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15106-62-4

Basic Information
CAS No.: 15106-62-4
Name: 3,5-Dichloro-L-tyrosine
Article Data: 8
Molecular Structure:
Molecular Structure of 15106-62-4 (3,5-Dichloro-L-tyrosine)
Formula: C9H9Cl2NO3
Molecular Weight: 250.081
Synonyms: Dichlorotyrosine;NSC 210501;Tyrosine,3,5-dichloro-, L- (8CI);3,5-Dichloro-L-tyrosine;3,5-Dichlorotyrosine;
Density: 1.565 g/cm3
Boiling Point: 392.507 °C at 760 mmHg
Flash Point: 191.182 °C
PSA: 83.55000
LogP: 2.35370
Synthetic route
127526-66-3

3,5-dichloro-L-tyrosine methyl ester

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran; methanol; water at 20℃; for 24h;100%
With potassium carbonate In tetrahydrofuran; methanol; water at 20℃; for 24h;100%

(S)-4-(3,5-Dichloro-4-hydroxy-benzyl)-5-oxo-oxazolidine-3-carboxylic acid benzyl ester

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
With boron trichloride In dichloromethane at 25℃; for 0.333333h;74%

(S)-2-Benzyloxycarbonylamino-3-(3,5-dichloro-4-hydroxy-phenyl)-propionic acid

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
With boron trichloride In dichloromethane at 25℃; for 0.333333h;45%
60-18-4

L-tyrosine

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
With chlorine; acetic acid
With sulfuryl dichloride In acetic acid for 5h; Ambient temperature;
With chlorine In methanol Sealed tube;
Multi-step reaction with 3 steps
1: thionyl chloride / 24 h / 70 °C
2: N-chloro-succinimide / methanol / 24 h / 20 °C
3: potassium carbonate / methanol; tetrahydrofuran; water / 24 h / 20 °C
View Scheme
7782-50-5

chlorine

60-18-4

L-tyrosine

64-19-7

acetic acid

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

5-<3.5-dichloro-4-oxy-benzyl>-hydantoin

5-<3.5-dichloro-4-oxy-benzyl>-hydantoin

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
With barium dihydroxide
205866-50-8

(S)-3-benzyloxycarbonyl-4-(4-hydroxyphenyl)methyloxazolidin-5-one

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuryl chlorid
2: 74 percent / BCl3 / CH2Cl2 / 0.33 h / 25 °C
View Scheme

methyl (S)-3-(3,5-dichloro-4-hydroxyphenyl)-2-((tert-butoxycarbonyl)amino) propanoate

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 24 h / 0 - 20 °C
2: potassium carbonate / methanol; water; tetrahydrofuran / 24 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 24 h / 20 °C
2: potassium carbonate / methanol; tetrahydrofuran; water / 24 h / 20 °C
View Scheme
3417-91-2

L-tyrosine methyl ester HCl

15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N-chloro-succinimide / methanol / 24 h / 20 °C
2: potassium carbonate / methanol; tetrahydrofuran; water / 24 h / 20 °C
View Scheme
15106-62-4

(S)-2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

3387-87-9

2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid

Conditions
ConditionsYield
With sodium hydroxide
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  • 3,5-Dichloro-L-tyrosine  CAS NO.15106-62-4

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  • 3,5-Dichloro-L-tyrosine15106-62-4

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  • L-Tyrosine,3,5-dichloro-

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  • (S)-2-amino-3-(3,5-difluoro-4-hydroxyphenyl)propanoic acid

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  • L-Tyrosine,3,5-dichloro-

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    15106-62-4

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Specification

The L-Tyrosine,3,5-dichloro- is an organic compound with the formula C9H9Cl2NO3. The IUPAC name of this chemical is 2-amino-3-(3,5-dichloro-4-hydroxyphenyl)propanoic acid. With the CAS registry number 15106-62-4, it is also named as 3,5-Dichloro-L-tyrosine.

Physical properties about L-Tyrosine,3,5-dichloro- are: (1)ACD/LogP: 1.50; (2)#H bond acceptors: 4; (3)#H bond donors: 4; (4)#Freely Rotating Bonds: 5; (5)Polar Surface Area: 38.77 Å2; (6)Index of Refraction: 1.634; (7)Molar Refractivity: 57.16 cm3; (8)Molar Volume: 159.7 cm3; (9)Polarizability: 22.6×10-24cm3; (10)Surface Tension: 67.8 dyne/cm; (11)Density: 1.565 g/cm3; (12)Flash Point: 191.2 °C; (13)Enthalpy of Vaporization: 67.74 kJ/mol; (14)Boiling Point: 392.5 °C at 760 mmHg; (15)Vapour Pressure: 7.27E-07 mmHg at 25°C.

You can still convert the following datas into molecular structure:
(1)SMILES: Clc1cc(cc(Cl)c1O)C[C@@H](C(=O)O)N
(2)InChI: InChI=1/C9H9Cl2NO3/c10-5-1-4(2-6(11)8(5)13)3-7(12)9(14)15/h1-2,7,13H,3,12H2,(H,14,15)/t7-/m0/s1
(3)InChIKey: MPHURJQUHZHALJ-ZETCQYMHBY
(4)Std. InChI: InChI=1S/C9H9Cl2NO3/c10-5-1-4(2-6(11)8(5)13)3-7(12)9(14)15/h1-2,7,13H,3,12H2,(H,14,15)/t7-/m0/s1
(5)Std. InChIKey: MPHURJQUHZHALJ-ZETCQYMHSA-N