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14387-18-9

Basic Information
CAS No.: 14387-18-9
Name: 3-CYANO-3-PHENYLPROPANOIC ACID
Article Data: 10
Molecular Structure:
Molecular Structure of 14387-18-9 (3-CYANO-3-PHENYLPROPANOIC ACID)
Formula: C10H9 N O2
Molecular Weight: 175.187
Synonyms: Hydrocinnamicacid, b-cyano- (8CI); (?à)-3-Cyano-3-phenylpropionic acid
Density: 1.216±0.06 g/cm3(Predicted)
Melting Point: 75 °C(Solv: benzene (71-43-2))
Boiling Point: 336.5±30.0 °C(Predicted)
PSA: 61.09000
LogP: 1.76848
Synthetic route
140-29-4

phenylacetonitrile

79-11-8

chloroacetic acid

14387-18-9

3-cyano-3-phenyl propionic acid

Conditions
ConditionsYield
Stage #1: chloroacetic acid With potassium carbonate In N,N-dimethyl-formamide
Stage #2: phenylacetonitrile With potassium hydroxide In N,N-dimethyl-formamide at 20 - 25℃; for 2h;
81%
64-17-5

ethanol

151-50-8

potassium cyanide

5292-53-5

diethyl benzalmalonate

14387-18-9

3-cyano-3-phenyl propionic acid

151-50-8

potassium cyanide

5292-53-5

diethyl benzalmalonate

14387-18-9

3-cyano-3-phenyl propionic acid

(+-)-2-phenyl-2-cyano-succinic acid diethyl ester

(+-)-2-phenyl-2-cyano-succinic acid diethyl ester

14387-18-9

3-cyano-3-phenyl propionic acid

Conditions
ConditionsYield
With potassium hydroxide
(+-)-phenylsuccinyl chloride

(+-)-phenylsuccinyl chloride

14387-18-9

3-cyano-3-phenyl propionic acid

Conditions
ConditionsYield
With ammonium hydroxide
14025-83-3

3-cyano-3-phenylpropanoic acid ethyl ester

KOH-solution

KOH-solution

14387-18-9

3-cyano-3-phenyl propionic acid

64-17-5

ethanol

185067-05-4

ethyl 2-carbethoxy-3-cyano-3-phenylpropionate

barium hydroxide

barium hydroxide

A

124-38-9

carbon dioxide

B

14387-18-9

3-cyano-3-phenyl propionic acid

aqueous DMF

aqueous DMF

4192-77-2

ethyl cinnamate

14387-18-9

3-cyano-3-phenyl propionic acid

Conditions
ConditionsYield
With sodium hydroxide; ammonium chloride In diethyl ether; ethanol
584-45-2

2-benzylidenemalonic acid

dicyclohexylammonium salt

dicyclohexylammonium salt

101-83-7

N-cyclohexyl-cyclohexanamine

14387-18-9

3-cyano-3-phenyl propionic acid

Conditions
ConditionsYield
In methanol; ethanol; water; ethyl acetate
14387-18-9

3-cyano-3-phenyl propionic acid

A

635-51-8, 10424-29-0

2-phenylsuccinic acid

B

140-10-3

(E)-3-phenylacrylic acid

Conditions
ConditionsYield
With potassium hydroxide; water
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