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1609373-99-0

Basic Information
CAS No.: 1609373-99-0
Name: 1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
Article Data: 5
Cas Database
Molecular Structure:
Molecular Structure of 1609373-99-0 (1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine)
Formula: N/A
Molecular Weight: 260.295
Synonyms: 1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
EINECS: N/A
Density: N/A
Melting Point: N/A
Boiling Point: N/A
Flash Point: N/A
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety:
Transport Information: N/A
PSA: N/A
LogP: N/A
Synthetic route
109-04-6

2-bromo-pyridine

1609374-04-0

2-methyl-8-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzofuro[2,3-b]pyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Stage #1: 2-bromo-pyridine; 2-methyl-8-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzofuro[2,3-b]pyridine With potassium carbonate In tetrahydrofuran for 0.5h; Inert atmosphere;
Stage #2: With tetrakis(triphenylphosphine) palladium(0) at 80℃; for 12h;
80%
1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

pyridin-2-ylzinc(II) bromide

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); XPhos In tetrahydrofuran at 60 - 65℃; for 12h;65%
40972-86-9

(2,3-dimethoxyphenyl)boronic acid

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 5 h / Reflux
2: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
3: pyridine hydrochloride / 15 h / 200 °C
4: pyridine / dichloromethane / 0 °C
5: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
126325-46-0

2-amino-3-bromo-6-methyl-pyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 5 h / Reflux
2: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
3: pyridine hydrochloride / 15 h / 200 °C
4: pyridine / dichloromethane / 0 °C
5: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
1609373-95-6

3-(2,3-dimethoxyphenyl)-6-methylpyridin-2-amine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
2: pyridine hydrochloride / 15 h / 200 °C
3: pyridine / dichloromethane / 0 °C
4: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
1609373-96-7

8-methoxy-2-methylbenzofuro[2,3-b]pyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine hydrochloride / 15 h / 200 °C
2: pyridine / dichloromethane / 0 °C
3: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
Multi-step reaction with 3 steps
1: pyridine hydrochloride / 200 °C
2: dichloromethane / 0 - 20 °C
3: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
1609373-97-8

2-methylbenzofuro[2,3-b]pyridine-8-ol

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 0 °C
2: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene / 1,4-dioxane / 80 °C
2.1: potassium carbonate / tetrahydrofuran / 0.5 h / Inert atmosphere
2.2: 12 h / 80 °C
View Scheme
109-04-6

2-bromo-pyridine

1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
With magnesium In tetrahydrofuran at 35 - 45℃;
1824-81-3

2-Amino-6-methylpyridine

1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: N-chloro-succinimide; bromine / tetrahydrofuran / 25 - 30 °C
2: toluene; ethanol; water / Reflux
3: acetic acid; tert.-butylnitrite / tetrahydrofuran / -20 °C
4: hydrogen; sodium carbonate; palladium on activated charcoal / tetrahydrofuran / 20 - 60 °C
5: pyridine hydrochloride / 200 °C
6: dichloromethane / 0 - 20 °C
7: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
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    Product Name: 2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine Synonyms: 2-methyl-8-(2-pyridinyl)Benzofuro[2,3-b]pyridine;2-methyl-8(pyridin-2-yl)benzofuro[2,3-b]bipyridine;2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine;

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    FOB Price:  USD $ 0.0-0.0/Gram

    Our company advantages: 1. The highest quality with the competitive price. 2. Professional human services. 3. The fastest and safest delivery service. 4. The high purity products. 5. We have a sufficient supply of stock. 6. A variety of

    Zhengzhou HQ material Co.,Ltd located in Zhengzhou High-tech Zone,is a High-tech manufacturer, which integrating R&D, manufacturing and sales.The company is committed to provide c

  • Zhengzhou HQ Material Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-371-67759225

    Address:No.32, Jinsuo Road, High-tech Zone

       Inquiry Now

  • 2-Methyl-8-(pyridin-2-yl)
benzofuro[2,3-b]pyridine

  • Casno:

    1609373-99-0

    2-Methyl-8-(pyridin-2-yl) benzofuro[2,3-b]pyridine

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

    Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

    Changzhou Extraordinary Pharmatech co., LTD. Is a full technical team and for the development of hardware and software facilities manufacturing enterprises,The company is located i

  • Changzhou Extraordinary Pharmatech co.,LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 519 82111935

    Address:Chinese Jiangsu Province Changzhou City Jintan District Jincheng Town Miaotou NO4(Pharmaceutical Park)

       Inquiry Now

  • National Research Platform  ISO 9001  1609373-99-0

  • Casno:

    1609373-99-0

    National Research Platform ISO 9001 1609373-99-0

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    Zhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The laboratory covers 600 m2 and the pilot plant covers 2000 m2. Kingorgchem i

    Zhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The

  • Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-371-65511936

    Address:NO.56,Hongzhuan Road

       Inquiry Now

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