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14316-06-4

Basic Information
CAS No.: 14316-06-4
Name: D-Alanine, methylester, hydrochloride (1:1)
Article Data: 28
Cas Database
Molecular Structure:
Molecular Structure of 14316-06-4 (D-Alanine, methylester, hydrochloride (1:1))
Formula: C4H9NO2.HCl
Molecular Weight: 139.582
Synonyms: Alanine,methyl ester, hydrochloride, D- (8CI);D-Alanine, methyl ester, hydrochloride(9CI);(R)-2-Aminopropionic acid methyl ester hydrochloride;(R)-Alanine methylester hydrochloride;NSC 523192;H-D-Ala-OMe·HCl;
EINECS: 238-258-3
Density: 1.01 g/cm3
Melting Point: 108-110 °C(lit.)
Boiling Point: 101.5 °C at 760 mmHg
Flash Point: N/A
Solubility: Soluble in Water 100 mg/ml.
Appearance: White crystalline powder
Hazard Symbols: IrritantXi
Risk Codes: N/A
Safety: 24/25
Transport Information: N/A
PSA: 40.54000
LogP: 0.43460
Synthetic route
67-56-1

methanol

338-69-2

D-Alanine

14316-06-4

D-alanine methyl ester hydrochloride

Conditions
ConditionsYield
With thionyl chloride at 20℃; for 2h;99%
With thionyl chloride for 8h; Heating;97%
With thionyl chloride95%
912290-10-9

methyl N-p-dimethylaminobenzylidenealaninate

A

2491-20-5

L-alanine methyl ester hydrochloride

B

14316-06-4

D-alanine methyl ester hydrochloride

Conditions
ConditionsYield
With (-)-O,O′-di-pivaloyl-L-tartaric acid; lithium diisopropyl amide Yield given. Yields of byproduct given. Title compound not separated from byproducts;
338-69-2

D-Alanine

74-88-4

methyl iodide

14316-06-4

D-alanine methyl ester hydrochloride

Conditions
ConditionsYield
Stage #1: D-Alanine With thionyl chloride
Stage #2: methyl iodide
338-69-2

D-Alanine

14316-06-4

D-alanine methyl ester hydrochloride

Conditions
ConditionsYield
With thionyl chloride In methanol
338-69-2

D-Alanine

77-76-9

2,2-dimethoxy-propane

14316-06-4

D-alanine methyl ester hydrochloride

Conditions
ConditionsYield
With hydrogenchloride at 20℃;

C4H9NO2*C40H40O8S2*ClH

C40H40O8S2

B

14316-06-4

D-alanine methyl ester hydrochloride

Conditions
ConditionsYield
In dichloromethane at 25℃; Equilibrium constant;
13515-97-4

methyl 2-aminopropanoate monohydrochloride

A

2491-20-5

L-alanine methyl ester hydrochloride

B

14316-06-4

D-alanine methyl ester hydrochloride

Conditions
ConditionsYield
With chiral stationary phase including isopropyl-functionalized CF6 In methanol; acetic acid; triethylamine; acetonitrile at 20℃; Purification / work up;
14316-06-4

D-alanine methyl ester hydrochloride

189060-51-3

(3R,5S)-7-chloro-5-(2,3-dimethoxyphenyl)-1-(3-hydroxy-2,2-dimethylpropyl)-2-oxo-1,2,3,5-tetrahydro-4,1-benzoxazepine-3-acetic acid

383662-15-5

methyl N-[[(3R,5S)-7-chloro-5-(2,3-dimethoxyphenyl)-1-(3-hydroxy-2,2-dimethylpropyl)-2-oxo-1,2,3,5-tetrahydro-4,1-benzoxazepin-3-yl]acetyl]-D-alaninate

Conditions
ConditionsYield
With diethylphosphoryl cyanide; triethylamine In N,N-dimethyl-formamide at 20℃; for 0.5h;100%
14316-06-4

D-alanine methyl ester hydrochloride

19430-76-3

p-bromophenyl phosphorodichloridate

p-bromophenyl methoxyalaninyl phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -70 - 20℃;100%
1352083-27-2

3-cyclohexyl-2-(pyridin-2-yl)-2H-indazole-6-carboxylic acid

14316-06-4

D-alanine methyl ester hydrochloride

1352083-28-3

methyl N-{[3-cyclohexyl-2-(pyridin-2-yl)-2H-indazol-6-yl]carbonyl}-D-alaninate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 17h;100%
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Chemistry

IUPAC Name:methyl (2R)-2-aminopropanoate hydrochloride
Molecular Formula:C4H10ClNO2
Molecular Weight:139.5807 g/mol
Melting Point:108-110 °C(lit.)
alpha:-8°(c=1.6, MeOH)
storage temp.:2-8°C
CAS DataBase Reference:14316-06-4(CAS DataBase Reference)
Synonyms of D-ALANINE METHYL ESTER HCL(14316-06-4):
METHYL D-ALANINATE HYDROCHLORIDE;H-D-ALA-OME HCL;D-2-AMINOPROPIONIC ACID METHYL ESTER HYDROCHLORIDE;D-ALA METHYL ESTER HCL;D-ALANINE METHYL ESTER HCL;D-ALANINE METHYL ESTER HYDROCHLORIDE;D-ALANINE METHYL ESTER HYDROCHLORIDE SALT;D-ALANINE-OME HCL
Categories of D-ALANINE METHYL ESTER HCL(14316-06-4):
Amino Acids Derivatives;Amino Acids;Alanine [Ala, A];Amino Acids and Derivatives;Amino Acid Methyl Esters;Amino Acids (C-Protected);Biochemistry;Amino hydrochloride;Alanine;Amino Acid Derivatives;Peptide Synthesis

Uses

D-ALANINE METHYL ESTER HCL(14316-06-4) is used as a pharmaceutical intermediate and raw  material of fine chemicals.

Safety Profile

Safety Information of D-ALANINE METHYL ESTER HCL(14316-06-4):
Hazard Codes:Xi 
WGK Germany:3