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152305-23-2

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Basic Information
CAS No.: 152305-23-2
Name: (S)-4-(4-Aminobenzyl)-2(1H)-oxazolidinone
Article Data: 6
Molecular Structure:
Molecular Structure of 152305-23-2 ((S)-4-(4-Aminobenzyl)-2(1H)-oxazolidinone)
Formula: C10H12N2O2
Molecular Weight: 192.217
Synonyms: 2-Oxazolidinone,4-[(4-aminophenyl)methyl]-, (S)-;(4S)-4-(4-Aminobenzyl)-1,3-oxazolidin-2-one;(S)-4-(4-Aminobenzyl)-2-oxazolidinone;
Density: 1.257 g/cm3
Melting Point: 107-111 °C
Boiling Point: 479.7 °C at 760 mmHg
Flash Point: 243.9 °C
Appearance: white crystalline powder
Hazard Symbols: HarmfulXn
Risk Codes: 22-36/37/38
Safety: 26-36/37
PSA: 64.35000
LogP: 1.82970
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152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethanol under 760 Torr; Ambient temperature;79%
With indium; ammonium chloride In ethanol for 4h; Heating;47%
With hydrogen; nickel In methanol at 30℃; for 6 - 7h;
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152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
potassium carbonate at 115 - 135℃; for 2.5h;75%
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(S)-4-Benzyl-2-oxazolidinone

MeX

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152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 65 percent / fuming HNO3 / CH2Cl2 / 2 h / 20 °C
2: 47 percent / NH4Cl; In / ethanol / 4 h / Heating
View Scheme
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L-phenylalanine

PhMgHal

PhMgHal

152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 53 percent / conc. H2SO4, conc. HNO3 / 0.5 h / Ambient temperature
2: 76 percent / SOCl2 / 4 h / -10 - 40 °C
3: 65 percent / NaBH4 / ethanol; H2O / 4 h / Heating
4: 75 percent / 0.2M aq. KOH / toluene / 2 h / 0 - 20 °C
5: 79 percent / H2, aq. HCl / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature
View Scheme
949-99-5

4-nitro-3-phenyl-L-alanine

152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 76 percent / SOCl2 / 4 h / -10 - 40 °C
2: 65 percent / NaBH4 / ethanol; H2O / 4 h / Heating
3: 75 percent / 0.2M aq. KOH / toluene / 2 h / 0 - 20 °C
4: 79 percent / H2, aq. HCl / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature
View Scheme
89288-22-2

(S)-(-)-2-amino-3-(4-nitrophenyl)propan-1-ol

152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 75 percent / 0.2M aq. KOH / toluene / 2 h / 0 - 20 °C
2: 79 percent / H2, aq. HCl / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature
View Scheme
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(S)-4-nitrophenylalanine methyl ester hydrochloride

152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 65 percent / NaBH4 / ethanol; H2O / 4 h / Heating
2: 75 percent / 0.2M aq. KOH / toluene / 2 h / 0 - 20 °C
3: 79 percent / H2, aq. HCl / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature
View Scheme
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(S)-N-butoxycarbonyl-4-aminophenylalaninol

152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

Conditions
ConditionsYield
With sodium methylate In methanol; butan-1-ol at 5 - 85℃; for 8.5h;
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4-iodophenyl isothiocyanate

152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

(S)-1-(4-iodophenyl)-3-(4-((2-oxooxazolidin-4-yl)methyl)phenyl)-thiourea

Conditions
ConditionsYield
With triethylamine In acetone Reflux;90%
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1-isothiocyanato-4-methylbenzene

152305-23-2

(S)-4-(4-aminobenzyl)-1,3-oxazolidin-2-one

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Conditions
ConditionsYield
With triethylamine In acetone Reflux;88%
Raw Materials
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Chemistry

Product Name: 2-Oxazolidinone,4-[(4-aminophenyl)methyl]-, (4S)- (CAS NO.152305-23-2)


Molecular Formula: C10H12N2O2
Molecular Weight: 192.21g/mol
Mol File: 152305-23-2.mol
Melting Point: 107-111 °C
H bond acceptors: 4
H bond donors: 3
Freely Rotating Bonds: 3
Polar Surface Area: 64.35Å2
Index of Refraction: 1.6
Molar Refractivity: 52.322 cm3
Molar Volume: 152.871 cm3
Surface Tension: 53.826 dyne/cm
Boiling point: 479.7 °C at 760 mmHg
Flash Point: 243.9 °C
Density: 1.257 g/cm3
Surface Tension: 53.8 dyne/cm
Enthalpy of Vaporization: 74.4 kJ/mol
Vapour Pressure: 2.32E-09 mmHg at 25°C
Product Categories: chiral; Chiral Reagents; Asymmetric Synthesis; Chiral Building Blocks; Glycidyl Compounds, etc. (Chiral); Synthetic Organic Chemistry; Intermediates & Fine Chemicals; Pharmaceuticals; API's

Safety Profile

Safety Information of 2-Oxazolidinone,4-[(4-aminophenyl)methyl]-, (4S)- (CAS NO.152305-23-2):
Hazard Codes: XnHarmful
Risk Statements: 22-36/37/38 
22:  Harmful if swallowed 
36:  Irritating to the eyes 
37:  Irritating to the respiratory system 
38:  Irritating to the skin 
Safety Statements: 26-36/37
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing  
37:  Wear suitable gloves 
WGK Germany: 2

Specification

 2-Oxazolidinone,4-[(4-aminophenyl)methyl]-, (4S)- , its CAS NO. is 152305-23-2, the synonyms are (4s)-4-[(4-Aminophenyl)methyl]-2-oxazolidinone ; (s)-4-(4'-Aminobenzyl)-1,3-oxazolidin-2-one ; (s)-4-(4-Aminobenzyl)-1,3-oxazolidin-2-one ; (s)-4-(4-Aminobenzyl)-2(1h)-oxazolidinone ; (s)-4-(4'-Aminobenzyl)-2-oxazolidinone ; (s)-4-(4-Aminobenzyl)-2-oxazolidinone ; (s)-4-(4-Amino-benzyl)-oxazolidin-2-one ; (s)-4-(4-Amino-benzyl)-oxazolidine-2-one .