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1572-99-2

Basic Information
CAS No.: 1572-99-2
Name: Ethyl 2-cyanopropanoate
Article Data: 41
Molecular Structure:
Molecular Structure of 1572-99-2 (Ethyl 2-cyanopropanoate)
Formula: C6H9NO2
Molecular Weight: 127.143
Synonyms: Propionicacid, 2-cyano-, ethyl ester (6CI,7CI,8CI);2-Cyanopropanoic acid ethyl ester;Ethyl 2-cyanopropanoate;Ethyl 2-cyanopropionate;Ethyl a-cyanopropionate;NSC 68508;
EINECS: 216-393-9
Density: 1.019 g/cm3
Boiling Point: 194.452 °C at 760 mmHg
Flash Point: 78.871 °C
Risk Codes: 20/21/22-36/37/38
Safety: 23-36/37/39
PSA: 50.09000
LogP: 0.70918
Synthetic route
109-06-8

α-picoline

Co2 (CO)8

Co2 (CO)8

107-13-1

acrylonitrile

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
In ethanol95%
7085-85-0

ethyl 2-cyanoacrylate

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
With trifluoroacetic acid at 0℃;85%
With trifluoroacetic acid at 0℃; Mechanism;85%
With hydrogen; hydrotalcite-supported palladium nanoparticles; palladium In toluene at 60℃; under 760 Torr; for 1h;
105-56-6

ethyl 2-cyanoacetate

74-88-4

methyl iodide

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
Stage #1: ethyl 2-cyanoacetate With sodium hydride In tetrahydrofuran; paraffin oil at 0℃; for 0.25h; Inert atmosphere;
Stage #2: methyl iodide In tetrahydrofuran; paraffin oil at 0 - 20℃; for 3h; Inert atmosphere;
83%
Stage #1: ethyl 2-cyanoacetate With potassium carbonate In acetonitrile at 20℃; for 0.25h;
Stage #2: methyl iodide In acetonitrile at 20℃; for 6h;
41%
With potassium hydroxide In ethanol at 0℃; for 4h;
68897-45-0

N,N,N',N',N'',N''-Hexamethylguanidiniumcyanid

535-11-5, 41978-69-2

Ethyl 2-bromopropionate

A

1572-99-2

ethyl 2-cyanopropionate

B

6926-43-8

1,1,2,2,3,3-Hexamethylguanidiniumbromid

Conditions
ConditionsYield
In dichloromethane at 40℃; for 18h;A 73%
B n/a
64-17-5

ethanol

201230-82-2

carbon monoxide

107-13-1

acrylonitrile

122-57-6

1-Phenylbut-1-en-3-one

A

10137-67-4

ethyl 3-cyanopropionate

B

30378-23-5

2,4-dicyano-2-methylbutanoic acid ethyl ester

C

115906-97-3

2-cyano-5-oxo-3-phenyl-2-methylhexanoic acid ethyl ester

D

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
With pyridine; dicobalt octacarbonyl at 110℃; under 75005.9 Torr; Further byproducts given;A n/a
B 59%
C 10%
D n/a
64-17-5

ethanol

201230-82-2

carbon monoxide

107-13-1

acrylonitrile

140-88-5

ethyl acrylate

A

10137-67-4

ethyl 3-cyanopropionate

B

30378-23-5

2,4-dicyano-2-methylbutanoic acid ethyl ester

C

91341-03-6

2-cyano-2-methyl-1,5-pentanedioic acid bis(ethyl ester)

D

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
With pyridine; dicobalt octacarbonyl at 110℃; under 75005.9 Torr; Further byproducts given;A n/a
B 44%
C 5%
D n/a
773837-37-9

sodium cyanide

535-11-5, 41978-69-2

Ethyl 2-bromopropionate

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide at 23℃; for 12h;30%
632-07-5

2-cyanopropanoic acid

64-17-5

ethanol

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
With sulfuric acid
64-17-5

ethanol

151-50-8

potassium cyanide

535-11-5, 41978-69-2

Ethyl 2-bromopropionate

A

54677-60-0

diethyl 2,3-dimethyl-2-cyanosuccinate

B

1572-99-2

ethyl 2-cyanopropionate

541-41-3

chloroformic acid ethyl ester

107-12-0

propiononitrile

1572-99-2

ethyl 2-cyanopropionate

Conditions
ConditionsYield
With diethyl ether; sodium
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    Product Name: Ethyl 2-cyanopropanoate CAS: 1572-99-2 MF: C6H9NO2 MW: 127.14 EINECS: 216-393-9 Mol File: 1572-99-2.mol Ethyl 2-cyanopropanoate Structure Ethyl 2-cyanopropanoate Chemical Properties Boiling point 193 °C densi

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  • Propanoic acid,2-cyano-, ethyl ester

  • Casno:

    1572-99-2

    Propanoic acid,2-cyano-, ethyl ester

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  • 1572-99-2 CAS No.1572-99-2

  • Casno:

    1572-99-2

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Chemistry

Molecular Structure:

Molecular Formula: C6H9NO2
Molecular Weight: 127.1412
IUPAC Name: Ethyl 2-cyanopropanoate
Synonyms of Ethyl 2-cyanopropionate (CAS NO.1572-99-2): AI3-05609 ; EINECS 216-393-9 ; Propanoic acid, 2-cyano-, ethyl ester
CAS NO: 1572-99-2 
Index of Refraction: 1.418
Molar Refractivity: 31.49 cm3
Molar Volume: 124.8 cm3
Surface Tension: 33.9 dyne/cm
Density: 1.018 g/cm3
Flash Point: 78.9 °C
Enthalpy of Vaporization: 43.06 kJ/mol
Boiling Point: 194.5 °C at 760 mmHg
Vapour Pressure of Ethyl 2-cyanopropionate (CAS NO.1572-99-2): 0.441 mmHg at 25°C

Safety Profile

Risk Statements of Ethyl 2-cyanopropionate (CAS NO.1572-99-2): 20/21/22-36/37/38 
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed. 
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 23-36/37/39 
S23: Do not breathe vapour. 
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
RIDADR: 3276