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14657-64-8

Basic Information
CAS No.: 14657-64-8
Name: Propanoic acid,3-(hydroxyphenylphosphinyl)-
Molecular Structure:
Molecular Structure of 14657-64-8 (Propanoic acid,3-(hydroxyphenylphosphinyl)-)
Formula: C9H11O4P
Molecular Weight: 214.16
Synonyms: Propionicacid, 3-(hydroxyphenylphosphinyl)- (8CI);2-Carboxyethyl(phenyl)phosphinicacid;3-(Hydroxyphenylphosphinyl)propanoic acid;3-(Phenylphosphinyl)propionic acid;H 205;H 205 (flame retardant);Hiretar 205;Phosgard PF 100;2-Carboxyethylphenylphosphinic acid;CEPPA;
EINECS: 411-200-6
Density: 1.358 g/cm3
Melting Point: 152oC
Boiling Point: 526.605 °C at 760 mmHg
Flash Point: 272.281 °C
Solubility:
Appearance: white powder
Hazard Symbols: IrritantXi
Risk Codes: 41
Safety: 26-39
Transport Information:
PSA: 84.41000
LogP: 1.05700
Synthetic route
644-97-3

Dichlorophenylphosphine

79-10-7

acrylic acid

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
Stage #1: Dichlorophenylphosphine; acrylic acid at 80 - 110℃; for 3h;
Stage #2: With water at 90℃; for 3h; Temperature; Concentration;
98%
With acetic anhydride96.8%
94.2%
14576-56-8

butyl 3-[butoxy(phenyl)phosphinyl]propionate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
With sulfuric acid In water97.2%
2071-68-3

3-(chlorophenylphosphinyl)-propionyl chloride

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
With water In acetone for 0.5h; Heating;92.6%
With water
857470-46-3

(2-cyano-ethyl)-phenyl-phosphinic acid butyl ester

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
With hydrogenchloride
202477-16-5

3-(butoxy-phenyl-phosphinoyl)-propionic acid methyl ester

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
With hydrogenchloride
644-97-3

Dichlorophenylphosphine

μ.μ-bis-diphenylacetylene-bis-Fe-Fe)

μ.μ-bis-diphenylacetylene-bis-Fe-Fe)

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 95.6 percent / 1.) -10 deg C, 2 h, 2.) 0 deg C, 1 h
2: 92.6 percent / water / acetone / 0.5 h / Heating
View Scheme
6172-81-2

butyl phenylphosphinate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium
2: aqueous HCl
View Scheme
Multi-step reaction with 2 steps
1: sodium
2: aqueous HCl
View Scheme
Multi-step reaction with 2 steps
1: sodium; benzene
2: aqueous HCl
View Scheme
644-97-3

Dichlorophenylphosphine

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
2: sodium
3: aqueous HCl
View Scheme
Multi-step reaction with 3 steps
2: sodium
3: aqueous HCl
View Scheme
Multi-step reaction with 3 steps
2: sodium; benzene
3: aqueous HCl
View Scheme
Multi-step reaction with 2 steps
2: H2O
View Scheme

hydroxyethyl 3-[hydroxy(phenyl)phosphinyl]propionate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

556-52-5

oxiranyl-methanol

C15H23O8P

Conditions
ConditionsYield
In ethanol at 50℃; for 8.5h;98%
124-09-4

1,6-Hexanediamine

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

(3-((6-aminohexyl)amino)-3-oxopropyl)(phenyl)phosphinic acid

Conditions
ConditionsYield
In ethanol at 0 - 70℃; for 4h;96.78%
108-78-1

2,4,6-triamino-s-triazine

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

C12H15N6O3P

Conditions
ConditionsYield
In water at 20 - 70℃;93%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

13317-44-7

ethyl(phenyl)phosphinic acid

Conditions
ConditionsYield
With sodium hydroxide In water at 50℃; for 40h; pH=3 - 4; Temperature; pH-value; Concentration;92.8%

aqueous cadmium chloride

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

2C9H9O4P(2-)*2HO(1-)*3Cd(2+)

Conditions
ConditionsYield
With triethylamine at 160℃; for 72h; pH=5; Autoclave; High pressure;87%

manganese(II) sulfate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

2C9H10O4P(1-)*Mn(2+)

Conditions
ConditionsYield
In water at 120℃; for 48h; Autoclave; High pressure;82%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

lead(II) chloride

[Pb(2-carboxyethyl(phenyl)phosphinate)2]

Conditions
ConditionsYield
In water High Pressure; mixt. PbCl2 and 2-carboxyethyl(phenyl)phosphinic acid in water in Parr Teflon-lined autoclave was heated at 150°C for 3 days; elem. anal.;81%
66-71-7

