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| CAS No.: | 1564-64-3 |
|---|---|
| Name: | 9-Bromoanthracene |
| Article Data: | 66 |
| Molecular Structure: | |
|
|
|
| Formula: | C14H9Br |
| Molecular Weight: | 257.129 |
| Synonyms: | 10-Bromoanthracene;9-Anthracenyl bromide;9-Anthracyl bromide;Anthracene,9-bromo-;NSC 803;9-Bromo anthracene; |
| EINECS: | 216-359-3 |
| Density: | 1.479 g/cm3 |
| Melting Point: | 97-100 °C(lit.) |
| Boiling Point: | 389.7 °C at 760 mmHg |
| Flash Point: | 190.3 °C |
| Solubility: | Insoluble in water. |
| Appearance: | white to light yellow crystal powder |
| Hazard Symbols: |
 Xi
|
| Safety: | 22-24/25 |
| PSA: | 0.00000 |
| LogP: | 4.75550 |
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| Conditions | Yield |
|---|---|
| With bis(trifluoroacetoxy)iodobencene; trimethylsilyl bromide In dichloromethane at 20℃; Inert atmosphere; | 100% |
| With N,N,N’,N’-tetrabromobenzene-1,3-disulfonamide In dichloromethane at 25℃; for 0.583333h; | 98% |
| With copper(ll) bromide In chloroform Reflux; | 94% |
- 641144-16-3
(10-bromo-9-anthracenyl)boronic acid
- 1564-64-3
9-Bromoanthracene
| Conditions | Yield |
|---|---|
| With [Pd(N-phenylbenzaldimine)(OAc)(PPh3)] In tetrahydrofuran at 20℃; for 24h; Schlenk technique; chemoselective reaction; | 99% |
| Conditions | Yield |
|---|---|
| With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; acetic acid for 0.7h; Irradiation; Inert atmosphere; | A 94% B 2% |
- 22362-86-3
9-iodoanthracene
- 1564-64-3
9-Bromoanthracene
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 25℃; for 3h; Reagent/catalyst; Time; Temperature; | 92% |
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; 2,4,6-trimethylaniline In dichloromethane at 0℃; for 8h; Inert atmosphere; regioselective reaction; | A 84% B 7% |
| With N-Bromosuccinimide; C5H13NO3S In n-heptane at 60℃; for 4.5h; Darkness; | A 81% B 8% |
| With N-Bromosuccinimide; iodine In tetrachloromethane Bromination; Heating; |
- 523-27-3
9,10-Dibromoanthracene
A
- 1564-64-3
9-Bromoanthracene
B
- 25882-75-1
9-<4-(N,N-dimethylamino)phenyl>-9,10-dihydroanthracene
C
- 101-61-1
4,4'-methylene-bis(N,N-dimethylaniline)
| Conditions | Yield |
|---|---|
| With N,N-dimethyl-aniline In acetonitrile Irradiation; Further byproducts given; | A 70% B 7.2% C 13.4% D 8.2% |
- 523-27-3
9,10-Dibromoanthracene
- 121-69-7
N,N-dimethyl-aniline
A
- 1564-64-3
9-Bromoanthracene
B
- 25882-75-1
9-<4-(N,N-dimethylamino)phenyl>-9,10-dihydroanthracene
C
- 3571-43-5
crystal violet bromide
D
- 101-61-1
4,4'-methylene-bis(N,N-dimethylaniline)
| Conditions | Yield |
|---|---|
| In acetonitrile Product distribution; Irradiation; photolysis; | A 70% B 7.2% C 1.2% D 13.4% E 8.2% |
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In chloroform at 60℃; for 2h; Inert atmosphere; | 61.2% |
- 523-27-3
9,10-Dibromoanthracene
- 100-67-4
potassium phenolate
A
- 1564-64-3
9-Bromoanthracene
B
- 23674-00-2
bromo-9 phenoxy-10 anthracene
C
- 84-65-1
9,10-phenanthrenequinone
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 153℃; for 3h; | A 3% B 35% C 2% |
| Conditions | Yield |
|---|---|
| Kinetics; |
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Chemistry
Molecule structure of 9-Bromoanthracene (CAS NO.1564-64-3):
IUPAC Name: 9-Bromoanthracene
Molecular Weight: 257.12526 g/mol
Molecular Formula: C14H9Br
Density: 1.479 g/cm3
Melting Point: 97-100 °C(lit.)
Boiling Point: 389.7 °C at 760 mmHg
Flash Point: 190.3 °C
Index of Refraction: 1.733
Molar Refractivity: 69.62 cm3
Molar Volume: 173.8 cm3
Surface Tension: 51.3 dyne/cm
Enthalpy of Vaporization: 61.41 kJ/mol
Vapour Pressure: 6.28E-06 mmHg at 25 °C
Storage Temp.: 0-6 °C
XLogP3: 5.2
Exact Mass: 255.988763
MonoIsotopic Mass: 255.988763
Canonical SMILES: C1=CC=C2C(=C1)C=C3C=CC=CC3=C2Br
InChI: InChI=1S/C14H9Br/c15-14-12-7-3-1-5-10(12)9-11-6-2-4-8-13(11)14/h1-9H
InChIKey: ZIRVQSRSPDUEOJ-UHFFFAOYSA-N
EINECS: 216-359-3
Product Categories: Aromatic Compounds; blocks; Bromides; Aromatic Halides (substituted); Anthracenes; Anthracene series; Aryl; C13 to C37+; Halogenated Hydrocarbons
Safety Profile
Hazard Codes: 
Xi
Safety Statements: 22-24/25
S22:Do not breathe dust.
S24/25:Avoid contact with skin and eyes.
WGK Germany: 3
Hazard Note: Irritant
May cause eye irritation. if absorbed through the skin，it will cause skin irritation.
Ingestion:if swallowed，it May cause the irritation of digestive tract.if inhaled.it May be harmful for your respiratory.
Specification
9-Bromoanthracene (CAS NO.1564-64-3) is also named as NSC 803 ; Anthracene, 9-bromo- ; 10-Bromoanthracene ; 9-Anthracenyl bromide ; 9-Bromo anthracene . 9-Bromoanthracene (CAS NO.1564-64-3) is white to light yellow crystal powder.
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