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Basic Information
CAS No.: 1609373-99-0
Name: 2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine
Article Data: 5
Molecular Structure:
Molecular Structure of 1609373-99-0 (2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine)
Formula: N/A
Molecular Weight: 260.295
Synonyms: 1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
Density: 1.248±0.06 g/cm3(Predicted)
Boiling Point: 444.0±40.0 °C(Predicted)
Related products
Synthetic route
109-04-6

2-bromo-pyridine

1609374-04-0

2-methyl-8-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzofuro[2,3-b]pyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Stage #1: 2-bromo-pyridine; 2-methyl-8-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzofuro[2,3-b]pyridine With potassium carbonate In tetrahydrofuran for 0.5h; Inert atmosphere;
Stage #2: With tetrakis(triphenylphosphine) palladium(0) at 80℃; for 12h;		80%
1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

pyridin-2-ylzinc(II) bromide

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); XPhos In tetrahydrofuran at 60 - 65℃; for 12h;65%
40972-86-9

(2,3-dimethoxyphenyl)boronic acid

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 5 h / Reflux
2: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
3: pyridine hydrochloride / 15 h / 200 °C
4: pyridine / dichloromethane / 0 °C
5: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
126325-46-0

2-amino-3-bromo-6-methyl-pyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 5 h / Reflux
2: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
3: pyridine hydrochloride / 15 h / 200 °C
4: pyridine / dichloromethane / 0 °C
5: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
1609373-95-6

3-(2,3-dimethoxyphenyl)-6-methylpyridin-2-amine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
2: pyridine hydrochloride / 15 h / 200 °C
3: pyridine / dichloromethane / 0 °C
4: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
1609373-96-7

8-methoxy-2-methylbenzofuro[2,3-b]pyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine hydrochloride / 15 h / 200 °C
2: pyridine / dichloromethane / 0 °C
3: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
Multi-step reaction with 3 steps
1: pyridine hydrochloride / 200 °C
2: dichloromethane / 0 - 20 °C
3: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
1609373-97-8

2-methylbenzofuro[2,3-b]pyridine-8-ol

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 0 °C
2: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene / 1,4-dioxane / 80 °C
2.1: potassium carbonate / tetrahydrofuran / 0.5 h / Inert atmosphere
2.2: 12 h / 80 °C
View Scheme
109-04-6

2-bromo-pyridine

1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
With magnesium In tetrahydrofuran at 35 - 45℃;
1824-81-3

2-Amino-6-methylpyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: N-chloro-succinimide; bromine / tetrahydrofuran / 25 - 30 °C
2: toluene; ethanol; water / Reflux
3: acetic acid; tert.-butylnitrite / tetrahydrofuran / -20 °C
4: hydrogen; sodium carbonate; palladium on activated charcoal / tetrahydrofuran / 20 - 60 °C
5: pyridine hydrochloride / 200 °C
6: dichloromethane / 0 - 20 °C
7: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
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