1,10-Phenanthroline

cadmium(II) nitrate tetrhydrate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

1428102-03-7

C9H9O4P(2-)*Cd(2+)*C12H8N2

Conditions
ConditionsYield
With urea In water at 150℃; for 72h; pH=7; Autoclave;81%
66-71-7

1,10-Phenanthroline

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

6046-93-1

copper(II) acetate monohydrate

C9H9O4P(2-)*Cu(2+)*4H2O*C12H8N2

Conditions
ConditionsYield
at 80 - 90℃; pH=4;78%
66-71-7

1,10-Phenanthroline

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

5743-04-4

cadmium(II) acetate dihydrate

3C9H9O4P(2-)*3Cd(2+)*3C12H8N2*6.5H2O

Conditions
ConditionsYield
at 80 - 90℃; pH=5;72%
108-78-1

2,4,6-triamino-s-triazine

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

melaminium (2-carboxyethyl)(phenyl)phosphinate monohydrate

Conditions
ConditionsYield
With water at 20℃; Heating;70%
66-71-7

1,10-Phenanthroline

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

6156-78-1

manganese (II) acetate tetrahydrate

1428102-00-4

C9H9O4P(2-)*Mn(2+)*H2O*C12H8N2

Conditions
ConditionsYield
With urea at 110℃; for 72h; pH=6; Autoclave;70%
69506-86-1

1,1'-(1,4-butanediyl)bis(imidazole)

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

5970-45-6

zinc(II) acetate dihydrate

[Zn(1,4-bis(1H-imidazol-1-yl)butane)0.5(2-carboxyethyl(phenyl)phosphinate)]n

Conditions
ConditionsYield
Stage #1: 1,1'-(1,4-butanediyl)bis(imidazole); 3-[hydroxy(phenyl)phosphinyl]propionic acid; zinc(II) acetate dihydrate With air In water at 20℃; for 0.5h;
Stage #2: In water at 150℃; for 96h; Concentration; High pressure;
70%

aqueous cadmium chloride

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

2C9H9O4P(2-)*2H(1+)*Cd(2+)

Conditions
ConditionsYield
In water at 160℃; for 72h; Autoclave; High pressure;68%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

{NaH(Ph-PO2-C2H4-COOH)2}∞

Conditions
ConditionsYield
With sodium hydroxide In water at 20℃; for 0.166667h;66%
553-26-4

4,4'-bipyridine

zinc(II) nitrate hexahydrate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

0.5C10H8N2*C9H9O4P(2-)*Zn(2+)

Conditions
ConditionsYield
With sodium hydroxide In ethanol; water at 140℃; for 48h; pH=Ca. 6; Autoclave; High pressure;65%
66-71-7

1,10-Phenanthroline

cadmium(II) nitrate tetrhydrate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

C9H9O4P(2-)*Cd(2+)*C12H8N2*3H2O

Conditions
ConditionsYield
at 150℃; for 72h; pH=4; Autoclave;61%
288-32-4

1H-imidazole

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

uranyl(VI) acetate dihydrate

Co(imidazole)2(UO2)3((2-carboxyethyl)(phenyl)phosphinic acid(-2H))4

Conditions
ConditionsYield
In water at 160℃; for 72h; pH=4 - 5; Autoclave; High pressure;61%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

uranyl(VI) acetate dihydrate

25372-07-0

1,4-bis-(1H-imidazol-1-yl)benzene

[Ni(1,4-di(1H-imidazol-1-yl)benzene)2(H2O)2][(UO2)3((2-carboxyethyl)(phenyl)phosphinic acid(-2H))4]·2H2O

Conditions
ConditionsYield
With ammonium hydroxide at 160℃; for 72h; pH=3.5 - 4.5; Autoclave; High pressure;61%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

{[KH(Ph-PO2-C2H4-COOH)2]·H2O}∞

Conditions
ConditionsYield
With potassium hydroxide In water at 20℃; for 0.166667h;60%
66-71-7

1,10-Phenanthroline

zinc(II) nitrate hexahydrate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

Zn(2-carboxyethyl(phenyl)phosphinate)(1,10-phenanthroline)*5H2O

Conditions
ConditionsYield
With sodium hydroxide In water at 150℃; for 73h; pH=5; Autoclave;60%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

uranyl(VI) acetate dihydrate

25372-07-0

1,4-bis-(1H-imidazol-1-yl)benzene

[Co(1,4-di(1H-imidazol-1-yl)benzene)2(H2O)2][(UO2)3((2-carboxyethyl)(phenyl)phosphinic acid(-2H))4]·2H2O

