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14264-16-5

Basic Information
CAS No.: 14264-16-5
Name: Bis(triphenylphosphine)nickel(II)chloride
Article Data: 40
Cas Database
Molecular Structure:
Molecular Structure of 14264-16-5 (Bis(triphenylphosphine)nickel(II)chloride)
Formula: C36H30Cl2NiP2
Molecular Weight: 654.18
Synonyms: Dichloronickel - triphenylphosphine (1:2);nickel(2+) chloride - triphenylphosphane (1:2:2);
EINECS: 238-154-8
Density: N/A
Melting Point: 250 °C (dec.)(lit.)
Boiling Point: 360 °C at 760 mmHg
Flash Point: 181.7 °C
Solubility: insoluble in water
Appearance: dark gray solid
Hazard Symbols: ToxicT
Risk Codes: 45-43-52/53-34-20/21/22
Safety: 53-45-60-36/37/39-26
Transport Information: UN 2923
PSA: 27.18000
LogP: 4.04770
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Chemistry

Molecular Structure:

Molecular Formula: C36H30Cl2NiP2
Molecular Weight: 654.1703
IUPAC Name: 1-Azabicyclo[2.2.2]octan-3-one hydrochloride
Synonyms of Bis(triphenylphosphine)dichloronickel (CAS NO.14264-16-5): EBis(triphenylphosphine)nickel dichloride ; Dichlorobis(triphenylphosphine)nickel ; EINECS 238-154-8 ; NSC 137147 ; Nickel, bis(triphenylphosphine)dichloro- ; Nickel, dichlorobis(triphenylphosphine)- ; Phosphine, tributyl-, compd. with nickelchloride (2:1) ; Bis(triphenylphosphine)nickel(II) chloride
CAS NO: 14264-16-5
Product Categories: Metal Compounds ; Catalysts for Organic Synthesis ; Classes of Metal Compounds ; Homogeneous Catalysts ; Metal Complexes ; Ni (Nickel) Compounds ; Synthetic Organic Chemistry ; Transition Metal Compounds
Melting point: 250 °C 
Freely Rotating Bonds: 3
Polar Surface Area: 13.59 Å2
Flash Point: 181.7 °C
Enthalpy of Vaporization: 58.18 kJ/mol
Boiling Point: 360 °C at 760 mmHg
Vapour Pressure: 4.74E-05 mmHg at 25°C

Uses

 Bis(triphenylphosphine)dichloronickel (CAS NO.14264-16-5) is used as catalyst in the coupling reaction of aryl mesylate salt, allyl carbonate with organic lithium borate.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intravenous 56mg/kg (56mg/kg)   U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#03119,

Consensus Reports

NTP 10th Report on Carcinogens. Reported in EPA TSCA Inventory. Nickel and its compounds are on the Community Right-To-Know List.

Safety Profile

The safety information of Bis(triphenylphosphine)dichloronickel (CAS NO.14264-16-5) is as follows:
Hazard Codes: T
Risk Statements: 45-43-52/53-34-20/21/22
45: May cause cancer
43: May cause sensitization by skin contact
52/53: Harmful to aquatic organisms, may cause long-term adverse effects in the aquatic environment
34: Causes burns
20/21/22: Harmful by inhalation, in contact with skin and if swallowed
Safety Statements: 53-36/37-45-60-36/37/39-26
53: Avoid exposure - obtain special instruction before use
36/37: Wear suitable protective clothing and gloves
45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
60: This material and/or its container must be disposed of as hazardous waste
36/37/39: Wear suitable protective clothing, gloves and eye/face protection
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
RIDADR: 3260
WGK Germany: 3
RTECS: QR6170000
HazardClass: 6.1(b)
PackingGroup: III
F: 21
Confirmed human carcinogen. Poison by intravenous route. See also NICKEL COMPOUNDS. When heated to decomposition it emits very toxic fumes of Cl and POx.

Standards and Recommendations

OSHA PEL: TWA 0.1 mg (Ni)/m3
ACGIH TLV: TWA 0.2 mg(Ni)/m3; Human Carcinogen)

Specification

Storage information of Bis(triphenylphosphine)dichloronickel (CAS NO.14264-16-5):
Store in a cool, dry place. Store in a tightly closed container. Keep under a nitrogen blanket. Corrosives area.