CAS No.156028-26-1,1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride Suppliers

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Basic Information

Molecular Structure:
CAS No.:	156028-26-1
Name:	1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride
Article Data:	26

Formula:	C₂₄H₄Cl₄O₆
Molecular Weight:	530.104
Synonyms:	1,6,7,12-Tetrachloro-3,4:9,10-perylenetetracarboxylicdianhydride;1,6,7,12-Tetrachloroperylene-3,4:9,10-tetracarboxylic aciddianhydride;1,6,7,12-Tetrachloroperylene-3,4:9,10-tetracarboxylic dianhydride;5,6,12,13-Tetrachloroperylenetetracarboxylic dianhydride;Perylo[3,4-cd:9,10-c'd']dipyran-1,3,8,10-tetrone,5,6,12,13-tetrachloro-;
EINECS:	937-421-2
Density:	1.962 g/cm³
Boiling Point:	757.1 °C at 760 mmHg
Flash Point:	287.5 °C
PSA:	86.74000
LogP:	6.97200

Synthetic route

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions

Conditions	Yield
With sulfuric acid; chlorine at 120℃;	99%
With chlorosulfonic acid; iodine at 65℃; for 20h;	98%
With chlorosulfonic acid; iodine at 65℃; for 20h;	94%

: tetrabutyl 1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxylate

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In chlorobenzene for 48h; Reflux;	87%

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A: C24H5Cl3O6

B: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions

Conditions	Yield
With chlorosulfonic acid; iodine at 70℃; for 5h;
With chlorosulfonic acid; iodine at 60℃; for 20h;	A 35 %Spectr. B 65 %Spectr.

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A: 1,2,6,7,12-pentachloroperylene-3,4,9,10-tetracarboxylic acid bisanhydride

B: C24H2Cl6O6

C: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions

Conditions	Yield
With chlorosulfonic acid; iodine at 70℃; for 20h;

...Expand

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A: 1,2,6,7,12-pentachloroperylene-3,4,9,10-tetracarboxylic acid bisanhydride

B: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions

Conditions	Yield
With chlorosulfonic acid; iodine at 70℃; for 10h;
With chlorosulfonic acid; iodine at 70℃; for 20h; Temperature; Time;	A 20 %Spectr. B 80 %Spectr.
With chlorosulfonic acid; iodine at 60℃; for 15h; Temperature; Time; Overall yield = 98 %;

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A: C24H5Cl3O6

B: 1,2,6,7,12-pentachloroperylene-3,4,9,10-tetracarboxylic acid bisanhydride

C: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions

Conditions	Yield
With chlorosulfonic acid; iodine at 65℃; for 20h;	A 9 %Spectr. B 7 %Spectr. C 84 %Spectr.

...Expand

: 108-91-8
cyclohexylamine

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

: 156028-27-2
N,N’-dicyclohexyl-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid bisimide

Conditions

Conditions	Yield
With acetic acid In 1-methyl-pyrrolidin-2-one at 90℃; for 11h;	100%
With 1-methyl-pyrrolidin-2-one; acetic acid at 85℃; for 8h; Inert atmosphere;	92%
at 135℃; for 24h; Inert atmosphere;	90%

: 2450-71-7
Propargylamine

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

: 1419865-47-6
N,N’-bis-propargyl-1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxylic diimide

Conditions

Conditions	Yield
In isopropyl alcohol at 90℃;	100%
In isopropyl alcohol for 24h; Reflux; Inert atmosphere;	52.8%
In isopropyl alcohol Reflux;

: 107-10-8
propylamine

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

: N,N'-bis-n-propyl-1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxdiimide

Conditions

Conditions	Yield
In water; butan-1-ol for 8h;	99%
In water; isopropyl alcohol at 65℃; for 9h; Temperature; Inert atmosphere;

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

: 2-(3,4,5-tris(dodec-1-yloxy)phenyl)ethylamine

: C112H166Cl4N2O10

Conditions

Conditions	Yield
With quinoline; zinc(II) acetate dihydrate at 180℃; for 5h; Inert atmosphere;	98%

Raw Materials

128-69-8

Downstream Products

156028-30-7

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Chemistry

Empirical Formula: C₂₄H₄Cl₄O₆
Molecular Weight: 530.097g/mol
Structure of 1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride (CAS NO.156028-26-1):

Index of Refraction: 1.931
Molar Refractivity: 128.74 cm³
Molar Volume: 270.1 cm³
Polarizability: 51.03×10^-24cm³
Surface Tension: 103 dyne/cm
Density: 1.962 g/cm³
Flash Point: 287.5 °C
Enthalpy of Vaporization: 110.3 kJ/mol
Boiling Point: 757.1 °C at 760 mmHg
Vapour Pressure: 8.19E-23 mmHg at 25 °C
SMILES: c1c2c3c(cc(c4c3c(c1Cl)c5c(cc6c7c5c4c(cc7C(=O)OC6=O)Cl)Cl)Cl)C(=O)OC2=O
InChI: InChI=1/C24H4Cl4O6/c25-9-1-5-13-6(22(30)33-21(5)29)2-11(27)17-18-12(28)4-8-14-7(23(31)34-24(8)32)3-10(26)16(20(14)18)15(9)19(13)17/h1-4H
InChIKey: YGRXZLAMYLGXMF-UHFFFAOYAS

Specification

1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride , its cas register number is 156028-26-1. It also can be called 5,6,12,13-Tetrachloroisochromeno[4',5',6':6,5,10]anthra[2,1,9-def]isochromene-1,3,8,10-tetrone ; Peryleno[10,9-cd:3,4-c'd']dipyran-1,3,8,10-tetrone, 5,6,12,13-tetrachloro- .