Conditions
ConditionsYield
With ammonium hydroxide at 160℃; for 72h; pH=3.5 - 5; Autoclave; High pressure;59%
66-71-7

1,10-Phenanthroline

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

6156-78-1

manganese (II) acetate tetrahydrate

C9H9O4P(2-)*Mn(2+)*3H2O*C12H8N2

Conditions
ConditionsYield
at 20℃; for 24h; pH=5;56%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

uranyl(VI) acetate dihydrate

25372-07-0

1,4-bis-(1H-imidazol-1-yl)benzene

Mn(1,4-di(1H-imidazol-1-yl)benzene)(UO2)2((2-carboxyethyl)(phenyl)phosphinic acid(-2H))3

Conditions
ConditionsYield
With ammonium hydroxide In water at 160℃; for 72h; pH=4 - 6; Autoclave; High pressure;51%
14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

C9H9O4P(2-)*Li(1+)*H(1+)

Conditions
ConditionsYield
With lithium hydroxide In water at 50℃;45%
66-71-7

1,10-Phenanthroline

cadmium(II) acetate monohydrate

14657-64-8

3-[hydroxy(phenyl)phosphinyl]propionic acid

C42H38Cd2N4O10P2*2H2O

Conditions
ConditionsYield
at 20℃; for 48h;45%
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    Chemical Name:3-Hydroxyphenylphosphinyl-propanoic acid (CEPPA) CAS 14657-64-8 CAS: 14657-64-8 Molecular Fomula: C9H11O4P Molecular weight: 214.15 Appearance: White powder Assay: 99%min Appearance: white powder Storage:Store in cool and

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  • 3-Hydroxyphenylphosphinyl-propanoic acid CAS NO.14657-64-8

  • Casno:

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    3-Hydroxyphenylphosphinyl-propanoic acid CAS NO.14657-64-8

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    3-Hydroxyphenylphosphinyl-propanoic acid 14657-64-8

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  • Propanoic acid,3-(hydroxyphenylphosphinyl)- 14657-64-8

  • Casno:

    14657-64-8

    Propanoic acid,3-(hydroxyphenylphosphinyl)- 14657-64-8

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  • 3-Hydroxyphenylphosphinyl-propanoic acid with CAS:	14657-64-8

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    Product name: 3-Hydroxyphenylphosphinyl-Propanoic Acid CAS No.:14657-64-8 Molecule Formula:C9H11O4P Molecule Weight:214.16 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard

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Specification

The 3-Hydroxyphenylphosphinyl-propanoic acid, with the CAS registry number 14657-64-8, is also known as 2-Carboxyethyl(phenyl)phosphinic acid. It belongs to the product category of Flame retardant. This chemical's molecular formula is C9H11O4P and molecular weight is 214.16. What's more, its systematic name is 3-[Hydroxy(phenyl)phosphoryl]propanoic acid.

Physical properties of 3-Hydroxyphenylphosphinyl-propanoic acid are: (1)ACD/LogP: -0.331; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -4.29; (4)ACD/LogD (pH 7.4): -5.07; (5)ACD/BCF (pH 5.5): 1.00; (6)ACD/BCF (pH 7.4): 1.00; (7)ACD/KOC (pH 5.5): 1.00; (8)ACD/KOC (pH 7.4): 1.00; (9)#H bond acceptors: 4; (10)#H bond donors: 2; (11)#Freely Rotating Bonds: 4; (12)Polar Surface Area: 84.41 Å2; (13)Index of Refraction: 1.554; (14)Molar Refractivity: 50.567 cm3; (15)Molar Volume: 157.658 cm3; (16)Polarizability: 20.046×10-24cm3; (17)Surface Tension: 57.6 dyne/cm; (18)Density: 1.358 g/cm3; (19)Flash Point: 272.281 °C; (20)Enthalpy of Vaporization: 84.319 kJ/mol; (21)Boiling Point: 526.605 °C at 760 mmHg; (22)Vapour Pressure: 0 mmHg at 25°C.

When you are using this chemical, please be cautious about it as the following:
This chemical has a risk of serious damage to eyes. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. When using it, you need wear suitable protective eye/face protection.

You can still convert the following datas into molecular structure:
(1)SMILES: O=P(O)(c1ccccc1)CCC(=O)O
(2)Std. InChI: InChI=1S/C9H11O4P/c10-9(11)6-7-14(12,13)8-4-2-1-3-5-8/h1-5H,6-7H2,(H,10,11)(H,12,13)
(3)Std. InChIKey: MORLYCDUFHDZKO-UHFFFAOYSA-N