation;84%
With phosphorus pentoxide In dichloromethane
With phosphorus pentoxide In dichloromethane at 0℃; for 10h; Inert atmosphere;
13811-71-7

diethyl (2S,3S)-tartrate

1034-39-5

dibromotriphenylphosphorane

(4S,5S)-2,2,2-Triphenyl-2λ5-[1,3,2]dioxaphospholane-4,5-dicarboxylic acid diethyl ester

Conditions
ConditionsYield
With triethylamine In toluene Cyclization;100%
13811-71-7

diethyl (2S,3S)-tartrate

77-78-1

dimethyl sulfate

21066-69-3

(-)-(2S,3S)-O,O-Dimethylweinsaeure-diethylester

Conditions
ConditionsYield
With sodium hydride In diethyl ether at 0 - 20℃; Inert atmosphere;100%
With sodium hydride In mineral oil at 0 - 20℃; for 12h;82%
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  • (-)-Diethyl D-tartrate

  • Casno:

    13811-71-7

    (-)-Diethyl D-tartrate

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  • Best Quality Diethyl D(-)-Tartrate with good supplier

  • Casno:

    13811-71-7

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    Product name: Diethyl D(-)-Tartrate CAS No.:13811-71-7 Molecule Formula:C8H14O6 Molecule Weight:206.19 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS

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  • Casno:

    13811-71-7

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  • (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester

  • Casno:

    13811-71-7

    (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester

    Min.Order: 1 Gram

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    Product Name: (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester CAS: 13811-71-7 MF: C8H14O6 MW: 206.19 EINECS: 237-458-8 Mol File: 13811-71-7.mol (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester Structure (2S,3S)(-)-D

    SHANGHAI MINSTAR CHEMICAL CO., LTD. is a leading, experienced, professional supplier of API & intermediates, plant extract, food additive, fine chemicals and industry chemicals, et

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     China (Mainland)  |  Contact Details

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  • Diethyl D-tartrate

  • Casno:

    13811-71-7

    Diethyl D-tartrate

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    factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

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  • (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester

  • Casno:

    13811-71-7

    (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester

    Min.Order: 1 Gram

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  • (-)-Diethyl D-tartrate

  • Casno:

    13811-71-7

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  • Casno:

    13811-71-7

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  • (-)-Diethyl D-tartrate

  • Casno:

    13811-71-7

    (-)-Diethyl D-tartrate

    Min.Order: 0

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    Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

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  • SAGECHEM/Diethyl-D-tartrate

  • Casno:

    13811-71-7

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  •  SAGECHEM LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86818502

    Address:5Fl. 501Room, Tower A, New Youth Plaza, 8 Jia Shan Road, Hangzhou, China

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Chemistry

Name : (-)-Diethyl D-tartrate
Synonyms : (-)-Diethyl-2,3-dihydroxysuccinate; (2S,3S)(-)-Dihydroxybutane-1,4-dioic acid diethyl ester
 
Molecular Structure :        
 
Molecular Formula : C8H14O6
Molecular Weight : 206.19
CAS Registry Number : 13811-71-7
EINECS : 237-458-8
Melting point : 17 oC
Boiling point : 280 oC
Flash point : 93 oC
Density : 1.205
Refractive index : 1.445-1.447 
Water solubility : insoluble

Safety Profile

(-)-Diethyl D-tartrate avoid contact with skin or eyes